Return to study ST000473 main page
MB Sample ID: SA024092
Local Sample ID: | AG290615_60 |
Subject ID: | SU000494 |
Subject Type: | Chemical |
Subject Species: | None |
Subject Comments: | Primary standards of nucleotide triphosphates (ATP, GTP, UTP and CTP). |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN000737 |
---|---|
Analysis type | MS |
Chromatography type | HILIC |
Chromatography system | Waters Acquity |
Column | Phenomenex Luna NH2 (100 x 2.0mm,3um) |
MS Type | ESI |
MS instrument type | QTOF |
MS instrument name | Waters Synapt-G2-Si |
Ion Mode | NEGATIVE |
Units | Peak area |
Chromatography:
Chromatography ID: | CH000530 |
Chromatography Summary: | Untargeted HILIC Method |
Instrument Name: | Waters Acquity |
Column Name: | Phenomenex Luna NH2 (100 x 2.0mm,3um) |
Column Temperature: | 20C |
Flow Gradient: | 30% eluent A to 99% eluent A in 8 min, followed by isocratic elution at 99% eluent A until 14 min. A conditioning cycle of 6 min with the initial proportions of eluents A and B was performed prior to the next analysis. |
Flow Rate: | 0.25 mL/min |
Sample Injection: | 10 µL |
Solvent A: | 100% water; 5 mM ammonium acetate, pH 9.9 |
Solvent B: | 100% acetonitrile |
Analytical Time: | 20 min |
Chromatography Type: | HILIC |