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MB Sample ID: SA051139
Local Sample ID: | S18 |
Subject ID: | SU000915 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Age Or Age Range: | 13 - 66 |
Gender: | Female and Male |
Human Ethnicity: | Brazillian |
Human Inclusion Criteria: | Retrospective serum samples from leprosy patients diagnosed or not with type 1 reaction that were not receiving multidrug therapy or corticosteroid therapy at the time of blood collection. |
Human Exclusion Criteria: | Retrospective serum samples from leprosy patients that were under multidrug therapy and/or corticosteroid therapy at the time of blood collection were excluded from the study. |
Subject Comments: | The patients exhibited borderline tuberculoid, borderline borderline and borderline lepromatous forms of leprosy and was diagnosed or not with type 1 reaction. |
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Combined analysis:
Analysis ID | AN001437 |
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Analysis type | MS |
Chromatography type | Reversed phase |
Chromatography system | Agilent 1290 |
Column | Waters Xbridge BEH C18 XP (100 x 2.1mm,2.5um) |
MS Type | ESI |
MS instrument type | QTOF |
MS instrument name | Agilent 6510 QTOF |
Ion Mode | NEGATIVE |
Units | arbitrary units |
Chromatography:
Chromatography ID: | CH001008 |
Chromatography Summary: | This analysis was performed only on negative mode. The solvent gradient used for all chromatography was 2% solvent B for 3 min followed by a 15 min linear gradient of 2% to 98% solvent B, which was held for 0.3 min. Then returned to starting conditions over 1.2 min. |
Instrument Name: | Agilent 1290 |
Column Name: | Waters Xbridge BEH C18 XP (100 x 2.1mm,2.5um) |
Column Temperature: | 50C |
Flow Gradient: | 0.25 mL/min |
Flow Rate: | 0.25 mL/min |
Injection Temperature: | 4C |
Sample Injection: | 20uL |
Solvent A: | 89% water/5% acetonitrile/5% isopropanol; 5 mM ammonium acetate |
Solvent B: | 50% acetonitrile/50% isopropanol; 5 mM ammonium acetate |
Capillary Voltage: | 2.8 kV |
Chromatography Type: | Reversed phase |