Return to study ST000991 main page
MB Sample ID: SA061356
Local Sample ID: | GLA_X500R_Lipids_SO103_SA108_1006eG1 |
Subject ID: | SU001030 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN001617 |
---|---|
Analysis type | MS |
Chromatography type | Reversed phase |
Chromatography system | Sciex X500R QTOF |
Column | Waters Acquity CSH C18 (100 x 2.1mm,1.7um) |
MS Type | ESI |
MS instrument type | QTOF |
MS instrument name | ABI Sciex X500R QTOF |
Ion Mode | POSITIVE |
Units | nanograms (absolute) |
Chromatography:
Chromatography ID: | CH001139 |
Methods Filename: | Data_Dictionary_Fiehn_laboratory_CSH_QTOF_lipidomics_05-29-2014.pdf |
Instrument Name: | Sciex X500R QTOF |
Column Name: | Waters Acquity CSH C18 (100 x 2.1mm,1.7um) |
Column Pressure: | 450-850 bar |
Column Temperature: | 65 C |
Flow Gradient: | 15% B to 99% B |
Flow Rate: | 0.6 mL/min |
Injection Temperature: | 4 C |
Internal Standard: | See data dictionary |
Retention Time: | See data dictionary |
Sample Injection: | 1.67 uL |
Solvent A: | 60% acetonitrile/40% water; 10mM formic acid; 10mM ammonium formate |
Solvent B: | 90% isopropanol/10% acetonitrile; 10mM formic acid; 10mM ammonium formate |
Analytical Time: | 13 min |
Capillary Voltage: | 3500 eV |
Oven Temperature: | 50°C for 1 min, then ramped at 20°C/min to 330°C, held constant for 5 min |
Time Program: | 15 min |
Washing Buffer: | Ethyl Acetate |
Weak Wash Solvent Name: | Isopropanol |
Strong Wash Solvent Name: | Isopropanol |
Target Sample Temperature: | Autosampler temp 4 C |
Sample Loop Size: | 30 m length x 0.25 mm internal diameter |
Randomization Order: | Excel generated |
Chromatography Type: | Reversed phase |