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MB Sample ID: SA092131
Local Sample ID: | GLD036 |
Subject ID: | SU001336 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Gender: | Male and female |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN002105 | AN002106 | AN002107 | AN002108 |
---|---|---|---|---|
Analysis type | MS | MS | MS | MS |
Chromatography type | Reversed phase | Reversed phase | HILIC | HILIC |
Chromatography system | Agilent 1290 | Agilent 1290 | Agilent 1290 | Agilent 1290 |
Column | Agilent Zorbax RRHD SB-C18 (100 x 2.1mm,1.8um) | Agilent Zorbax RRHD SB-C18 (100 x 2.1mm,1.8um) | Phenomenex Kinetex HILIC 100A (50 x 2.1 mm,2.6um) | Phenomenex Kinetex HILIC 100A (50 x 2.1 mm,2.6um) |
MS Type | ESI | ESI | ESI | ESI |
MS instrument type | QTOF | QTOF | QTOF | QTOF |
MS instrument name | Agilent 6520 QTOF | Agilent 6520 QTOF | Agilent 6550 QTOF | Agilent 6550 QTOF |
Ion Mode | POSITIVE | NEGATIVE | POSITIVE | NEGATIVE |
Units | Abundance | Abundance | Abundance | Abundance |
Chromatography:
Chromatography ID: | CH001537 |
Chromatography Summary: | Gradient was as follows: 0–1 minutes 30–70% B, 1–7.92 minutes 70–100% B, 7.92–10.4 minutes 100% B, 10.4–10.5 minutes 100–30% B, 10.5–15.1 minutes 30% B. |
Instrument Name: | Agilent 1290 |
Column Name: | Agilent Zorbax RRHD SB-C18 (100 x 2.1mm,1.8um) |
Column Temperature: | 60 °C |
Flow Rate: | 0.7 mL/min |
Injection Temperature: | 4 °C |
Solvent A: | 100% water; 0.1% formic acid |
Solvent B: | 60% isopropanol/36% acetonitrile/4% water; 0.1% formic acid |
Chromatography Type: | Reversed phase |
Chromatography ID: | CH001538 |
Chromatography Summary: | Gradient elution was as follows: 0–2 minutes 100% B, 2–2.1 minutes 100–90% B, 2.1–8.6 minutes 90–50% B, 8.6–8.7 minutes 50–0% B, 8.7–14.7 minutes 0% B, 14.7–14.8 minutes 0–100% B, 14.8–24.8 minutes 100% B. |
Instrument Name: | Agilent 1290 |
Column Name: | Phenomenex Kinetex HILIC 100A (50 x 2.1 mm,2.6um) |
Column Temperature: | 20 °C |
Flow Rate: | 0.6 mL/min |
Injection Temperature: | 4 °C |
Solvent A: | 50% acetonitrile/50% water; ammonium acetate, pH 5.8 |
Solvent B: | 90% acetonitrile/10% water; pH 5.8 ammonium acetate |
Chromatography Type: | HILIC |