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MB Sample ID: SA216332
Local Sample ID: | Plasma04-02_9_1_2839 |
Subject ID: | SU002336 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Age Or Age Range: | 39.48 +-10.0 |
Weight Or Weight Range: | 29.09 +-4.76 |
Gender: | Male and female |
Human Inclusion Criteria: | Overweight (BMI>=25), otherwise healthy, between 18 and 60 years, no chronic disease, willingness to observe Ramadan Fasting |
Human Exclusion Criteria: | Medication use within 1 week, bariatric surgery within 6 months, or any weight reduction regimen within 1 month of the commencement of Ramadan |
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Combined analysis:
Analysis ID | AN003676 |
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Analysis type | MS |
Chromatography type | Reversed phase |
Chromatography system | Bruker Elute |
Column | Hamilton Intensity Solo 2 C18 |
MS Type | ESI |
MS instrument type | QTOF |
MS instrument name | Bruker timsTOF |
Ion Mode | POSITIVE |
Units | AU |
Chromatography:
Chromatography ID: | CH002726 |
Chromatography Summary: | Samples were chromatographically separated using a Hamilton® Intensity Solo 2 C18 column (100 mm x 2.1 mm x 1.8 µm) and eluted using 0.1% formic acid in water (A) and 0.1% formic acid in ACN (B) using the following gradient: at a flow rate of 0.250 ml/min 1% B from 0-2 min, then gradient elution to 99% B from 2-17 min, held at 99% B from 17-20 min, then re-equilibrated to 1% B from 20-30 min using a flow rate of 0.350 ml/min. The autosampler temperature was set at 8℃ and the column oven temperature at 35℃. |
Instrument Name: | Bruker Elute |
Column Name: | Hamilton Intensity Solo 2 C18 |
Column Temperature: | 35 |
Flow Gradient: | 1%B to 99%B in 15 min |
Flow Rate: | 250 uL/min |
Solvent A: | 100% water; 0.1% formic acid |
Solvent B: | 100% acetonitrile; 0.1% formic acid |
Oven Temperature: | 35C |
Chromatography Type: | Reversed phase |