Return to study ST002496 main page
MB Sample ID: SA256806
Local Sample ID: | sample_0075 |
Subject ID: | SU002655 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Gender: | Not applicable |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN004206 |
---|---|
Analysis type | MS |
Chromatography type | Reversed phase |
Chromatography system | Agilent 1290 Infinity II |
Column | Waters ACQUITY UPLC BEH C18 (100 x 2.1mm,1.7um) |
MS Type | ESI |
MS instrument type | QTOF |
MS instrument name | Agilent 6545 QTOF |
Ion Mode | NEGATIVE |
Units | ng/ml |
Chromatography:
Chromatography ID: | CH003117 |
Instrument Name: | Agilent 1290 Infinity II |
Column Name: | Waters ACQUITY UPLC BEH C18 (100 x 2.1mm,1.7um) |
Column Temperature: | 50 |
Flow Gradient: | from min 0-1.5, the percentage of phase B was increased from 5% to 30%, from min 1.5-4.5, the percentage of B was increased to 70%, from min 4.5-7.5 the percentage of B was increased to 100% and held for 5.5 mins. A post-time of 5 min was used to regain the initial conditions for the next analysis. |
Flow Rate: | 0.4 mL/min |
Solvent A: | 70% water/30% methanol; 2mM ammonium acetate |
Solvent B: | 100% methanol; 2mM ammonium acetate |
Chromatography Type: | Reversed phase |