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MB Sample ID: SA323895
Local Sample ID: | 5Ax* |
Subject ID: | SU003098 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Age Or Age Range: | < 5 years old |
Gender: | Male and female |
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Combined analysis:
Analysis ID | AN004905 |
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Analysis type | MS |
Chromatography type | Reversed phase |
Chromatography system | Thermo Dionex Ultimate 3000 |
Column | Waters ACQUITY UPLC HSS T3 (150 x 2.1mm,1.8um) |
MS Type | ESI |
MS instrument type | Orbitrap |
MS instrument name | Thermo Q Exactive Orbitrap |
Ion Mode | UNSPECIFIED |
Units | a.u. |
Chromatography:
Chromatography ID: | CH003700 |
Instrument Name: | Thermo Dionex Ultimate 3000 |
Column Name: | Waters ACQUITY UPLC HSS T3 (150 x 2.1mm,1.8um) |
Column Temperature: | 45 |
Flow Gradient: | A gradient profile with following proportions (v/v) of solvent A was applied: 0-1.5 min at 98%, 1.5-7.0 min from 98% to 75%, 7.0-8.0 min from 75% to 40%, 8.0-12.0 min from 40% to 5%, 12.0-14.0 min at 5%, 14.0-14.1 min from 5 to 98%, followed by 4.0 min of re-equilibration. |
Flow Rate: | 0.4 mL/min |
Internal Standard: | L-alanine-d3, D-valine-d8 |
Sample Injection: | 10 uL |
Solvent A: | 0.1% formic acid in ultrapure water |
Solvent B: | 0.1% formic acid in acetonitrile |
Chromatography Type: | Reversed phase |