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MB Sample ID: SA338749
Local Sample ID: | S159_LP |
Subject ID: | SU003241 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN005119 | AN005120 | AN005121 | AN005122 |
---|---|---|---|---|
Analysis type | MS | MS | MS | MS |
Chromatography type | Reversed phase | Reversed phase | HILIC | HILIC |
Chromatography system | Thermo Dionex Ultimate 3000 | Thermo Dionex Ultimate 3000 | Thermo Dionex Ultimate 3000 | Thermo Dionex Ultimate 3000 |
Column | Waters ACQUITY UPLC CSH C18 (100 x 2.1mm,1.7um) | Waters ACQUITY UPLC CSH C18 (100 x 2.1mm,1.7um) | Waters ACQUITY UPLC BEH Amide (150 x 2.1mm,1.7um) | Waters ACQUITY UPLC BEH Amide (150 x 2.1mm,1.7um) |
MS Type | ESI | ESI | ESI | ESI |
MS instrument type | Orbitrap | Orbitrap | Orbitrap | Orbitrap |
MS instrument name | Thermo Q Exactive Plus Orbitrap | Thermo Q Exactive Plus Orbitrap | Thermo Q Exactive Orbitrap | Thermo Q Exactive Orbitrap |
Ion Mode | POSITIVE | NEGATIVE | POSITIVE | NEGATIVE |
Units | Peak area | Peak area | Peak area | Peak area |
Chromatography:
Chromatography ID: | CH003873 |
Chromatography Summary: | Chromatography methods for lipid extract, positive-ion mode. |
Instrument Name: | Thermo Dionex Ultimate 3000 |
Column Name: | Waters ACQUITY UPLC CSH C18 (100 x 2.1mm,1.7um) |
Column Temperature: | 50℃ |
Flow Gradient: | 0–1 min, 15% B; 1–15 min, 15–70% B; 15-16 min, 70–99% B; 16–18.5 min, 99% B; 18.5–19 min, 99–15% B; and 19-–21 min, 15% B |
Flow Rate: | 0.2 mL/min |
Solvent A: | Acetonitrile/water (4/6); 0.1% formic acid |
Solvent B: | Isopropyl alcohol/acetonitrile (9/1); 0.1% formic acid |
Chromatography Type: | Reversed phase |
Chromatography ID: | CH003874 |
Chromatography Summary: | Chromatography methods for lipid extract, negative-ion mode. |
Instrument Name: | Thermo Dionex Ultimate 3000 |
Column Name: | Waters ACQUITY UPLC CSH C18 (100 x 2.1mm,1.7um) |
Column Temperature: | 50℃ |
Flow Gradient: | 0–0.5 min, 15% B; 0.5–4 min, 15–70% B; 4–15 min, 70–99% B; 15–16.5 min, 99% B; 16.15–17 min, 99–15% B; and 17–19 min, 15% B |
Flow Rate: | 0.2 mL/min |
Solvent A: | Acetonitrile/water (4/6); 5 mM ammonium acetate |
Solvent B: | Isopropyl alcohol/acetonitrile (9/1); 5 mM ammonium acetate |
Chromatography Type: | Reversed phase |
Chromatography ID: | CH003875 |
Chromatography Summary: | Chromatography methods for metabolite extract, positive-ion mode. |
Instrument Name: | Thermo Dionex Ultimate 3000 |
Column Name: | Waters ACQUITY UPLC BEH Amide (150 x 2.1mm,1.7um) |
Column Temperature: | 40℃ |
Flow Gradient: | 0–1 min, 90% B; 1–9 min, 90-40% B; 9–11.5 min, 40% B; 11.5–12 min, 40–90% B; and 12–14 min, 90% B |
Flow Rate: | 0.25 mL/min |
Solvent A: | 100% Water; 0.1% formic acid |
Solvent B: | 100% Acetonitrile; 0.1% formic acid |
Chromatography Type: | HILIC |
Chromatography ID: | CH003876 |
Chromatography Summary: | Chromatography methods for metabolite extract, negative-ion mode. |
Instrument Name: | Thermo Dionex Ultimate 3000 |
Column Name: | Waters ACQUITY UPLC BEH Amide (150 x 2.1mm,1.7um) |
Column Temperature: | 40℃ |
Flow Gradient: | 0–1 min, 90% B; 1–9 min, 90-40% B; 9–11.5 min, 40% B; 11.5–12 min, 40–90% B; and 12–14 min, 90% B |
Flow Rate: | 0.25 mL/min |
Solvent A: | 100% Water; 5 mM ammonium acetate |
Solvent B: | 100% Acetonitrile; 5 mM ammonium acetate |
Chromatography Type: | HILIC |