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MB Sample ID: SA258032
Local Sample ID: | 2021-11-29_005_H2_E2 |
Subject ID: | SU002668 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Gender: | Male |
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Combined analysis:
Analysis ID | AN004228 |
---|---|
Analysis type | MS |
Chromatography type | Reversed phase |
Chromatography system | Agilent 6530 qTOF |
Column | Agilent Zorbax Extend C18 (150 x 2.1mm, 1.8um) with matched guard column |
MS Type | ESI |
MS instrument type | QTOF |
MS instrument name | Agilent 6530 QTOF |
Ion Mode | NEGATIVE |
Units | EicCoreArea/Peak Area |
MS:
MS ID: | MS003975 |
Analysis ID: | AN004228 |
Instrument Name: | Agilent 6530 QTOF |
Instrument Type: | QTOF |
MS Type: | ESI |
MS Comments: | MS acquisition was performed in negative ion mode, scan rate 2 spectra/sec, mass range 50-1200 m/z. Source parameters were: drying gas temperature 250°C, drying gas flow rate 13 L/min, nebulizer pressure 35 psig, sheath gas temp 325°C and flow 12 l/min, capillary voltage 3500V, internal reference mass correction enabled. Data analysis was performed using Agilent Profinder 10.0 software in batch isotopologue extraction mode with automated natural isotope abundance correction enabled. Compound identification was performed by matching accurate mass and retention time to those of authentic standards analyzed using the same method. |
Ion Mode: | NEGATIVE |
Capillary Voltage: | 3500V |
Dry Gas Flow: | 13L/min |
Dry Gas Temp: | 250 C |
Fragment Voltage: | 150V |
Nebulizer: | 35 psig |