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MB Sample ID: SA323852
Local Sample ID: | 66 |
Subject ID: | SU003097 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Gender: | Male and female |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN004903 | AN004904 |
---|---|---|
Analysis type | MS | MS |
Chromatography type | Ion exchange | Reversed phase |
Chromatography system | Thermo Dionex ICS-5000+ | Shimadzu Nexera X2 |
Column | Dionex IonPac AS11-HC (250 x 2mm, 4um) | Sigma-Aldrich Discovery HS F5-3 (150 x 2.1 mm, 3 um) |
MS Type | ESI | ESI |
MS instrument type | Orbitrap | Triple quadrupole |
MS instrument name | Thermo Q Exactive Focus | LCMS-8060, Shimadzu Corporation |
Ion Mode | UNSPECIFIED | UNSPECIFIED |
Units | Peak area/Internal Standard | Peak area/Internal Standard |
MS:
MS ID: | MS004646 |
Analysis ID: | AN004903 |
Instrument Name: | Thermo Q Exactive Focus |
Instrument Type: | Orbitrap |
MS Type: | ESI |
MS Comments: | For IC-HR-MS data analysis, the Trace Finder compound identification and confirmation setup parameters included a molecular ion intensity threshold override of 10,000, S/N 5, and mass tolerance of 5 ppm. Isotope pattern analysis using a 90% fit threshold, 30% allowable relative intensity deviation, and 5 ppm mass deviation was also performed to ensure that the relative intensities of the M + 1 and/or M + 2 isotope peaks for each compound were consistent with the theoretical relative intensities. |
Ion Mode: | UNSPECIFIED |
MS ID: | MS004647 |
Analysis ID: | AN004904 |
Instrument Name: | LCMS-8060, Shimadzu Corporation |
Instrument Type: | Triple quadrupole |
MS Type: | ESI |
MS Comments: | For LC-MS/MS analysis, chromatographic peaks obtained with compound-specific SRM channels were integrated and manually reviewed. For a single target compound, one or more confirmatory SRM channels were set (if available) to confirm peak compound identification. Chromatograms were acquired using Lab Solutions (ver. 5.113, Shimadzu). Peak areas were determined using Data browser software. |
Ion Mode: | UNSPECIFIED |