INSTRUMENT CONTROL PARAMETERS: 5975C Inert XL MSD with Triple A ------------------------------------------------------------------ D:\Methods\MET_ROUTINE.M Fri Sep 18 14:28:03 2009 Control Information ------- ----------- Sample Inlet : GC Injection Source : CTC PAL ALS Mass Spectrometer : Enabled ============================================================================ CTCPAL METHOD ============================================================================ Injection Volume: 1.00 ul Syringe Size: 10ul Cycle File: GC-Inj CYCLE DETAILS --------------- Air Volume (µl): 0 Pre Clean with Solvent 1 (): 0 Pre Clean with Solvent 2 (): 0 Pre Clean with Sample (): 0 Filling Speed (µl/s): 2 Filling Strokes (): 5 Inject to: GC Inj1 Injection Speed (µl/s): 5 Pre Inject Delay (ms): 500 Post Inject Delay (ms): 500 Post Clean with Solvent 1 (): 6 Post Clean with Solvent 2 (): 6 Oven Equilibration Time 0.5 min Oven Program On 80 °C for 3.5 min then 65 °C/min to 315 °C for 0 min then 65 °C/min to 315 °C for 7.8 min Run Time 14.915 min Front Injector Front SS Inlet He Mode Split Heater On 250 °C Pressure On 8.4443 psi Total Flow On 5.7708 mL/min Septum Purge Flow On 3 mL/min Gas Saver On 30 mL/min After 3.5 min Split Ratio 2 :1 Split Flow 1.8472 mL/min Thermal Aux 2 {MSD Transfer Line} Heater On Temperature Program On 280 °C for 0 min Run Time 14.915 min Column #1 HP-5MS 5% Phenyl Methyl Silox: 446.64151 HP-5MS 5% Phenyl Methyl Silox 325 °C: 30 m x 250 µm x 0.25 µm In: Front SS Inlet He Out: Vacuum (Initial) 80 °C Pressure 8.4443 psi Flow 0.92359 mL/min Average Velocity 35.526 cm/sec Holdup Time 1.4074 min Flow Program Off 0.92359 mL/min for 0 min Run Time 14.915 min Aux Pressure 1 N2 Pressure Program Off 10 psi for 0 min Run Time 14.915 min Aux Pressure 2 N2 Pressure Program Off 10 psi for 0 min Run Time 14.915 min Aux Pressure 3 N2 Pressure Program Off 10 psi for 0 min Run Time 14.915 min Signals Test Plot Save Off Test Plot Save Off Test Plot Save Off Test Plot Save Off MS ACQUISITION PARAMETERS General Information ------- ----------- Tune File : atune.u Acquistion Mode : Scan in FastScan mode MS Information -- ----------- Solvent Delay : 4.00 min EMV Mode : Gain Factor Gain Factor : 5.00 Resulting EM Voltage : 1412 [Scan Parameters] Low Mass : 50.0 High Mass : 800.0 Threshold : 100 Sample # : 0 A/D Samples 1 Plot 2 low mass : 50.0 Plot 2 high mass : 550.0 [Data Filters] Mass Filter : Time Filter : Standard [MSZones] MS Source : 230 C maximum 250 C MS Quad : 150 C maximum 200 C END OF MS ACQUISITION PARAMETERS TUNE PARAMETERS for SN: US80838766 ----------------------------- Trace Ion Detection is OFF. EMISSION : 34.610 ENERGY : 69.922 REPELLER : 34.814 IONFOCUS : 90.157 ENTRANCE_LE : 16.000 EMVOLTS : 1223.529 Actual EMV : 1411.77 GAIN FACTOR : 5.01 AMUGAIN : 1614.000 AMUOFFSET : 121.688 FILAMENT : 2.000 DCPOLARITY : 0.000 ENTLENSOFFS : 18.322 MASSGAIN : -859.000 MASSOFFSET : -40.000 END OF TUNE PARAMETERS ------------------------------------ END OF INSTRUMENT CONTROL PARAMETERS ------------------------------------