{ "METABOLOMICS WORKBENCH":{"STUDY_ID":"ST000188","ANALYSIS_ID":"AN000289","VERSION":"1","CREATED_ON":"2016-09-17"}, "PROJECT":{"PROJECT_TITLE":"Murine AxP","PROJECT_SUMMARY":"Plasma Nucleotide/adenosine concentrations","INSTITUTE":"University of Michigan","DEPARTMENT":"Internal Medicine-Cardiology","LABORATORY":"Visovatti Lab","LAST_NAME":"Visovatti","FIRST_NAME":"Scott","ADDRESS":"Ann Arbor, MI","EMAIL":"shv@med.umich.edu","PHONE":"734-657-6917"}, "STUDY":{"STUDY_TITLE":"Murine apyrase","STUDY_TYPE":"This experiment was performed in wild type vs. CD39 knockout (KO) mice that had infusions of either saline or apyrase over the course of 2 weeks. Whole blood obtained via intracardiac puncture, and was drawn into a syringe prefilled with anti-enzyme stop solution.","STUDY_SUMMARY":"This experiment was performed in wild type vs. CD39 knockout (KO) mice that had infusions of either saline or apyrase over the course of 2 weeks. Whole blood obtained via intracardiac puncture, and was drawn into a syringe prefilled with anti-enzyme stop solution.","INSTITUTE":"University of Michigan","DEPARTMENT":"Biomedical Research Core Facilities","LABORATORY":"Metabolomics core","LAST_NAME":"Kachman","FIRST_NAME":"Maureen","ADDRESS":"6300 Brehm Tower, 1000 Wall Street, Ann Arbor, MI 48105-5714","EMAIL":"mkachman@umich.edu","PHONE":"-","NUM_GROUPS":"4","TOTAL_SUBJECTS":"15"}, "SUBJECT":{"SUBJECT_TYPE":"-","SUBJECT_SPECIES":"Mus musculus","TAXONOMY_ID":"10090"}, "SUBJECT_SAMPLE_FACTORS":[ { "Subject ID":"SU0011768", "Sample ID":"S00017521", "Factors":{"Type":"KO","Treatment":"apyrase"} }, { "Subject ID":"SU0011769", "Sample ID":"S00017522", "Factors":{"Type":"KO","Treatment":"apyrase"} }, { "Subject ID":"SU0011770", "Sample ID":"S00017523", "Factors":{"Type":"KO","Treatment":"apyrase"} }, { "Subject ID":"SU0011771", "Sample ID":"S00017524", "Factors":{"Type":"KO","Treatment":"apyrase"} }, { "Subject ID":"SU0011772", "Sample ID":"S00017525", "Factors":{"Type":"KO","Treatment":"apyrase"} }, { "Subject ID":"SU0011764", "Sample ID":"S00017517", "Factors":{"Type":"KO","Treatment":"saline"} }, { "Subject ID":"SU0011765", "Sample ID":"S00017518", "Factors":{"Type":"KO","Treatment":"saline"} }, { "Subject ID":"SU0011766", "Sample ID":"S00017519", "Factors":{"Type":"KO","Treatment":"saline"} }, { "Subject ID":"SU0011767", "Sample ID":"S00017520", "Factors":{"Type":"KO","Treatment":"saline"} }, { "Subject ID":"SU0011761", "Sample ID":"S00017514", "Factors":{"Type":"wild type","Treatment":"apyrase"} }, { "Subject ID":"SU0011762", "Sample ID":"S00017515", "Factors":{"Type":"wild type","Treatment":"apyrase"} }, { "Subject ID":"SU0011763", "Sample ID":"S00017516", "Factors":{"Type":"wild type","Treatment":"apyrase"} }, { "Subject ID":"SU0011758", "Sample ID":"S00017511", "Factors":{"Type":"wild type","Treatment":"saline"} }, { "Subject ID":"SU0011759", "Sample ID":"S00017512", "Factors":{"Type":"wild type","Treatment":"saline"} }, { "Subject ID":"SU0011760", "Sample ID":"S00017513", "Factors":{"Type":"wild type","Treatment":"saline"} } ], "COLLECTION":{"COLLECTION_SUMMARY":"-","SAMPLE_TYPE":"Plasma"}, "TREATMENT":{"TREATMENT_SUMMARY":"-"}, "SAMPLEPREP":{"SAMPLEPREP_SUMMARY":"-","SAMPLEPREP_PROTOCOL_FILENAME":"Gly-TCA-nucleotides_analysis_protocol-2015-03-09.docx"}, "CHROMATOGRAPHY":{"CHROMATOGRAPHY_TYPE":"HILIC","INSTRUMENT_NAME":"Agilent 1260","COLUMN_NAME":"Phenomenex Luna NH2 (150 x 1mm, 3um)","METHODS_ID":"AQM016","METHODS_FILENAME":"QQQ-ATP_ADP_AMP_A-update.m.zip"}, "ANALYSIS":{"ANALYSIS_TYPE":"MS","LABORATORY_NAME":"MRC2 (University of Michigan)","ACQUISITION_PARAMETERS_FILE":"QQQ-ATP_ADP_AMP_A-update.m.zip"}, "MS":{"MS_COMMENTS":"-","INSTRUMENT_NAME":"Agilent 6530 QTOF","INSTRUMENT_TYPE":"QTOF","MS_TYPE":"ESI","ION_MODE":"NEGATIVE"}, "MS_METABOLITE_DATA":{ "Units":"nM", "Data":[{"Metabolite":"Adenosine","S00017521":"1007.6439","S00017522":"1988.2942","S00017523":"679.9533","S00017524":"551.9662","S00017525":"569.2651","S00017517":"496.4092","S00017518":"431.3598","S00017519":"476.1889","S00017520":"507.5593","S00017514":"1037.3029","S00017515":"401.5582","S00017516":"1231.7558","S00017511":"654.5788","S00017512":"505.2897","S00017513":"1478.9099"},{"Metabolite":"ADP","S00017521":"678.3967","S00017522":"307.0083","S00017523":"335.1569","S00017524":"712.2886","S00017525":"914.1922","S00017517":"373.0058","S00017518":"1227.3699","S00017519":"593.9100","S00017520":"385.4795","S00017514":"412.2719","S00017515":"499.7845","S00017516":"1650.6618","S00017511":"422.9659","S00017512":"560.9905","S00017513":"1377.3388"},{"Metabolite":"AMP","S00017521":"1489.2214","S00017522":"468.3687","S00017523":"651.4922","S00017524":"1134.1691","S00017525":"1127.8465","S00017517":"456.9382","S00017518":"1312.9491","S00017519":"793.3782","S00017520":"683.6140","S00017514":"1581.2815","S00017515":"862.9433","S00017516":"3830.1950","S00017511":"997.9530","S00017512":"1428.6222","S00017513":"3966.3137"},{"Metabolite":"ATP","S00017521":"559.9511","S00017522":"227.4434","S00017523":"616.6604","S00017524":"941.8111","S00017525":"1399.1277","S00017517":"555.2832","S00017518":"1926.9506","S00017519":"744.4616","S00017520":"869.5108","S00017514":"248.0403","S00017515":"688.3181","S00017516":"2039.4192","S00017511":"501.3441","S00017512":"578.7499","S00017513":"1304.7201"}], "Metabolites":[{"Metabolite":"Adenosine","moverz_quant":"","ri":"","ri_type":"","pubchem_id":"60961","inchi_key":"","kegg_id":"","other_id":"Adenosine","other_id_type":"UM_Target_ID"},{"Metabolite":"ADP","moverz_quant":"","ri":"","ri_type":"","pubchem_id":"6022","inchi_key":"","kegg_id":"","other_id":"ADP","other_id_type":"UM_Target_ID"},{"Metabolite":"AMP","moverz_quant":"","ri":"","ri_type":"","pubchem_id":"6083","inchi_key":"","kegg_id":"","other_id":"AMP","other_id_type":"UM_Target_ID"},{"Metabolite":"ATP","moverz_quant":"","ri":"","ri_type":"","pubchem_id":"5957","inchi_key":"","kegg_id":"","other_id":"ATP","other_id_type":"UM_Target_ID"}] } }