{
"METABOLOMICS WORKBENCH":{"STUDY_ID":"ST000364","ANALYSIS_ID":"AN000597","VERSION":"1","CREATED_ON":"March 14, 2016, 3:24 pm"},

"PROJECT":{"PROJECT_TITLE":"The Newborn Epigenetic STudy (NEST)","PROJECT_TYPE":"Epigenetic","PROJECT_SUMMARY":"The overall goals of the Newborn Epigenetic STudy (NEST) research study are to identify epigenetic features in the genome that affect gene regulation and that can be altered by endogenous and exogenous influences. We hypothesize that such differences in the global epigenetic profile may be due to differences in race, maternal behaviors (e.g., nutritional status, cigarette smoking, etc.) before and throughout pregnancy, or result from conception via assisted reproductive technologies.","INSTITUTE":"North Carolina State University","LAST_NAME":"Hoyo","FIRST_NAME":"Cathrine","ADDRESS":"Box 7614 NCSU Campus Raleigh, NC 27695","EMAIL":"choyo@ncsu.edu","PHONE":"919-515-0540"},

"STUDY":{"STUDY_TITLE":"Metabolomics Profiling of NEST Cord Blood Plasma","STUDY_TYPE":"Metabolomics","STUDY_SUMMARY":"This metabolomics pilot study evaluated cord blood plasma from these children to understand how these factors influence the metabotype.","INSTITUTE":"RTI International","LAST_NAME":"Sumner","FIRST_NAME":"Susan","ADDRESS":"3040 E. Cornwallis Road","EMAIL":"ssumner@rti.org","PHONE":"919-541-7479"},

"SUBJECT":{"SUBJECT_TYPE":"Human","SUBJECT_SPECIES":"Homo sapiens"},
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"Subject ID":"-",
"Sample ID":"S_90",
"Factors":{"Pool":"-","Metal Exposure":"high Pb, low Cd = Pb 75th pct+, Cd 5-25th","Gender":"Male","Prenatal Smoking":"-","Race":"Hispanic","Asthma":"-"}
},
{
"Subject ID":"-",
"Sample ID":"S_91",
"Factors":{"Pool":"-","Metal Exposure":"high Cd, low Pb = Cd 75th pct+, Pb 5-25th pct","Gender":"Female","Prenatal Smoking":"1","Race":"Black","Asthma":"-"}
},
{
"Subject ID":"-",
"Sample ID":"S_92",
"Factors":{"Pool":"Pool 2 Sample","Metal Exposure":"high Cd & Pb = Cd 80th pct+, Pb 80th pct+","Gender":"Male","Prenatal Smoking":"-","Race":"Black","Asthma":"1"}
},
{
"Subject ID":"-",
"Sample ID":"S_93",
"Factors":{"Pool":"-","Metal Exposure":"-","Gender":"Male","Prenatal Smoking":"1","Race":"Black","Asthma":"-"}
},
{
"Subject ID":"-",
"Sample ID":"S_94",
"Factors":{"Pool":"-","Metal Exposure":"-","Gender":"Male","Prenatal Smoking":"-","Race":"White","Asthma":"-"}
},
{
"Subject ID":"-",
"Sample ID":"S_95",
"Factors":{"Pool":"Pool 2 Sample","Metal Exposure":"high Cd & Pb = Cd 80th pct+, Pb 80th pct+","Gender":"Female","Prenatal Smoking":"-","Race":"Hispanic","Asthma":"-"}
},
{
"Subject ID":"-",
"Sample ID":"S_96",
"Factors":{"Pool":"Pool 2 Sample","Metal Exposure":"-","Gender":"Male","Prenatal Smoking":"-","Race":"Black","Asthma":"-"}
},
{
"Subject ID":"-",
"Sample ID":"S_97",
"Factors":{"Pool":"-","Metal Exposure":"high Pb, low Cd = Pb 75th pct+, Cd 5-25th","Gender":"Female","Prenatal Smoking":"-","Race":"White","Asthma":"1"}
},
{
"Subject ID":"-",
"Sample ID":"S_98",
"Factors":{"Pool":"-","Metal Exposure":"-","Gender":"Female","Prenatal Smoking":"-","Race":"Black","Asthma":"1"}
},
{
"Subject ID":"-",
"Sample ID":"S_99",
"Factors":{"Pool":"Pool 2 Sample","Metal Exposure":"-","Gender":"Male","Prenatal Smoking":"-","Race":"Black","Asthma":"1"}
}
],
"COLLECTION":{"COLLECTION_SUMMARY":"Cord Blood Plasma"},

"TREATMENT":{"TREATMENT_SUMMARY":"NA"},

"SAMPLEPREP":{"SAMPLEPREP_SUMMARY":"An aliquot (125 μl) of thawed plasma from each study sample was mixed with 375 μl of methanol, vortexed, and centrifuged. 400 uL of the supernatant was dried in vacuum overnight. Each sample was reconstituted with 250 μL of 0.2 mM phosphate buffer (pH 7.5) containing 10% Chenomx Internal Standard - 0.5 mM DSS-d6. Two random study pools were created by mixing 30 μl of plasma from a subset of study samples. Five replicates were created of each pool for a total of ten pooled samples, and these prepared identically to the study samples. The tubes were vortexed for 2 min on a multi-tube vortexer and centrifuged at 16,000 rcf for 10 min. A 200 µl aliquot of the supernatant was transferred into pre-labeled 3 mm (4”) NMR tubes for data acquisition on a 700 MHz spectrometer."},

"CHROMATOGRAPHY":{"CHROMATOGRAPHY_TYPE":"-","INSTRUMENT_NAME":"-","COLUMN_NAME":"-"},

"ANALYSIS":{"ANALYSIS_TYPE":"NMR"},

"NM":{"INSTRUMENT_NAME":"Bruker Avance III","INSTRUMENT_TYPE":"FT-NMR","NMR_EXPERIMENT_TYPE":"1D-1H","SPECTROMETER_FREQUENCY":"700.13 MHz"},

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