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"PROJECT":{"PROJECT_TITLE":"Metabolomics Changes in the feces of infants exposed to arsenic","PROJECT_SUMMARY":"Exposure to arsenic (As) during the vulnerable window of fetal development and early childhood has shown significant clinical effects. In highly exposed populations, altered immunity is one of the most affected pathways and can lead to an elevated risk of infection and a predisposition to allergy/atopy. Since well water in the New Hampshire region has been determined to be a potential source of As exposure, this study includes motherinfant dyads living in the area, who obtain household water from private wells. This study seeks to determine if in utero and early life As exposure is related to increase occurrence of childhood: infections, allergy and atopy, and diminished vaccine response. It has been observed that the microbiome is an important mediator of immune impairment due to As exposure. Therefore, we will further investigate the relation between in utero and early life As exposure on the development of the infant intestinal microbiome in the first year of life. For this study fecal samples, from infants at risk of As exposure, were collected at 6 weeks and 12 months of age. Metabolomics data will allow for a more complete picture of the relationships between the microbiome, As exposure and immune function.","INSTITUTE":"Dartmouth College","DEPARTMENT":"Department of Epidemiology","LAST_NAME":"Margaret","FIRST_NAME":"Karagas","ADDRESS":"One Medical Center Road, 7927 HB, Rubin Building, Lebanon, NH 03756","EMAIL":"Margaret.Karagas@Dartmouth.edu","PHONE":"6036539010"},

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"TREATMENT":{"TREATMENT_SUMMARY":"None"},

"SAMPLEPREP":{"SAMPLEPREP_SUMMARY":"The samples of thawed feces from each participant were transferred to massed MagNA tubes, frozen, and lyophilized. Lyophilized samples were massed and phosphate buffer was added depending on the mass of each sample (500 µL for up to 200 mg, and 1.0 mL for over 200 mg of feces) and homogenized in 30 second pulses at 2000 rpm. Homogenized samples were centrifuged and the supernatant was filtered. A volume of the filtered supernatant necessary to analyze 25 mg per sample was mixed with 70 µL of Chenomx ISTD solution, and a calculated volume of 0.5 mM phosphate buffer (pH 7.5) needed to bring the total sample volume to 630 µL. The tubes were vortexed for 2 min on a multitube vortexer and centrifuged at 16,000 rcf for 5 min. A 600 µl aliquot of the supernatant was transferred into prelabeled 5mm NMR tubes for data acquisition on a 700 MHz spectrometer. Additionally, ten random QC pools were created from the samples with adequate mass to spare. An aliquot containing 5 mg of fecal water from each individual sample was transferred into the pools, and three replicates were created from each pool for a total of 30 pooled samples. Each pool was run once a day over the 3 day experimental run time."},

"CHROMATOGRAPHY":{"CHROMATOGRAPHY_TYPE":"-","INSTRUMENT_NAME":"-","COLUMN_NAME":"-"},

"ANALYSIS":{"ANALYSIS_TYPE":"NMR"},

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