#METABOLOMICS WORKBENCH Zhulab_20221115_103729 DATATRACK_ID:3574 STUDY_ID:ST002379 ANALYSIS_ID:AN003878 PROJECT_ID:PR001524 VERSION 1 CREATED_ON December 1, 2022, 10:24 am #PROJECT PR:PROJECT_TITLE Pyruvate dehydrogenase kinase supports macrophage NLRP3 inflammasome activation PR:PROJECT_TITLE during acute inflammation PR:PROJECT_TYPE Basic research PR:PROJECT_SUMMARY Activating macrophage NLRP3 inflammasome can promote excessive inflammation, PR:PROJECT_SUMMARY with severe cell and tissue damage and organ dysfunction. Here, we show that PR:PROJECT_SUMMARY pharmacological or genetic inhibition of pyruvate dehydrogenase kinase (PDHK) PR:PROJECT_SUMMARY significantly attenuates NLRP3 inflammasome activation in murine and human PR:PROJECT_SUMMARY macrophages and septic mice by lowering caspase-1 cleavage and IL-1beta PR:PROJECT_SUMMARY secretion. Inhibiting PDHK reverses NLRP3 inflammasome-induced metabolic PR:PROJECT_SUMMARY reprogramming, enhances autophagy, promotes mitochondrial fusion over fission, PR:PROJECT_SUMMARY preserves cristae ultrastructure, and attenuates mitochondrial ROS production. PR:PROJECT_SUMMARY The suppressive effect of PDHK inhibition on the NLRP3 inflammasome is PR:PROJECT_SUMMARY independent of its canonical role as a pyruvate dehydrogenase regulator. We PR:PROJECT_SUMMARY suggest that PDHK inhibition improves mitochondrial fitness by reversing NLRP3 PR:PROJECT_SUMMARY inflammasome activation in acutely inflamed macrophages. PR:INSTITUTE Wake Forest School of Medicine PR:LAST_NAME Zhu PR:FIRST_NAME Xuewei PR:ADDRESS 575 Patterson Ave PR:EMAIL xwzhu@wakehealth.edu PR:PHONE 3367131445 #STUDY ST:STUDY_TITLE Glucose flux analysis of NLRP3 inflammasome activated macrophages ST:STUDY_TYPE Basic research ST:STUDY_SUMMARY Activating macrophage NLRP3 inflammasome can promote excessive inflammation, ST:STUDY_SUMMARY with severe cell and tissue damage and organ dysfunction. Here, we show that ST:STUDY_SUMMARY pharmacological or genetic inhibition of pyruvate dehydrogenase kinase (PDHK) ST:STUDY_SUMMARY significantly attenuates NLRP3 inflammasome activation in murine and human ST:STUDY_SUMMARY macrophages and septic mice by lowering caspase-1 cleavage and IL-1beta ST:STUDY_SUMMARY secretion. Inhibiting PDHK reverses NLRP3 inflammasome-induced metabolic ST:STUDY_SUMMARY reprogramming, enhances autophagy, promotes mitochondrial fusion over fission, ST:STUDY_SUMMARY preserves cristae ultrastructure, and attenuates mitochondrial ROS production. ST:STUDY_SUMMARY The suppressive effect of PDHK inhibition on the NLRP3 inflammasome is ST:STUDY_SUMMARY independent of its canonical role as a pyruvate dehydrogenase regulator. We ST:STUDY_SUMMARY suggest that PDHK inhibition improves mitochondrial fitness by reversing NLRP3 ST:STUDY_SUMMARY inflammasome activation in acutely inflamed macrophages. ST:INSTITUTE Wake Forest School of Medicine ST:LAST_NAME Zhu ST:FIRST_NAME Xuewei ST:ADDRESS 575 Patterson Ave, Winston-Salem, NC 27101 ST:EMAIL xwzhu@wakehealth.edu ST:PHONE 3367131445 #SUBJECT SU:SUBJECT_TYPE Cultured cells SU:SUBJECT_SPECIES Mus musculus SU:TAXONOMY_ID 10090 #SUBJECT_SAMPLE_FACTORS: SUBJECT(optional)[tab]SAMPLE[tab]FACTORS(NAME:VALUE pairs separated by |)[tab]Raw file names and additional sample data SUBJECT_SAMPLE_FACTORS - Ctrl_C_1 Treatment:No treatment RAW_FILE_NAME=Ctril_C_1.raw SUBJECT_SAMPLE_FACTORS - Ctrl_C_2 Treatment:No treatment RAW_FILE_NAME=Ctril_C_2.raw SUBJECT_SAMPLE_FACTORS - Ctrl_C_3 Treatment:No treatment RAW_FILE_NAME=Ctril_C_3.raw SUBJECT_SAMPLE_FACTORS - LPS_1 Treatment:LPS RAW_FILE_NAME=LPS_1.raw SUBJECT_SAMPLE_FACTORS - LPS_2 Treatment:LPS RAW_FILE_NAME=LPS_2.raw SUBJECT_SAMPLE_FACTORS - LPS_3 Treatment:LPS RAW_FILE_NAME=LPS_3.raw SUBJECT_SAMPLE_FACTORS - LPS_ATP_1 Treatment:LPS+ATP RAW_FILE_NAME=LPS_ATP_1.raw SUBJECT_SAMPLE_FACTORS - LPS_ATP_2 Treatment:LPS+ATP RAW_FILE_NAME=LPS_ATP_2.raw SUBJECT_SAMPLE_FACTORS - LPS_ATP_3 Treatment:LPS+ATP RAW_FILE_NAME=LPS_ATP_3.raw SUBJECT_SAMPLE_FACTORS - LPS_JX06_ATP_1 Treatment:JPS+JX06+ATP RAW_FILE_NAME=LPS_JX06_ATP_1.raw SUBJECT_SAMPLE_FACTORS - LPS_JX06_ATP_2 Treatment:JPS+JX06+ATP RAW_FILE_NAME=LPS_JX06_ATP_2.raw SUBJECT_SAMPLE_FACTORS - LPS_JX06_ATP_3 Treatment:JPS+JX06+ATP RAW_FILE_NAME=LPS_JX06_ATP_3.raw #COLLECTION CO:COLLECTION_SUMMARY Mouse bone marrow was cultured in low glucose DMEM supplemented with 30% L929 CO:COLLECTION_SUMMARY cell-conditioned medium, 20% FBS, 2 mM L-glutamine, 1 mM sodium pyruvate, 100 CO:COLLECTION_SUMMARY U/ml penicillin, and 100 µg/ml streptomycin for 6-7 days until the cells CO:COLLECTION_SUMMARY reached confluence. BMDMs were then reseeded in culture dishes overnight in CO:COLLECTION_SUMMARY RPMI-1640 medium containing 1% Nutridoma-SP medium (Sigma-Aldrich). LPS-primed CO:COLLECTION_SUMMARY BMDMs were stimulated with 5 mM ATP in the presence or absence of 10 uM JX06 for CO:COLLECTION_SUMMARY 30 min. Unstimulated macrophages were used as control.13C tracing started by CO:COLLECTION_SUMMARY replacing medium with glucose-free medium supplemented with 2.06 g/L CO:COLLECTION_SUMMARY [U-13C]-glucose (Cayman Chemical) for 90 min. Cells were washed with ice-cold CO:COLLECTION_SUMMARY saline and intracellular metabolites were extracted using cold methanol and H2O CO:COLLECTION_SUMMARY (80:20; HPLC Grade; Sigma-Aldrich). Here, we show that pharmacological or CO:COLLECTION_SUMMARY genetic inhibition of pyruvate dehydrogenase kinase (PDHK) significantly CO:COLLECTION_SUMMARY attenuates NLRP3 inflammasome activation in murine and human macrophages and CO:COLLECTION_SUMMARY septic mice by lowering caspase-1 cleavage and IL-1beta secretion. Inhibiting CO:COLLECTION_SUMMARY PDHK reverses NLRP3 inflammasome-induced metabolic reprogramming, enhances CO:COLLECTION_SUMMARY autophagy, promotes mitochondrial fusion over fission, preserves cristae CO:COLLECTION_SUMMARY ultrastructure, and attenuates mitochondrial ROS production. The suppressive CO:COLLECTION_SUMMARY effect of PDHK inhibition on the NLRP3 inflammasome is independent of its CO:COLLECTION_SUMMARY canonical role as a pyruvate dehydrogenase regulator. We suggest that PDHK CO:COLLECTION_SUMMARY inhibition improves mitochondrial fitness by reversing NLRP3 inflammasome CO:COLLECTION_SUMMARY activation in acutely inflamed macrophages. CO:SAMPLE_TYPE Macrophages CO:COLLECTION_METHOD Cells were washed with ice-cold saline and intracellular metabolites were CO:COLLECTION_METHOD extracted using cold methanol and H2O (80:20; HPLC Grade; Sigma-Aldrich). The CO:COLLECTION_METHOD samples were pre-dissolved into 40 µL solution (LC-water, methanol, CO:COLLECTION_METHOD Acetonitrile 2:1:1) before injection. CO:STORAGE_CONDITIONS -80℃ #TREATMENT TR:TREATMENT_SUMMARY LPS-primed BMDMs were stimulated with or without 5 mM ATP in the presence or TR:TREATMENT_SUMMARY absence of 10 uM JX06 for 30 min. 13C tracing started by replacing medium with TR:TREATMENT_SUMMARY glucose-free medium supplemented with 2.06 g/L [U-13C]-glucose (Cayman Chemical) TR:TREATMENT_SUMMARY for 90 min. TR:TREATMENT in vitro cell culture treatment TR:TREATMENT_COMPOUND LPS, ATP, JX06 #SAMPLEPREP SP:SAMPLEPREP_SUMMARY Macrophages were lysed, and polar metabolites were extracted using methanol and SP:SAMPLEPREP_SUMMARY H2O (80:20; HPLC Grade; Sigma-Aldrich) (Liu et al., 2015). Extracts were dried SP:SAMPLEPREP_SUMMARY in a vacuum concentrator at room temperature and stored at -80 freezer. #CHROMATOGRAPHY CH:CHROMATOGRAPHY_SUMMARY Ultimate 3000 UHPLC (Dionex) is coupled to Q Exactive Plus-Mass spectrometer CH:CHROMATOGRAPHY_SUMMARY (QE-MS, Thermo Scientific) for metabolite profiling. CH:CHROMATOGRAPHY_TYPE HILIC CH:INSTRUMENT_NAME Thermo Dionex Ultimate 3000 CH:COLUMN_NAME Waters XBridge Amide (100 x 4.6mm, 3.5um) #ANALYSIS AN:ANALYSIS_TYPE MS AN:LABORATORY_NAME Jason Locosale AN:OPERATOR_NAME Likun Duan #MS MS:INSTRUMENT_NAME Thermo Q Exactive Plus Orbitrap MS:INSTRUMENT_TYPE Orbitrap MS:MS_TYPE ESI MS:ION_MODE NEGATIVE MS:MS_COMMENTS For each sample, 3 µL solution was injected into the LC-MS for analysis. The MS:MS_COMMENTS HPLC analysis of the isotope-labeled samples was performed using Ultimate 3000 MS:MS_COMMENTS UHPLC (Dionex) as described (Duan et al., 2022). The mass spectrometry analysis MS:MS_COMMENTS was performed using Q Exactive Plus mass spectrometer (Thermo Fisher MS:MS_COMMENTS Scientific). The mass spectrometers were equipped with a HESI probe and operated MS:MS_COMMENTS in the positive/negative switching mode. When Q Exactive Plus mass spectrometer MS:MS_COMMENTS was used, the relevant parameters were as listed: heater temperature, 120 °C; MS:MS_COMMENTS sheath gas, 30; auxiliary gas, 10; sweep gas, 3; spray voltage, 3.0 kV; MS:MS_COMMENTS capillary temperature, 320°C; S-lens, 55. The resolution was set at 70,000 (at MS:MS_COMMENTS m/z 200). Maximum injection time (max IT) was set at 200 ms and automated gain MS:MS_COMMENTS control (AGC) was set at 3 × 106. The LC-MS peak extraction and integration of MS:MS_COMMENTS the raw data were performed using commercially available software Sieve 2.0 MS:MS_COMMENTS (Thermo Fisher Scientific). The integrated peak area was used to calculate 13C MS:MS_COMMENTS enrichment. Natural abundance correction was performed using software R with MS:MS_COMMENTS Bioconductor R package IsoCorrectoR. #MS_METABOLITE_DATA MS_METABOLITE_DATA:UNITS Fractional enrichment MS_METABOLITE_DATA_START Samples Ctrl_C_1 Ctrl_C_2 Ctrl_C_3 LPS_1 LPS_2 LPS_3 LPS_ATP_1 LPS_ATP_2 LPS_ATP_3 LPS_JX06_ATP_1 LPS_JX06_ATP_2 LPS_JX06_ATP_3 Factors Treatment:No treatment Treatment:No treatment Treatment:No treatment Treatment:LPS Treatment:LPS Treatment:LPS Treatment:LPS+ATP Treatment:LPS+ATP Treatment:LPS+ATP Treatment:JPS+JX06+ATP Treatment:JPS+JX06+ATP Treatment:JPS+JX06+ATP Aspartate 0.501974129 0.500588398 0.496940099 0.552796716 0.550747014 0.554508096 0.728527353 0.727321206 0.718723128 0.642121406 0.642863874 0.646908071 1[13C]Aspartate 0.068509798 0.06998721 0.06837107 0.040223885 0.038462313 0.040660272 0.050028016 0.048485326 0.051964024 0.050036639 0.049182269 0.049022698 2[13C]Aspartate 0.251399598 0.25334779 0.253672986 0.244887449 0.248624285 0.244503616 0.147124351 0.148095874 0.155351321 0.188349106 0.187303587 0.18627021 3[13C]Aspartate 0.141846164 0.141322062 0.144298263 0.129618123 0.130350579 0.129131105 0.063022107 0.064476718 0.062792344 0.098821038 0.100314951 0.097832114 4[13C]Aspartate 0.036270312 0.03475454 0.036717582 0.032473827 0.031815808 0.031196911 0.011298172 0.011620877 0.011169183 0.02067181 0.020335318 0.019966907 N(omega)-(L-Arginino)succinate 0.723301766 0.653685643 0.707759661 0.636279874 0.624716829 0.616000559 0.742562123 0.730305855 0.715430595 0.63159895 0.646392055 0.634170605 1[13C]N(omega)-(L-Arginino)succinate 0 0.025296223 0.006759818 0.024093265 0.022761538 0.03101938 0.055753185 0.074959487 0.06106321 0.053690418 0.057083471 0.042852353 2[13C]N(omega)-(L-Arginino)succinate 0.18969426 0.225638617 0.19076019 0.22323286 0.221034913 0.234624577 0.160901891 0.141202715 0.159752411 0.196596833 0.18929238 0.208763261 3[13C]N(omega)-(L-Arginino)succinate 0.087003974 0.090509766 0.09472033 0.094667925 0.115657166 0.101937731 0.035896998 0.04978177 0.058145822 0.101325584 0.095136117 0.092374966 4[13C]N(omega)-(L-Arginino)succinate 0 0.00486975 0 0.021726076 0.015829554 0.016417753 0.004885804 0.002488925 0.005607963 0.016788214 0.012095977 0.021838816 5[13C]N(omega)-(L-Arginino)succinate 0 0 0 0 0 0 0 0 0 0 0 0 6[13C]N(omega)-(L-Arginino)succinate 0 0 0 0 0 0 0 0 0 0 0 0 7[13C]N(omega)-(L-Arginino)succinate 0 0 0 0 0 0 0 0 0 0 0 0 8[13C]N(omega)-(L-Arginino)succinate 0 0 0 0 0 0 0 0 0 0 0 0 9[13C]N(omega)-(L-Arginino)succinate 0 0 0 0 0 0 0 0 0 0 0 0 10[13C]N(omega)-(L-Arginino)succinate 0 0 0 0 0 0 0 0.001261247 0 0 0 0 laurate 1 1 1 1 1 1 1 0.999997043 1 1 1 1 1[13C]laurate 0 0 0 0 0 0 0 2.95716E-06 0 0 0 0 2[13C]laurate 0 0 0 0 0 0 0 0 0 0 0 0 3[13C]laurate 0 0 0 0 0 0 0 0 0 0 0 0 4[13C]laurate 0 0 0 0 0 0 0 0 0 0 0 0 5[13C]laurate 0 0 0 0 0 0 0 0 0 0 0 0 6[13C]laurate 0 0 0 0 0 0 0 0 0 0 0 0 7[13C]laurate 0 0 0 0 0 0 0 0 0 0 0 0 8[13C]laurate 0 0 0 0 0 0 0 0 0 0 0 0 9[13C]laurate 0 0 0 0 0 0 0 0 0 0 0 0 10[13C]laurate 0 0 0 0 0 0 0 0 0 0 0 0 11[13C]laurate 0 0 0 0 0 0 0 0 0 0 0 0 12[13C]laurate 0 0 0 0 0 0 0 0 0 0 0 0 myristate 0.99330967 0.993808397 0.990362245 0.992828503 0.990465109 0.990675828 0.991654815 0.99251803 0.992275896 0.980344427 0.980011022 0.980344993 1[13C]myristate 0 0 0 0 0 0 0 0 0 0.00055903 0 0 2[13C]myristate 0 0 0 0 0 0 0.00080193 0.001458824 0.000775058 0.000408325 0.00037151 0.000428354 3[13C]myristate 0 0 0 0 0 0 0 0 0 0 0 0 4[13C]myristate 0 0 0.000311129 0 0 0 0.002291922 0.002198339 0.002301589 0.003297295 0.003733725 0.003212802 5[13C]myristate 0 0 0 0 0 0 0 3.65326E-05 0 0 0 0 6[13C]myristate 0.000357732 0 0.000683 0.000402099 0 0 0.002208524 0.002120381 0.002798034 0.005182756 0.005282221 0.005294107 7[13C]myristate 0 0 0 0 1.90569E-07 3.31597E-07 0 0 0 0.000107621 0 6.73299E-05 8[13C]myristate 0.002165289 0.001675293 0.002195071 0.001855725 0.001185208 0.00206023 0.001866216 0.001401038 0.00154788 0.005513162 0.005146688 0.005667726 9[13C]myristate 0 0.000412679 0.000121198 0.000266397 0 0 0 0 0 1.76302E-05 0 0 10[13C]myristate 0.002454119 0.001759896 0.002689903 0.002632131 0.003405874 0.003185816 0.001176592 0.000266856 0.000301544 0.003527508 0.003852443 0.00379376 11[13C]myristate 0 0 0 0 0 0 0 0 0 0 0 4.39034E-06 12[13C]myristate 0.001423126 0.002343734 0.003637453 0.002015145 0.004594633 0.004077795 0 0 0 0.001042246 0.00160239 0.001186538 13[13C]myristate 0 0 0 0 0.000348986 0 0 0 0 0 0 0 14[13C]myristate 0.000290064 0 0 0 0 0 0 0 0 0 0 0 palmitate 0.995606682 0.996037276 0.995759809 0.99465371 0.994964512 0.994659755 0.999757926 0.999915684 0.999897573 0.997313319 0.997867618 0.997834934 1[13C]palmitate 0 0 0 0 0 0 0 0 0 0 0 0 2[13C]palmitate 0 0 0 0 0 0 0 0 0 0 0 0 3[13C]palmitate 0 1.97142E-06 0 0 0 0 2.99914E-05 0 4.79832E-06 5.34995E-05 0 0 4[13C]palmitate 2.34564E-05 0 0 0 0 0 0 0 0 0.000392877 0.0001599 0.000172343 5[13C]palmitate 0 0 0 0 0 0 0 0 0 0 0 3.9031E-06 6[13C]palmitate 0.000164245 0.000118235 0.000101797 0.000163406 0 4.92728E-05 6.52778E-05 8.92464E-06 1.48333E-05 0.000556018 0.000347268 0.000373599 7[13C]palmitate 1.11596E-05 0 0 0 0 0 0 0 0 0 3.05406E-05 0 8[13C]palmitate 0.000593097 0.00043061 0.000431203 0.000572861 0.000405266 0.000514379 0.000103956 7.53909E-05 8.27956E-05 0.000548728 0.000457645 0.000580461 9[13C]palmitate 8.28467E-05 0 8.43136E-05 3.14539E-05 9.49034E-05 1.24593E-05 0 0 0 1.68792E-05 1.16365E-06 5.47602E-05 10[13C]palmitate 0.000776884 0.000744269 0.000884711 0.000896392 0.001229004 0.00130948 4.28488E-05 0 0 0.000485423 0.00059246 0.000603969 11[13C]palmitate 0.000237945 0.000116145 0.000158043 0.000189367 6.30675E-05 0.000153907 0 0 0 6.53061E-06 0 2.21719E-05 12[13C]palmitate 0.001005393 0.001133851 0.001131527 0.001571419 0.001355411 0.001563524 0 0 0 0.000449317 0.000440726 0.000273401 13[13C]palmitate 0.000164516 0.000220174 0.000174325 0.000174328 7.92381E-05 4.85104E-05 0 0 0 0 0 0 14[13C]palmitate 0.000948568 0.000890409 0.000984492 0.00127012 0.001332036 0.001283344 0 0 0 0.000177409 0.000102679 8.04581E-05 15[13C]palmitate 0 3.24235E-05 6.2831E-06 0 5.40632E-05 1.10763E-05 0 0 0 0 0 0 16[13C]palmitate 0.000385208 0.000274635 0.000283497 0.000476943 0.000422499 0.000394292 0 0 0 0 0 0 UDP-D-glucuronate 0.280288414 0.268635555 0.285720316 0.22413777 0.239762277 0.226222696 0.652206322 0.436581381 0.399439258 0.419761259 0.384421184 0.479307779 1[13C]UDP-D-glucuronate 0 0 0 0 0 0 0 0 0 0 0 0 2[13C]UDP-D-glucuronate 0 0.013077671 0 0 0 0 0 0 0 0 0 0 3[13C]UDP-D-glucuronate 0 0.011879218 0 0 0.004359863 0.006274771 0 0.019864243 0.02335339 0.014377419 0.047632164 0.059763081 4[13C]UDP-D-glucuronate 0 0 0.006872754 0 0 0 0 0.013801877 0.016575469 0 0.029819273 0 5[13C]UDP-D-glucuronate 0.042167764 0.085156153 0.05674416 0.040403315 0.031389347 0.067630657 0.000180229 0.02053052 0.022012214 0.043081043 0.088899209 0 6[13C]UDP-D-glucuronate 0.677543822 0.621251403 0.650662769 0.735458915 0.704854205 0.681407913 0.347613449 0.509221979 0.538619668 0.52278028 0.445253532 0.46092914 7[13C]UDP-D-glucuronate 0 0 0 0 0 0 0 0 0 0 0 0 8[13C]UDP-D-glucuronate 0 0 0 0 0.006876639 0.010183341 0 0 0 0 0 0 9[13C]UDP-D-glucuronate 0 0 0 0 0 0 0 0 0 0 0 0 10[13C]UDP-D-glucuronate 0 0 0 0 0 0 0 0 0 0 0 0 11[13C]UDP-D-glucuronate 0 0 0 0 0.012757669 0.008280622 0 0 0 0 0 0 12[13C]UDP-D-glucuronate 0 0 0 0 0 0 0 0 0 0 3.04438E-08 0 13[13C]UDP-D-glucuronate 0 0 0 0 0 0 0 0 0 0 0.003974607 0 14[13C]UDP-D-glucuronate 0 0 0 0 0 0 0 0 0 0 0 0 15[13C]UDP-D-glucuronate 0 0 0 0 0 0 0 0 0 0 0 0 UDP-glucose 0.157027463 0.152967584 0.15678583 0.132162556 0.1280652 0.129885077 0.207286074 0.208684213 0.199183661 0.194949042 0.203422223 0.19595191 1[13C]UDP-glucose 0 0.003371167 0.003373209 0.000867726 0 0.001468059 0.006299421 0.004341974 0.008512169 0.00741465 0.008522061 0.008011834 2[13C]UDP-glucose 0.00879134 0.012375832 0.011290696 0.006191858 0.007009709 0.00567472 0.023320911 0.024101416 0.025474873 0.024858286 0.024462471 0.026405203 3[13C]UDP-glucose 0.031371055 0.03121843 0.031657708 0.018126571 0.018487408 0.019304899 0.060862351 0.066400125 0.058797892 0.068801236 0.067001436 0.065628949 4[13C]UDP-glucose 0.013965418 0.01460299 0.017184271 0.007558352 0.007637782 0.008148379 0.036637882 0.038646407 0.037331975 0.048342374 0.046451469 0.046306266 5[13C]UDP-glucose 0.059858124 0.063567269 0.060573999 0.05249325 0.055995649 0.055151505 0.08451212 0.080479697 0.079471734 0.095052751 0.088876336 0.092410461 6[13C]UDP-glucose 0.684197342 0.675691894 0.673453768 0.689831046 0.69133734 0.686444573 0.554910031 0.55292519 0.565806499 0.535075088 0.534993843 0.539678595 7[13C]UDP-glucose 0.006341677 0.007057604 0.010292655 0.006645937 0.008797322 0.009515097 0.006907676 0.006439005 0.007060644 0.00778224 0.007649122 0.008565861 8[13C]UDP-glucose 0.023090053 0.023283892 0.022353299 0.026192766 0.023808462 0.026819997 0.019263535 0.017868372 0.018276322 0.017509638 0.018006221 0.017040922 9[13C]UDP-glucose 0.000368674 0.000425954 0 0.002947302 0.003782883 0.003083312 0 0 0 0.000214697 0.000575346 0 10[13C]UDP-glucose 0.000403988 0.001695835 0.001504285 0.006823465 0.006366125 0.00616461 0 0 0 0 0 0 11[13C]UDP-glucose 0.011381383 0.010598814 0.009147066 0.039021899 0.037462841 0.037012792 0 0 0 0 0 0 12[13C]UDP-glucose 0.000891424 0.000813318 0.000555686 0.004430123 0.005274293 0.004468353 0 0 0 0 0 0 13[13C]UDP-glucose 0.001356536 0.002329417 0.001827528 0.006445893 0.005414428 0.005690532 0 0 0 0 0 0 14[13C]UDP-glucose 0 0 0 0.000261257 0.000560558 0.001168095 0 0 0 0 0 0 15[13C]UDP-glucose 0.000955523 0 0 0 0 0 0 0.0001136 8.42299E-05 0 3.94722E-05 0 UDP-N-acetyl-alpha-D-glucosamine 0.781131374 0.766887152 0.772276632 0.630077204 0.633966782 0.63302323 0.706545877 0.711575428 0.690446525 0.56913609 0.57144294 0.574975879 1[13C]UDP-N-acetyl-alpha-D-glucosamine 0.006706934 0.014553625 0.00673805 0.009852425 0.008369531 0.006174564 0.017152654 0.016515237 0.016800798 0.014945826 0.01755941 0.014979555 2[13C]UDP-N-acetyl-alpha-D-glucosamine 0.059071244 0.05849957 0.056386247 0.055969651 0.055768698 0.054693395 0.053881537 0.054836304 0.051739389 0.070228368 0.071119607 0.068698277 3[13C]UDP-N-acetyl-alpha-D-glucosamine 0.004240503 0.003628075 0.00167753 0.004563024 0.004452786 0.004842432 0.017492257 0.016831702 0.018117297 0.021218702 0.023107942 0.023330149 4[13C]UDP-N-acetyl-alpha-D-glucosamine 0.006189963 0.008218818 0.008373169 0.009281748 0.011401068 0.012949307 0.022874915 0.033387604 0.033111622 0.040609274 0.050818671 0.043674659 5[13C]UDP-N-acetyl-alpha-D-glucosamine 0.012410391 0.012645172 0.012016668 0.033901071 0.031589762 0.033412263 0.019659288 0.019264748 0.021667992 0.031411099 0.031605435 0.030217781 6[13C]UDP-N-acetyl-alpha-D-glucosamine 0.037855557 0.038789344 0.040296119 0.063238239 0.059914218 0.064094389 0.093315748 0.085154726 0.097859291 0.118526687 0.109837843 0.118765555 7[13C]UDP-N-acetyl-alpha-D-glucosamine 0.007596098 0.012478638 0.011243 0.016549993 0.023295878 0.018719355 0.005936556 0.009839475 0.004249418 0.02592913 0.021744261 0.017379178 8[13C]UDP-N-acetyl-alpha-D-glucosamine 0.080902726 0.080322196 0.086495411 0.155509451 0.151287441 0.153843903 0.062106336 0.051316086 0.063982687 0.104560674 0.099212539 0.105428534 9[13C]UDP-N-acetyl-alpha-D-glucosamine 0.000404758 0 0.000148784 0.002491997 0.001383299 0 0 0 0.000551707 0.000862583 0.001029373 1.32962E-05 10[13C]UDP-N-acetyl-alpha-D-glucosamine 0.001558649 0.001966039 0.002783011 0.00567573 0.005544852 0.004950524 0.001034831 0.00127869 0.001473274 0.002499536 0.002521979 0.002537137 11[13C]UDP-N-acetyl-alpha-D-glucosamine 0.000746683 0.000386525 0.000349504 0.003454556 0.003297584 0.002957009 0 0 0 7.20327E-05 0 0 12[13C]UDP-N-acetyl-alpha-D-glucosamine 0 0.000291209 0 0.00090158 0.00203719 0.000907479 0 0 0 0 0 0 13[13C]UDP-N-acetyl-alpha-D-glucosamine 0.00118512 0.001333635 0.001099721 0.007312909 0.006836323 0.007661977 0 0 0 0 0 0 14[13C]UDP-N-acetyl-alpha-D-glucosamine 0 0 0 0.000588587 0.000282726 0.001091624 0 0 0 0 0 0 15[13C]UDP-N-acetyl-alpha-D-glucosamine 0 0 0.000116154 0.000631833 0.000571862 0.000678547 0 0 0 0 0 0 16[13C]UDP-N-acetyl-alpha-D-glucosamine 0 0 0 0 0 0 0 0 0 0 0 0 17[13C]UDP-N-acetyl-alpha-D-glucosamine 0 0 0 0 0 0 0 0 0 0 0 0 myo-inositol 0.945660534 0.944909177 0.943245877 0.952395506 0.95182168 0.951059524 0.959029525 0.962806401 0.961645976 0.954517262 0.957652654 0.95850747 1[13C]myo-inositol 3.85775E-05 0.000270779 2.50077E-05 0.000120215 0.000346415 0 0.000790336 2.21126E-05 0.000641343 0.002773295 0.000512687 0 2[13C]myo-inositol 0 0 0 0 0 0 0 0 0 0 0 0 3[13C]myo-inositol 0.001749448 0.001848236 0.001976408 0.000706172 0.000850334 0.000840659 0.001495927 0.001572222 0.001724322 0.003457233 0.003011282 0.002945514 4[13C]myo-inositol 0.000814888 0.001085665 0.001059602 4.5866E-05 0.000261082 0.000403351 0.00062057 0.000881673 0.001010841 0.002035628 0.001698699 0.002093884 5[13C]myo-inositol 0.004596761 0.004694328 0.004241173 0.003602305 0.003009374 0.003118409 0.003581119 0.003206367 0.003713419 0.004823379 0.005156452 0.004922487 6[13C]myo-inositol 0.047139791 0.047191813 0.049451932 0.043129936 0.043711116 0.044578056 0.034482523 0.031511224 0.031264098 0.032393203 0.031968225 0.031530645 ATP 0.949034119 0.942663278 0.943792127 0.901440444 0.900339732 0.893342904 0.922393925 0.957239826 0.955111548 0.969278155 0.966721997 0.965847132 1[13C]-ATP 0.001882862 0.005667434 0.00586755 0.00545388 0.006517689 0.008423986 0 0.008043147 0.008485899 0.004418685 0.008569345 0.006605437 2[13C]-ATP 0.024178329 0.024990226 0.024192282 0.025185586 0.024639328 0.02355124 0.009488489 0.024683924 0.024695429 0.023934138 0.023219853 0.025267668 3[13C]-ATP 0 0.000942176 0.000466646 0.002602226 0.002249433 0.003845503 0 0 0 0 0 0 4[13C]-ATP 0.000368201 0.002545706 0.001166336 0.003976844 0.004852539 0.004218387 0 0 0 0 0 0 5[13C]-ATP 0.024536489 0.022959786 0.024515059 0.060592523 0.05949123 0.064561533 0.068117586 0.010033104 0.011707125 0.002369023 0.001488805 0.002279763 6[13C]-ATP 0 2.52106E-05 0 0.000150705 0.000890152 0.001191602 0 0 0 0 0 0 7[13C]-ATP 0 0.000206182 0 0.000597792 0.001019897 0.000636376 0 0 0 0 0 0 8[13C]-ATP 0 0 0 0 0 0.000228469 0 0 0 0 0 0 9[13C]-ATP 0 0 0 0 0 0 0 0 0 0 0 0 10[13C]-ATP 0 0 0 0 0 0 0 0 0 0 0 0 AMP 0.967250824 0.962314649 0.965369381 0.91629799 0.921388255 0.919105826 0.986429789 0.983867354 0.983551509 0.988539804 0.987622859 0.988084992 1[13C]AMP 0 0 0 0 0 0 0 0 0 0 0 0 2[13C]AMP 0.010256311 0.008780778 0.008237622 0.01479948 0.01233538 0.016306578 0.012813978 0.012468368 0.012340665 0.010772442 0.010406184 0.010446109 3[13C]AMP 0.000125157 0 0 0.000524296 0.004084494 0.000903243 0 0.000271344 0.000182757 0.000687754 9.14041E-05 0.00021978 4[13C]AMP 0 0.001140457 0 0 0.000876479 0 0 0 0 0 0 0 5[13C]AMP 0.022367708 0.027764117 0.026392997 0.068378234 0.061315393 0.063684353 0.000756233 0.003392935 0.003925069 0 0.001438627 0.001249119 6[13C]AMP 0 0 0 0 0 0 0 0 0 0 0 0 7[13C]AMP 0 0 0 0 0 0 0 0 0 0 0.000440926 0 8[13C]AMP 0 0 0 0 0 0 0 0 0 0 0 0 9[13C]AMP 0 0 0 0 0 0 0 0 0 0 0 0 10[13C]AMP 0 0 0 0 0 0 0 0 0 0 0 0 UMP 0.874527313 0.831450082 0.817146821 0.822719194 0.818949396 0.828717652 0.657240092 0.735802466 0.657396222 0.862302186 0.955491203 0.93506037 1[13C]-UMP 0.007973949 0.002818408 0 0 0.001097493 0.002753779 0 0 0 0 0 0 2[13C]-UMP 0.081696527 0.128963582 0.12214105 0.096203116 0.084193996 0.070487869 0.315376318 0.243465648 0.31722109 0.12512637 0.03929538 0.054761032 3[13C]-UMP 0 0 0 0 0 0 0 0.004158773 0.000758876 0 0 0 4[13C]-UMP 0 0 0.002751327 0.000291646 0 0.004342596 0.005883078 0.001789761 0.006711101 0.002383327 0.000160176 0.00036194 5[13C]-UMP 0.031938931 0.019220201 0.041725642 0.057701899 0.063189333 0.061689236 0.005472223 0.002769221 0.006179379 0.002626593 0.000847235 0.002206006 6[13C]-UMP 0.000239942 0 0 0 0 0 0.000220548 0 0.003670726 0 0 0 7[13C]-UMP 0 0.009168689 0 0.004920464 0.007038737 0.00855687 0 0.000481157 0 0.005219562 0 0.001357195 8[13C]-UMP 0.003623338 0.008379038 0.016235161 0.018163681 0.025531045 0.023451997 0.015807741 0.011532974 0.008062605 0.002341962 0.004206006 0.006253457 9[13C]-UMP 0 0 0 0 0 0 0 0 0 0 0 0 CTP 0.949097256 0.969051904 0.932428401 0.925071169 0.925371088 0.911669861 0.911880222 0.98193484 0.988718421 0.979621573 0.963678324 0.973897198 1[13C]CTP 0 0 0 0 0 0 0 0 0 0 0 0 2[13C]CTP 0 0.017652954 0.008558586 0.011630242 0.010017804 0.013560217 0 0.005878868 0.011281579 0.009916192 0.02966906 0.020438146 3[13C]CTP 0.050902744 0.013295141 0.059013012 0.059764117 0.064611108 0.071527994 0.088119778 0.009122789 0 0.010462235 0.006652616 0.005664657 4[13C]CTP 0 0 0 0.000297823 0 0.000815174 0 0 0 0 0 0 5[13C]CTP 0 0 0 0.003236649 0 0 0 0 0 0 0 0 6[13C]CTP 0 0 0 0 0 0 0 0 0 0 0 0 7[13C]CTP 0 0 0 0 0 0 0 0.003063504 0 0 0 0 8[13C]CTP 0 0 0 0 0 0.002426754 0 0 0 0 0 0 9[13C]CTP 0 0 0 0 0 0 0 0 0 0 0 0 UTP 0.941629744 0.944245773 0.946881012 0.876313036 0.878280237 0.869478674 1 0.975297238 0.972235329 0.967133871 0.970021033 0.970895814 1[13C]UTP 0.010305618 0.003723167 0.004244034 0.008692651 0.006358643 0.010595068 0 0.002351086 0.004807867 0.006433841 0.002194954 0.001977142 2[13C]UTP 0.029229406 0.028321452 0.025195048 0.030535904 0.027280088 0.027289939 0 0.022351676 0.022956804 0.026432288 0.027784012 0.027127044 3[13C]UTP 0 0 0 0.002146117 0.002380339 0.003691867 0 0 0 0 0 0 4[13C]UTP 0 0 0.001082685 0.002989807 0.003627048 0.004824044 0 0 0 0 0 0 5[13C]UTP 0.0178704 0.01936294 0.01908396 0.059784837 0.060484288 0.062332332 0 0 0 0 0 0 6[13C]UTP 0 0.00212306 0 0.007906892 0.009351195 0.009076202 0 0 0 0 0 0 7[13C]UTP 0.000964833 0.002223609 0.003050204 0.010162374 0.011110446 0.011286847 0 0 0 0 0 0 8[13C]UTP 0 0 0.000463056 0.001468382 0.001127716 0.001425027 0 0 0 0 0 0 9[13C]UTP 0 0 0 0 0 0 0 0 0 0 0 0 citrate/isocitrate 0.198732739 0.194392736 0.193360057 0.197154701 0.175675948 0.191457292 0.380073472 0.424441801 0.422619044 0.259331606 0.257977666 0.258331913 1[13C]citrate/isocitrate 0.049284109 0.04714232 0.047608197 0.032229913 0.031146578 0.029920197 0.05144188 0.055647146 0.056520636 0.04565906 0.044609287 0.045938739 2[13C]citrate/isocitrate 0.354531758 0.357046407 0.354940922 0.39419499 0.403918724 0.402369922 0.323684663 0.311891649 0.311928625 0.388195192 0.388278414 0.388447136 3[13C]citrate/isocitrate 0.1056545 0.106643694 0.105356468 0.082689758 0.079278528 0.080488666 0.078377129 0.076454144 0.07748813 0.091731815 0.093654043 0.094152672 4[13C]citrate/isocitrate 0.17440032 0.174444308 0.175927092 0.179611168 0.187616519 0.18110107 0.107417968 0.086764173 0.08925168 0.135192326 0.136384493 0.134587851 5[13C]citrate/isocitrate 0.09498924 0.097283991 0.09853595 0.092664622 0.098655892 0.093597533 0.048933487 0.037792774 0.035850352 0.066635637 0.065540589 0.065303206 6[13C]citrate/isocitrate 0.022407334 0.023046543 0.024271315 0.021454849 0.023707811 0.02106532 0.0100714 0.007008313 0.006341533 0.013254364 0.013555508 0.013238483 cis-aconitate 0.335696674 0.323300087 0.315308367 0.502397886 0.393843843 0.380566444 0.673597784 0.751072899 0.688433112 0.353794327 0.362479425 0.362168418 1[13C]cis-aconitate 0.037480455 0.031158379 0.032765686 0.012175458 0.013835134 0.015625956 0.038341334 0.028040318 0.042637787 0.037058722 0.045457827 0.044361415 2[13C]cis-aconitate 0.303101052 0.309426674 0.311939418 0.253859668 0.312741606 0.316951626 0.189717265 0.145061681 0.169477367 0.354024157 0.346655505 0.338420619 3[13C]cis-aconitate 0.102233202 0.102415687 0.102619853 0.057784804 0.069987764 0.0710325 0.050126628 0.037301226 0.047762977 0.085471757 0.086673753 0.086676089 4[13C]cis-aconitate 0.1530414 0.151431514 0.157134198 0.119729365 0.139992857 0.142095836 0.040881593 0.028618733 0.038697297 0.11025873 0.107838371 0.111961203 5[13C]cis-aconitate 0.066720757 0.074235297 0.072582407 0.05055387 0.067763647 0.065487264 0.007335397 0.009905143 0.012315021 0.052691496 0.044073623 0.048785069 6[13C]cis-aconitate 0.00172646 0.008032363 0.007650071 0.003498949 0.001835149 0.008240374 0 0 0.000676439 0.006700811 0.006821495 0.007627187 2-oxoglutarate 0.507098569 0.514033564 0.506448659 0.524960121 0.527689328 0.518765801 0.598401951 0.597992557 0.579273701 0.488267912 0.481525172 0.493903257 1[13C]2-oxoglutarate 0.026126124 0.027792541 0.009614954 0.017374318 0.019606399 0.018416259 0.043592242 0.040267138 0.054569396 0.042429487 0.044849362 0.040430086 2[13C]2-oxoglutarate 0.234165318 0.248695782 0.261626376 0.268384564 0.26477473 0.263821025 0.257412449 0.250342547 0.24982271 0.289490734 0.292037079 0.287976757 3[13C]2-oxoglutarate 0.090589591 0.085716108 0.076563537 0.071117348 0.066109189 0.075263915 0.053103887 0.051639484 0.058075498 0.084574321 0.076733627 0.075983606 4[13C]2-oxoglutarate 0.099163468 0.092443306 0.106906292 0.091918759 0.097213434 0.094933035 0.039254252 0.047656906 0.04416646 0.072088453 0.080077456 0.076269023 5[13C]2-oxoglutarate 0.04285693 0.0313187 0.038840182 0.02624489 0.024606919 0.028799965 0.00823522 0.012101368 0.014092235 0.023149093 0.024777304 0.025437271 succinate 0.491041904 0.496415511 0.490505985 0.530676729 0.537565639 0.539326055 0.66585395 0.697922554 0.666436685 0.538975879 0.53190953 0.536531001 1[13C]succinate 0.05519573 0.054426156 0.053726719 0.032479765 0.030507801 0.031597399 0.068276106 0.062155162 0.06848202 0.065850815 0.066906356 0.065962811 2[13C]succinate 0.2389415 0.23572552 0.240600962 0.251643692 0.248617262 0.245583668 0.180799841 0.163193561 0.179809031 0.249237486 0.250526632 0.247326496 3[13C]succinate 0.15808082 0.157754331 0.159252832 0.136404291 0.136209194 0.135298666 0.063087623 0.057013261 0.063672252 0.106688313 0.108708533 0.108831494 4[13C]succinate 0.056740046 0.055678481 0.055913503 0.048795523 0.047100104 0.048194211 0.02198248 0.019715463 0.021600013 0.039247507 0.041948948 0.041348199 Fumarate 0.536211363 0.539045749 0.544612641 0.595974845 0.585753621 0.594108687 0.727628085 0.739141536 0.723780917 0.623556515 0.621384673 0.617279492 1[13C]Fumarate 0.06755731 0.065978868 0.061611387 0.040611827 0.037699597 0.039326682 0.053078869 0.050238426 0.048683506 0.053886585 0.055758602 0.058240713 2[13C]Fumarate 0.254512678 0.24922118 0.251700259 0.24331298 0.254475068 0.244591526 0.154123996 0.145487687 0.154428844 0.213212694 0.210692241 0.214119184 3[13C]Fumarate 0.141718649 0.145754203 0.142075713 0.120100348 0.122071714 0.121973105 0.06516905 0.065132352 0.073106734 0.109344205 0.112164484 0.110360611 4[13C]Fumarate 0 0 0 0 0 0 0 0 0 0 0 0 Malate 0.514804915 0.510364666 0.511246213 0.56976341 0.565376247 0.571846963 0.684986436 0.708206123 0.677095614 0.578895565 0.577617529 0.571649087 1[13C]Malate 0.060900046 0.061851561 0.059450983 0.04021133 0.03935848 0.038342386 0.05377429 0.053112636 0.0614347 0.062142985 0.059010276 0.061380908 2[13C]Malate 0.240674319 0.243516228 0.243766296 0.234134614 0.237421613 0.236399682 0.168382037 0.153739441 0.167994551 0.215813454 0.216801629 0.218879246 3[13C]Malate 0.142821271 0.143675679 0.145016236 0.122900164 0.124453847 0.121831561 0.073924633 0.068724129 0.07580147 0.116159286 0.11844052 0.11890229 4[13C]Malate 0.04079945 0.040591865 0.040520272 0.032990482 0.033389813 0.031579408 0.018932603 0.016217671 0.017673666 0.02698871 0.028130047 0.029188469 L-glutamate 0.447599921 0.441435816 0.441661723 0.503767837 0.502291817 0.509832607 0.570566304 0.571804864 0.566524735 0.461639992 0.459234878 0.463614978 1[13C]L-glutamate 0.037342119 0.037683096 0.036970189 0.022065419 0.020806531 0.021225295 0.053598882 0.052359272 0.054226244 0.046421063 0.045741654 0.045246688 2[13C]L-glutamate 0.263214611 0.268456425 0.264216566 0.270676816 0.274085939 0.269251458 0.253227042 0.252360037 0.255138505 0.307327776 0.306464175 0.30566387 3[13C]L-glutamate 0.099929151 0.101260481 0.102623847 0.077757679 0.076721998 0.075771306 0.061543821 0.061721906 0.062480464 0.08186181 0.081722201 0.08100838 4[13C]L-glutamate 0.115528544 0.115474753 0.117160117 0.096329287 0.096822216 0.094770114 0.047388747 0.047596327 0.048043843 0.077212651 0.07983601 0.078430421 5[13C]L-glutamate 0.036385654 0.035689428 0.037367557 0.029402962 0.029271499 0.029149219 0.013675203 0.014157595 0.013586208 0.025536707 0.027001081 0.026035663 D-glucose 0.124986614 0.113472755 0.101555068 0.087974507 0.0924176 0.137507122 0.030193637 0.034675885 0.048167766 0.090447126 0.112877466 0.267970784 1[13C]D-glucose 0 0 0 0 0 0 0 0 0 0 0 0 2[13C]D-glucose 0 0.001054871 0 0 0 0 0.000580825 0.000724548 0.000420512 0.002920853 0.000171721 0 3[13C]D-glucose 0 0 0 0 0 0 0 0 0 0 0 0 4[13C]D-glucose 0 0 0 0 0 0 0.001274787 0.000882807 0.001149004 0.000568804 0.000402913 0.000231354 5[13C]D-glucose 0.047876588 0.051043891 0.054585481 0.056303313 0.050558954 0.046896589 0.062239314 0.059523442 0.058359234 0.05583266 0.052429661 0.044607096 6[13C]D-glucose 0.827136797 0.834428483 0.843859451 0.855722181 0.857023446 0.815596289 0.905711437 0.904193318 0.891903484 0.850230558 0.834118238 0.687190765 Hexose phosphate 0.299984748 0.29875398 0.320258106 0.326251533 0.317614032 0.328124336 0.22330149 0.243363941 0.248443438 0.162100397 0.16418586 0.157254043 1[13C]Hexose phosphate 0.00826012 0.007681765 0.007887288 0.003497779 0.001525958 0.002375257 0.008240804 0.01104564 0.010067465 0.009487631 0.010962903 0.008827553 2[13C]Hexose phosphate 0.017934172 0.018510792 0.015207947 0.009408233 0.005161639 0.009661321 0.015830525 0.013668659 0.016175346 0.015758263 0.016726782 0.015239126 3[13C]Hexose phosphate 0.111878683 0.103727501 0.094381367 0.086542626 0.069889625 0.083324054 0.122056147 0.125623172 0.122638175 0.13314791 0.1341728 0.131403239 4[13C]Hexose phosphate 0.02640926 0.026849206 0.022831872 0.016371137 0.014264656 0.016167096 0.046685067 0.049279616 0.053240453 0.057580083 0.058620572 0.05758641 5[13C]Hexose phosphate 0.05489664 0.056008095 0.050712516 0.044851207 0.045782894 0.046542967 0.067885636 0.066811078 0.064934872 0.074799566 0.075772491 0.074841199 6[13C]Hexose phosphate 0.480636377 0.488468662 0.488720904 0.513077485 0.545761196 0.513804969 0.516000331 0.490207894 0.48450025 0.54712615 0.539558592 0.55484843 Fructose-1,6-bisphosphate 0.2217257 0.233980718 0.219293116 0.228915127 0.214107664 0.226779808 0.206445246 0.202047311 0.192764137 0.083065291 0.077655523 0.073298164 1[13C]Fructose-1,6-bisphosphate 0 0 0 0 0 0 0 0 0 0.000563103 0.002674292 0 2[13C]Fructose-1,6-bisphosphate 0.024897018 0.014803489 0.025205317 0.007938434 0.011483448 0.011083807 0.004492645 0.005139534 0.003888039 0.00971601 0.009884886 0.011104786 3[13C]Fructose-1,6-bisphosphate 0.036227524 0.048583731 0.04873985 0.051848848 0.043638352 0.050538724 0.088195337 0.098870485 0.102170074 0.142786727 0.15404661 0.150320402 4[13C]Fructose-1,6-bisphosphate 0.012880444 0.010109169 0.009527399 0.00808928 0.005515485 0.008260628 0.056543693 0.049207131 0.057471056 0.032407328 0.033856948 0.033849414 5[13C]Fructose-1,6-bisphosphate 0.082143576 0.078300498 0.068238526 0.049016183 0.05170955 0.050894887 0.030703465 0.058682664 0.059477012 0.070658748 0.071108699 0.069785297 6[13C]Fructose-1,6-bisphosphate 0.622125737 0.614222396 0.628995793 0.654192128 0.673545501 0.652442145 0.613619613 0.586052874 0.584229682 0.660802793 0.650773042 0.661641937 3PG/2PG 0.090571294 0.060877228 0.245193577 0.188937553 0.236070311 0.253182903 0.366972811 0.385925784 0.364314619 0.256525802 0.207037435 0.215942225 1[13C]3PG/2PG 0 0 0 0 0 0 0 0 0 0 0 0 2[13C]3PG/2PG 0 0 0 0 0 0 0 0 0 0.007358405 0 0.008392336 3[13C]3PG/2PG 0.909428706 0.939122772 0.754806423 0.811062447 0.763929689 0.746817097 0.633027189 0.614074216 0.635685381 0.736115792 0.792962565 0.775665439 pyruvate 0.68997463 0.653446296 0.690945613 0.498483533 0.500073603 0.486134666 0.595439008 0.627042002 0.631376078 0.431738103 0.559726495 0.582070115 1[13C]pyruvate 0.027125514 0.026773891 0.023710095 0.022496248 0.025656002 0.026637174 0.010329553 0.011813588 0.007885724 0.023423756 0.025036078 0.019663535 2[13C]pyruvate 0.04333767 0.040379817 0.042691574 0.045529748 0.044440618 0.045158863 0.018979132 0.020181602 0.017758309 0.036010606 0.035146585 0.034999012 3[13C]pyruvate 0.239562185 0.279399996 0.242652718 0.433490471 0.429829776 0.442069297 0.375252307 0.340962809 0.342979888 0.508827534 0.380090842 0.363267337 Lactate 0.292990561 0.292414074 0.286296215 0.188264611 0.195300641 0.190555311 0.231235761 0.246146978 0.221857919 0.113174123 0.116102155 0.119431611 1[13C]Lactate 0.018731487 0.018544848 0.017603197 0.0105957 0.010595653 0.010618209 0.015065907 0.014860624 0.015691697 0.016959594 0.01663615 0.015990483 2[13C]Lactate 0.045224668 0.044698955 0.043964426 0.039795886 0.038452901 0.038992446 0.038724075 0.037271615 0.038280415 0.045656713 0.044498983 0.04393822 3[13C]Lactate 0.643053284 0.644342123 0.652136162 0.761343803 0.755650805 0.759834033 0.714974256 0.701720783 0.724169969 0.824209569 0.822762712 0.820639686 Glycerol 3-phosphate 0.503364782 0.489418878 0.486836358 0.347425514 0.340680879 0.350539043 0.375982525 0.386810275 0.389029901 0.335389954 0.348476747 0.343025086 1[13C]Glycerol 3-phosphate 0.015547783 0.010793065 0.021299009 0.013648812 0.012164742 0.013988338 0.014402835 0.007100553 0.008007632 0.017281203 0.018891511 0.018940619 2[13C]Glycerol 3-phosphate 0.030326623 0.023299923 0.028043442 0.03267432 0.027602737 0.027159497 0.032196649 0.028558835 0.027272803 0.033390537 0.032860856 0.030722298 3[13C]Glycerol 3-phosphate 0.450760813 0.476488135 0.463821191 0.606251354 0.619551642 0.608313123 0.577417991 0.577530337 0.575689664 0.613938306 0.599770886 0.607311997 D-ribose-5-phosphate 0.68153642 0.661968725 0.607541145 0.44047796 0.465269805 0.387370308 0.797497324 0.799821418 0.77843397 0.526145448 0.498599346 0.536944435 1[13C]ribose-5-phosphate 0 0 0 0 0 0 0 0.002332225 0.008583454 0.00628263 0.004624051 0.004975336 2[13C]ribose-5-phosphate 0 0 0 0.008188137 0 0.014488646 0 0.002217516 0 0.024834369 0.028956796 0.023293129 3[13C]ribose-5-phosphate 0.018132656 0.012790902 0.011412781 0.04477474 0.033815849 0.064622211 0.04887826 0.041399711 0.043009879 0.18911336 0.186776394 0.177204977 4[13C]ribose-5-phosphate 0 0.011413761 0.033113457 0.015643655 0.011426405 0.015690994 0.014135156 0.017183983 0.022805001 0.032053964 0.031673094 0.029144295 5[13C]ribose-5-phosphate 0.300330924 0.313826613 0.347932617 0.490915508 0.489487942 0.517827842 0.139489261 0.137045147 0.147167696 0.221570229 0.249370319 0.228437828 Sedoheptulose 7-phosphate 0.526015306 0.537194048 0.575207679 0.660367128 0.680005677 0.654830175 0.673416782 0.681925512 0.659508602 0.487007636 0.479259892 0.485875216 1[13C]Sedoheptulose 7-phosphate 0.012588784 0.021376218 0.006283567 0.005253909 0 0 0.01599495 0.005555011 0.015239746 0.007131661 0.017239936 0.011905754 2[13C]Sedoheptulose 7-phosphate 0.020762667 0.006279211 0.019121889 0.006010891 0.010815789 0.010922111 0.025190559 0.021990572 0.025628933 0.02659522 0.031776623 0.02565742 3[13C]Sedoheptulose 7-phosphate 0.077634422 0.049654283 0.044408672 0.017158462 0.011769402 0.021914342 0.028565841 0.031118268 0.025460242 0.054491882 0.06262863 0.062556187 4[13C]Sedoheptulose 7-phosphate 0.072653192 0.063272343 0.058133801 0.031145552 0.027297798 0.033248519 0.048631762 0.05541946 0.059105151 0.077863294 0.078169298 0.070013488 5[13C]Sedoheptulose 7-phosphate 0.024851951 0.01483192 0.014518134 0.012346719 0.016848449 0.010026443 0.017617407 0.020115947 0.018941555 0.033669914 0.031775542 0.0383143 6[13C]Sedoheptulose 7-phosphate 0.019609591 0.041162193 0.033608738 0.027553478 0.013610283 0.029753548 0.031627738 0.030472197 0.029135503 0.064124592 0.054965734 0.061247199 7[13C]Sedoheptulose 7-phosphate 0.245884086 0.266229785 0.248717519 0.240163861 0.239652602 0.239304863 0.158954961 0.153403032 0.166980269 0.249115802 0.244184346 0.244430437 ornithine 1 1 1 1 1 1 1 1 1 1 0.999994653 1 1[13C]ornithine 0 0 0 0 0 0 0 0 0 0 5.34733E-06 0 2[13C]ornithine 0 0 0 0 0 0 0 0 0 0 0 0 3[13C]ornithine 0 0 0 0 0 0 0 0 0 0 0 0 4[13C]ornithine 0 0 0 0 0 0 0 0 0 0 0 0 5[13C]ornithine 0 0 0 0 0 0 0 0 0 0 0 0 asparagine 0.432845151 0.435694074 0.434760162 0.417271252 0.413542977 0.417246796 0.544481351 0.534727619 0.534908872 0.475848118 0.473492534 0.486242366 1[13C]asparagine 0.439772576 0.436951765 0.434332639 0.454271868 0.456970788 0.449937991 0.353069505 0.360805851 0.366240597 0.398968095 0.406854362 0.392217976 2[13C]asparagine 0.127382273 0.127354161 0.1309072 0.12845688 0.129486235 0.132815213 0.102449144 0.10446653 0.098850531 0.125183787 0.119653104 0.121539658 3[13C]asparagine 0 0 0 0 0 0 0 0 0 0 0 0 4[13C]asparagine 0 0 0 0 0 0 0 0 0 0 0 0 2-Ketobutyric acid/acetoacetate 0.645205745 0.685076883 0.660587928 0.70186994 0.693455248 0.720546704 0.668432094 0.690049771 0.668998825 0.624325317 0.594645505 0.62406645 2-Ketobutyric acid/acetoacetate-1 0.041434511 0.029461483 0.033687789 0.016726261 0.024813328 0.021054957 0.060778146 0.056663993 0.066037188 0.046084785 0.052340612 0.049787311 2-Ketobutyric acid/acetoacetate-2 0.164722267 0.150274891 0.157297555 0.164368356 0.160374682 0.149478128 0.186638372 0.172742331 0.185740787 0.208420256 0.224474817 0.204255683 2-Ketobutyric acid/acetoacetate-3 0.094549532 0.091338374 0.094997863 0.069120925 0.073800999 0.063881669 0.055635051 0.050917081 0.051611772 0.078025495 0.08758792 0.075795055 2-Ketobutyric acid/acetoacetate-4 0.054087946 0.043848368 0.053428865 0.047914518 0.047555743 0.045038542 0.028516337 0.029626824 0.027611428 0.043144147 0.040951145 0.046095501 5-oxoproline/L-1-Pyrroline-3-hydroxy-5-carboxylate 0.479804222 0.476784575 0.476059996 0.537273255 0.533621968 0.53987358 0.600675073 0.602701729 0.59636769 0.49484582 0.492788979 0.49359754 5-oxoproline/L-1-Pyrroline-3-hydroxy-5-carboxylate-1 0.037022474 0.036068935 0.035066531 0.019582815 0.022276864 0.021043021 0.051243752 0.05178397 0.053171416 0.047528719 0.044306188 0.0455513 5-oxoproline/L-1-Pyrroline-3-hydroxy-5-carboxylate-2 0.251919417 0.256398243 0.252945142 0.254920528 0.259296751 0.256229378 0.233138719 0.233115785 0.239365657 0.292339734 0.289578968 0.288960679 5-oxoproline/L-1-Pyrroline-3-hydroxy-5-carboxylate-3 0.093960003 0.094464718 0.096396473 0.072734919 0.07026649 0.070323554 0.061145595 0.058077868 0.05659812 0.072391424 0.076002746 0.077772593 5-oxoproline/L-1-Pyrroline-3-hydroxy-5-carboxylate-4 0.105238395 0.104233124 0.106013059 0.088871834 0.088093613 0.085779594 0.041282595 0.041749778 0.042628118 0.070020162 0.074508891 0.071065789 5-oxoproline/L-1-Pyrroline-3-hydroxy-5-carboxylate-5 0.032055489 0.032050405 0.033518801 0.026616648 0.026444315 0.026750873 0.012514267 0.012570871 0.011868999 0.022874141 0.022814228 0.023052099 L-2-aminoadipate 0.976216012 0.977692469 0.974319104 0.968801746 0.969558129 0.967010497 0.998139079 1 0.998074215 0.998959672 0.999730423 1 L-2-aminoadipate-1 0 0 0.003417773 0.000319478 0 0 0 0 0 0 0 0 L-2-aminoadipate-2 0.023783988 0.021970003 0.022093917 0.03047691 0.030252244 0.032547001 5.79505E-06 0 0 0 0 0 L-2-aminoadipate-3 0 0 0 0 0 0 0 0 0 0 0 0 L-2-aminoadipate-4 0 0 0 0 0.000189627 0 0 0 0 0 0 0 L-2-aminoadipate-5 0 0.000337528 0.000169206 0.000401867 0 0.000442501 0.001855126 0 0.001925785 0.001040328 0.000269577 0 L-2-aminoadipate-6 0 0 0 0 0 0 0 0 0 0 0 0 N-acetyl-L-aspartate 0.977594362 0.978594478 0.976882052 0.978602807 0.980302602 0.979225825 0.984969309 0.986299146 0.982806998 0.973206456 0.976939891 0.975206405 N-acetyl-L-aspartate-1 0.001006577 0.001222322 0.001031024 0.001165681 0.002148063 0.001193901 0.002688594 0.000893657 0.003634638 0.003216333 0.002366685 0.002553502 N-acetyl-L-aspartate-2 0.014319322 0.013541361 0.015191675 0.014503447 0.012710367 0.01463831 0.009258941 0.009405183 0.009817958 0.017668712 0.015316203 0.016119712 N-acetyl-L-aspartate-3 0.001824304 0.001432666 0.00180282 0.001201236 0.000838313 0.001113684 0.001473962 0.001920994 0.001831676 0.002795488 0.002610293 0.003167498 N-acetyl-L-aspartate-4 0.005255435 0.005209172 0.00509243 0.004526829 0.004000654 0.00382828 0.001609194 0.001481021 0.00190873 0.003113011 0.002766927 0.002952883 N-acetyl-L-aspartate-5 0 0 0 0 0 0 0 0 0 0 0 0 N-acetyl-L-aspartate-6 0 0 0 0 0 0 0 0 0 0 0 0 MS_METABOLITE_DATA_END #METABOLITES METABOLITES_START metabolite_name Chemical Formula HMDB PubChem KEGG HMDB PubChem KEGG Aspartate C4H7NO4 HMDB00191 5960 C00049 1[13C]Aspartate C4H7NO4 HMDB00191 5960 C00049 2[13C]Aspartate C4H7NO4 HMDB00191 5960 C00049 3[13C]Aspartate C4H7NO4 HMDB00191 5960 C00049 4[13C]Aspartate C4H7NO4 HMDB00191 5960 C00049 N(omega)-(L-Arginino)succinate C10H18N4O6 HMDB00052 16950 C03406 1[13C]N(omega)-(L-Arginino)succinate C10H18N4O6 HMDB00052 16950 C03406 2[13C]N(omega)-(L-Arginino)succinate C10H18N4O6 HMDB00052 16950 C03406 3[13C]N(omega)-(L-Arginino)succinate C10H18N4O6 HMDB00052 16950 C03406 4[13C]N(omega)-(L-Arginino)succinate C10H18N4O6 HMDB00052 16950 C03406 5[13C]N(omega)-(L-Arginino)succinate C10H18N4O6 HMDB00052 16950 C03406 6[13C]N(omega)-(L-Arginino)succinate C10H18N4O6 HMDB00052 16950 C03406 7[13C]N(omega)-(L-Arginino)succinate C10H18N4O6 HMDB00052 16950 C03406 8[13C]N(omega)-(L-Arginino)succinate C10H18N4O6 HMDB00052 16950 C03406 9[13C]N(omega)-(L-Arginino)succinate C10H18N4O6 HMDB00052 16950 C03406 10[13C]N(omega)-(L-Arginino)succinate C10H18N4O6 HMDB00052 16950 C03406 laurate C12H24O2 HMDB00638 3893 C02679 1[13C]laurate C12H24O2 HMDB00638 3893 C02679 2[13C]laurate C12H24O2 HMDB00638 3893 C02679 3[13C]laurate C12H24O2 HMDB00638 3893 C02679 4[13C]laurate C12H24O2 HMDB00638 3893 C02679 5[13C]laurate C12H24O2 HMDB00638 3893 C02679 6[13C]laurate C12H24O2 HMDB00638 3893 C02679 7[13C]laurate C12H24O2 HMDB00638 3893 C02679 8[13C]laurate C12H24O2 HMDB00638 3893 C02679 9[13C]laurate C12H24O2 HMDB00638 3893 C02679 10[13C]laurate C12H24O2 HMDB00638 3893 C02679 11[13C]laurate C12H24O2 HMDB00638 3893 C02679 12[13C]laurate C12H24O2 HMDB00638 3893 C02679 myristate C14H28O2 HMDB00806 11005 C06424 1[13C]myristate C14H28O2 HMDB00806 11005 C06424 2[13C]myristate C14H28O2 HMDB00806 11005 C06424 3[13C]myristate C14H28O2 HMDB00806 11005 C06424 4[13C]myristate C14H28O2 HMDB00806 11005 C06424 5[13C]myristate C14H28O2 HMDB00806 11005 C06424 6[13C]myristate C14H28O2 HMDB00806 11005 C06424 7[13C]myristate C14H28O2 HMDB00806 11005 C06424 8[13C]myristate C14H28O2 HMDB00806 11005 C06424 9[13C]myristate C14H28O2 HMDB00806 11005 C06424 10[13C]myristate C14H28O2 HMDB00806 11005 C06424 11[13C]myristate C14H28O2 HMDB00806 11005 C06424 12[13C]myristate C14H28O2 HMDB00806 11005 C06424 13[13C]myristate C14H28O2 HMDB00806 11005 C06424 14[13C]myristate C14H28O2 HMDB00806 11005 C06424 palmitate C16H32O2 HMDB00220 985 C00249 1[13C]palmitate C16H32O2 HMDB00220 985 C00249 2[13C]palmitate C16H32O2 HMDB00220 985 C00249 3[13C]palmitate C16H32O2 HMDB00220 985 C00249 4[13C]palmitate C16H32O2 HMDB00220 985 C00249 5[13C]palmitate C16H32O2 HMDB00220 985 C00249 6[13C]palmitate C16H32O2 HMDB00220 985 C00249 7[13C]palmitate C16H32O2 HMDB00220 985 C00249 8[13C]palmitate C16H32O2 HMDB00220 985 C00249 9[13C]palmitate C16H32O2 HMDB00220 985 C00249 10[13C]palmitate C16H32O2 HMDB00220 985 C00249 11[13C]palmitate C16H32O2 HMDB00220 985 C00249 12[13C]palmitate C16H32O2 HMDB00220 985 C00249 13[13C]palmitate C16H32O2 HMDB00220 985 C00249 14[13C]palmitate C16H32O2 HMDB00220 985 C00249 15[13C]palmitate C16H32O2 HMDB00220 985 C00249 16[13C]palmitate C16H32O2 HMDB00220 985 C00249 UDP-D-glucuronate C15H22N2O18P2 HMDB00935 17473 C00167 1[13C]UDP-D-glucuronate C15H22N2O18P2 HMDB00935 17473 C00167 2[13C]UDP-D-glucuronate C15H22N2O18P2 HMDB00935 17473 C00167 3[13C]UDP-D-glucuronate C15H22N2O18P2 HMDB00935 17473 C00167 4[13C]UDP-D-glucuronate C15H22N2O18P2 HMDB00935 17473 C00167 5[13C]UDP-D-glucuronate C15H22N2O18P2 HMDB00935 17473 C00167 6[13C]UDP-D-glucuronate C15H22N2O18P2 HMDB00935 17473 C00167 7[13C]UDP-D-glucuronate C15H22N2O18P2 HMDB00935 17473 C00167 8[13C]UDP-D-glucuronate C15H22N2O18P2 HMDB00935 17473 C00167 9[13C]UDP-D-glucuronate C15H22N2O18P2 HMDB00935 17473 C00167 10[13C]UDP-D-glucuronate C15H22N2O18P2 HMDB00935 17473 C00167 11[13C]UDP-D-glucuronate C15H22N2O18P2 HMDB00935 17473 C00167 12[13C]UDP-D-glucuronate C15H22N2O18P2 HMDB00935 17473 C00167 13[13C]UDP-D-glucuronate C15H22N2O18P2 HMDB00935 17473 C00167 14[13C]UDP-D-glucuronate C15H22N2O18P2 HMDB00935 17473 C00167 15[13C]UDP-D-glucuronate C15H22N2O18P2 HMDB00935 17473 C00167 UDP-glucose C15H24N2O17P2 HMDB00286 53477679 C00029 1[13C]UDP-glucose C15H24N2O17P2 HMDB00286 53477679 C00029 2[13C]UDP-glucose C15H24N2O17P2 HMDB00286 53477679 C00029 3[13C]UDP-glucose C15H24N2O17P2 HMDB00286 53477679 C00029 4[13C]UDP-glucose C15H24N2O17P2 HMDB00286 53477679 C00029 5[13C]UDP-glucose C15H24N2O17P2 HMDB00286 53477679 C00029 6[13C]UDP-glucose C15H24N2O17P2 HMDB00286 53477679 C00029 7[13C]UDP-glucose C15H24N2O17P2 HMDB00286 53477679 C00029 8[13C]UDP-glucose C15H24N2O17P2 HMDB00286 53477679 C00029 9[13C]UDP-glucose C15H24N2O17P2 HMDB00286 53477679 C00029 10[13C]UDP-glucose C15H24N2O17P2 HMDB00286 53477679 C00029 11[13C]UDP-glucose C15H24N2O17P2 HMDB00286 53477679 C00029 12[13C]UDP-glucose C15H24N2O17P2 HMDB00286 53477679 C00029 13[13C]UDP-glucose C15H24N2O17P2 HMDB00286 53477679 C00029 14[13C]UDP-glucose C15H24N2O17P2 HMDB00286 53477679 C00029 15[13C]UDP-glucose C15H24N2O17P2 HMDB00286 53477679 C00029 UDP-N-acetyl-alpha-D-glucosamine C17H27N3O17P2 HMDB00290 445675 C00043 1[13C]UDP-N-acetyl-alpha-D-glucosamine C17H27N3O17P2 HMDB00290 445675 C00043 2[13C]UDP-N-acetyl-alpha-D-glucosamine C17H27N3O17P2 HMDB00290 445675 C00043 3[13C]UDP-N-acetyl-alpha-D-glucosamine C17H27N3O17P2 HMDB00290 445675 C00043 4[13C]UDP-N-acetyl-alpha-D-glucosamine C17H27N3O17P2 HMDB00290 445675 C00043 5[13C]UDP-N-acetyl-alpha-D-glucosamine C17H27N3O17P2 HMDB00290 445675 C00043 6[13C]UDP-N-acetyl-alpha-D-glucosamine C17H27N3O17P2 HMDB00290 445675 C00043 7[13C]UDP-N-acetyl-alpha-D-glucosamine C17H27N3O17P2 HMDB00290 445675 C00043 8[13C]UDP-N-acetyl-alpha-D-glucosamine C17H27N3O17P2 HMDB00290 445675 C00043 9[13C]UDP-N-acetyl-alpha-D-glucosamine C17H27N3O17P2 HMDB00290 445675 C00043 10[13C]UDP-N-acetyl-alpha-D-glucosamine C17H27N3O17P2 HMDB00290 445675 C00043 11[13C]UDP-N-acetyl-alpha-D-glucosamine C17H27N3O17P2 HMDB00290 445675 C00043 12[13C]UDP-N-acetyl-alpha-D-glucosamine C17H27N3O17P2 HMDB00290 445675 C00043 13[13C]UDP-N-acetyl-alpha-D-glucosamine C17H27N3O17P2 HMDB00290 445675 C00043 14[13C]UDP-N-acetyl-alpha-D-glucosamine C17H27N3O17P2 HMDB00290 445675 C00043 15[13C]UDP-N-acetyl-alpha-D-glucosamine C17H27N3O17P2 HMDB00290 445675 C00043 16[13C]UDP-N-acetyl-alpha-D-glucosamine C17H27N3O17P2 HMDB00290 445675 C00043 17[13C]UDP-N-acetyl-alpha-D-glucosamine C17H27N3O17P2 HMDB00290 445675 C00043 myo-inositol C6H12O6 HMDB00211 NA C00137 1[13C]myo-inositol C6H12O6 HMDB00211 NA C00137 2[13C]myo-inositol C6H12O6 HMDB00211 NA C00137 3[13C]myo-inositol C6H12O6 HMDB00211 NA C00137 4[13C]myo-inositol C6H12O6 HMDB00211 NA C00137 5[13C]myo-inositol C6H12O6 HMDB00211 NA C00137 6[13C]myo-inositol C6H12O6 HMDB00211 NA C00137 ATP C10H16N5O13P3 HMDB00538 5957 C00002 1[13C]-ATP C10H16N5O13P3 HMDB00538 5957 C00002 2[13C]-ATP C10H16N5O13P3 HMDB00538 5957 C00002 3[13C]-ATP C10H16N5O13P3 HMDB00538 5957 C00002 4[13C]-ATP C10H16N5O13P3 HMDB00538 5957 C00002 5[13C]-ATP C10H16N5O13P3 HMDB00538 5957 C00002 6[13C]-ATP C10H16N5O13P3 HMDB00538 5957 C00002 7[13C]-ATP C10H16N5O13P3 HMDB00538 5957 C00002 8[13C]-ATP C10H16N5O13P3 HMDB00538 5957 C00002 9[13C]-ATP C10H16N5O13P3 HMDB00538 5957 C00002 10[13C]-ATP C10H16N5O13P3 HMDB00538 5957 C00002 AMP C10H14N5O7P HMDB00045 6083 C00020 1[13C]AMP C10H14N5O7P HMDB00045 6083 C00020 2[13C]AMP C10H14N5O7P HMDB00045 6083 C00020 3[13C]AMP C10H14N5O7P HMDB00045 6083 C00020 4[13C]AMP C10H14N5O7P HMDB00045 6083 C00020 5[13C]AMP C10H14N5O7P HMDB00045 6083 C00020 6[13C]AMP C10H14N5O7P HMDB00045 6083 C00020 7[13C]AMP C10H14N5O7P HMDB00045 6083 C00020 8[13C]AMP C10H14N5O7P HMDB00045 6083 C00020 9[13C]AMP C10H14N5O7P HMDB00045 6083 C00020 10[13C]AMP C10H14N5O7P HMDB00045 6083 C00020 UMP C9H13N2O9P HMDB00288 6030 C00105 METPA0176 NA C01368 1[13C]-UMP C9H13N2O9P HMDB00288 6030 C00105 METPA0176 NA C01368 2[13C]-UMP C9H13N2O9P HMDB00288 6030 C00105 METPA0176 NA C01368 3[13C]-UMP C9H13N2O9P HMDB00288 6030 C00105 METPA0176 NA C01368 4[13C]-UMP C9H13N2O9P HMDB00288 6030 C00105 METPA0176 NA C01368 5[13C]-UMP C9H13N2O9P HMDB00288 6030 C00105 METPA0176 NA C01368 6[13C]-UMP C9H13N2O9P HMDB00288 6030 C00105 METPA0176 NA C01368 7[13C]-UMP C9H13N2O9P HMDB00288 6030 C00105 METPA0176 NA C01368 8[13C]-UMP C9H13N2O9P HMDB00288 6030 C00105 METPA0176 NA C01368 9[13C]-UMP C9H13N2O9P HMDB00288 6030 C00105 METPA0176 NA C01368 CTP C9H16N3O14P3 HMDB00082 6176 C00063 1[13C]CTP C9H16N3O14P3 HMDB00082 6176 C00063 2[13C]CTP C9H16N3O14P3 HMDB00082 6176 C00063 3[13C]CTP C9H16N3O14P3 HMDB00082 6176 C00063 4[13C]CTP C9H16N3O14P3 HMDB00082 6176 C00063 5[13C]CTP C9H16N3O14P3 HMDB00082 6176 C00063 6[13C]CTP C9H16N3O14P3 HMDB00082 6176 C00063 7[13C]CTP C9H16N3O14P3 HMDB00082 6176 C00063 8[13C]CTP C9H16N3O14P3 HMDB00082 6176 C00063 9[13C]CTP C9H16N3O14P3 HMDB00082 6176 C00063 UTP C9H15N2O15P3 HMDB00285 6133 C00075 1[13C]UTP C9H15N2O15P3 HMDB00285 6133 C00075 2[13C]UTP C9H15N2O15P3 HMDB00285 6133 C00075 3[13C]UTP C9H15N2O15P3 HMDB00285 6133 C00075 4[13C]UTP C9H15N2O15P3 HMDB00285 6133 C00075 5[13C]UTP C9H15N2O15P3 HMDB00285 6133 C00075 6[13C]UTP C9H15N2O15P3 HMDB00285 6133 C00075 7[13C]UTP C9H15N2O15P3 HMDB00285 6133 C00075 8[13C]UTP C9H15N2O15P3 HMDB00285 6133 C00075 9[13C]UTP C9H15N2O15P3 HMDB00285 6133 C00075 citrate/isocitrate C6H8O7 HMDB00094 311 C00158 HMDB00193 1198 C00311 1[13C]citrate/isocitrate C6H8O7 HMDB00094 311 C00158 HMDB00193 1198 C00311 2[13C]citrate/isocitrate C6H8O7 HMDB00094 311 C00158 HMDB00193 1198 C00311 3[13C]citrate/isocitrate C6H8O7 HMDB00094 311 C00158 HMDB00193 1198 C00311 4[13C]citrate/isocitrate C6H8O7 HMDB00094 311 C00158 HMDB00193 1198 C00311 5[13C]citrate/isocitrate C6H8O7 HMDB00094 311 C00158 HMDB00193 1198 C00311 6[13C]citrate/isocitrate C6H8O7 HMDB00094 311 C00158 HMDB00193 1198 C00311 cis-aconitate C6H6O6 HMDB00072 643757 C00417 1[13C]cis-aconitate C6H6O6 HMDB00072 643757 C00417 2[13C]cis-aconitate C6H6O6 HMDB00072 643757 C00417 3[13C]cis-aconitate C6H6O6 HMDB00072 643757 C00417 4[13C]cis-aconitate C6H6O6 HMDB00072 643757 C00417 5[13C]cis-aconitate C6H6O6 HMDB00072 643757 C00417 6[13C]cis-aconitate C6H6O6 HMDB00072 643757 C00417 2-oxoglutarate C5H6O5 HMDB00208 51 C00026 1[13C]2-oxoglutarate C5H6O5 HMDB00208 51 C00026 2[13C]2-oxoglutarate C5H6O5 HMDB00208 51 C00026 3[13C]2-oxoglutarate C5H6O5 HMDB00208 51 C00026 4[13C]2-oxoglutarate C5H6O5 HMDB00208 51 C00026 5[13C]2-oxoglutarate C5H6O5 HMDB00208 51 C00026 succinate C4H6O4 HMDB00254 1110 C00042 1[13C]succinate C4H6O4 HMDB00254 1110 C00042 2[13C]succinate C4H6O4 HMDB00254 1110 C00042 3[13C]succinate C4H6O4 HMDB00254 1110 C00042 4[13C]succinate C4H6O4 HMDB00254 1110 C00042 Fumarate C4H4O4 HMDB00134 444972 C00122 1[13C]Fumarate C4H4O4 HMDB00134 444972 C00122 2[13C]Fumarate C4H4O4 HMDB00134 444972 C00122 3[13C]Fumarate C4H4O4 HMDB00134 444972 C00122 4[13C]Fumarate C4H4O4 HMDB00134 444972 C00122 Malate C4H6O5 HMDB00156 222656 C00149 1[13C]Malate C4H6O5 HMDB00156 222656 C00149 2[13C]Malate C4H6O5 HMDB00156 222656 C00149 3[13C]Malate C4H6O5 HMDB00156 222656 C00149 4[13C]Malate C4H6O5 HMDB00156 222656 C00149 L-glutamate C5H9NO4 HMDB00148 33032 C00025 1[13C]L-glutamate C5H9NO4 HMDB00148 33032 C00025 2[13C]L-glutamate C5H9NO4 HMDB00148 33032 C00025 3[13C]L-glutamate C5H9NO4 HMDB00148 33032 C00025 4[13C]L-glutamate C5H9NO4 HMDB00148 33032 C00025 5[13C]L-glutamate C5H9NO4 HMDB00148 33032 C00025 D-glucose C6H12O6 HMDB03345 79025 C00267 1[13C]D-glucose C6H12O6 HMDB03345 79025 C00267 2[13C]D-glucose C6H12O6 HMDB03345 79025 C00267 3[13C]D-glucose C6H12O6 HMDB03345 79025 C00267 4[13C]D-glucose C6H12O6 HMDB03345 79025 C00267 5[13C]D-glucose C6H12O6 HMDB03345 79025 C00267 6[13C]D-glucose C6H12O6 HMDB03345 79025 C00267 Hexose phosphate C6H13O9P HMDB0001586 439165 C00103 HMDB0001076 10400369 C01094 1[13C]Hexose phosphate C6H13O9P HMDB0001586 439165 C00103 HMDB0001076 10400369 C01094 2[13C]Hexose phosphate C6H13O9P HMDB0001586 439165 C00103 HMDB0001076 10400369 C01094 3[13C]Hexose phosphate C6H13O9P HMDB0001586 439165 C00103 HMDB0001076 10400369 C01094 4[13C]Hexose phosphate C6H13O9P HMDB0001586 439165 C00103 HMDB0001076 10400369 C01094 5[13C]Hexose phosphate C6H13O9P HMDB0001586 439165 C00103 HMDB0001076 10400369 C01094 6[13C]Hexose phosphate C6H13O9P HMDB0001586 439165 C00103 HMDB0001076 10400369 C01094 Fructose-1,6-bisphosphate C6H14O12P2 HMDB60444 10267 C05378 1[13C]Fructose-1,6-bisphosphate C6H14O12P2 HMDB60444 10267 C05378 2[13C]Fructose-1,6-bisphosphate C6H14O12P2 HMDB60444 10267 C05378 3[13C]Fructose-1,6-bisphosphate C6H14O12P2 HMDB60444 10267 C05378 4[13C]Fructose-1,6-bisphosphate C6H14O12P2 HMDB60444 10267 C05378 5[13C]Fructose-1,6-bisphosphate C6H14O12P2 HMDB60444 10267 C05378 6[13C]Fructose-1,6-bisphosphate C6H14O12P2 HMDB60444 10267 C05378 3PG/2PG C3H7O6P HMDB0001112 439168 C00118 HMDB0060180 439278 C00631 1[13C]3PG/2PG C3H7O6P HMDB0001112 439168 C00118 HMDB0060180 439278 C00631 2[13C]3PG/2PG C3H7O6P HMDB0001112 439168 C00118 HMDB0060180 439278 C00631 3[13C]3PG/2PG C3H7O6P HMDB0001112 439168 C00118 HMDB0060180 439278 C00631 pyruvate C3H4O3 HMDB00243 1060 C00022 1[13C]pyruvate C3H4O3 HMDB00243 1060 C00022 2[13C]pyruvate C3H4O3 HMDB00243 1060 C00022 3[13C]pyruvate C3H4O3 HMDB00243 1060 C00022 Lactate C3H6O3 HMDB00190 107689 C00186 1[13C]Lactate C3H6O3 HMDB00190 107689 C00186 2[13C]Lactate C3H6O3 HMDB00190 107689 C00186 3[13C]Lactate C3H6O3 HMDB00190 107689 C00186 Glycerol 3-phosphate C3H9O6P HMDB00126 439162 C00093 1[13C]Glycerol 3-phosphate C3H9O6P HMDB00126 439162 C00093 2[13C]Glycerol 3-phosphate C3H9O6P HMDB00126 439162 C00093 3[13C]Glycerol 3-phosphate C3H9O6P HMDB00126 439162 C00093 D-ribose-5-phosphate C5H11O8P HMDB01548 3417 C00117 1[13C]ribose-5-phosphate C5H11O8P HMDB01548 3417 C00117 2[13C]ribose-5-phosphate C5H11O8P HMDB01548 3417 C00117 3[13C]ribose-5-phosphate C5H11O8P HMDB01548 3417 C00117 4[13C]ribose-5-phosphate C5H11O8P HMDB01548 3417 C00117 5[13C]ribose-5-phosphate C5H11O8P HMDB01548 3417 C00117 Sedoheptulose 7-phosphate C7H15O10P METPA0585 NA C05382 1[13C]Sedoheptulose 7-phosphate C7H15O10P METPA0585 NA C05382 2[13C]Sedoheptulose 7-phosphate C7H15O10P METPA0585 NA C05382 3[13C]Sedoheptulose 7-phosphate C7H15O10P METPA0585 NA C05382 4[13C]Sedoheptulose 7-phosphate C7H15O10P METPA0585 NA C05382 5[13C]Sedoheptulose 7-phosphate C7H15O10P METPA0585 NA C05382 6[13C]Sedoheptulose 7-phosphate C7H15O10P METPA0585 NA C05382 7[13C]Sedoheptulose 7-phosphate C7H15O10P METPA0585 NA C05382 ornithine C5H12N2O2 HMDB00214 6262 C00077 1[13C]ornithine C5H12N2O2 HMDB00214 6262 C00077 2[13C]ornithine C5H12N2O2 HMDB00214 6262 C00077 3[13C]ornithine C5H12N2O2 HMDB00214 6262 C00077 4[13C]ornithine C5H12N2O2 HMDB00214 6262 C00077 5[13C]ornithine C5H12N2O2 HMDB00214 6262 C00077 asparagine C4H8N2O3 HMDB00168 6267 C00152 1[13C]asparagine C4H8N2O3 HMDB00168 6267 C00152 2[13C]asparagine C4H8N2O3 HMDB00168 6267 C00152 3[13C]asparagine C4H8N2O3 HMDB00168 6267 C00152 4[13C]asparagine C4H8N2O3 HMDB00168 6267 C00152 2-Ketobutyric acid/acetoacetate C4H6O3 HMDB00005 58 C00109 HMDB0000060 6971017 C00164 2-Ketobutyric acid/acetoacetate-1 C4H6O3 HMDB00005 58 C00109 HMDB0000060 6971017 C00164 2-Ketobutyric acid/acetoacetate-2 C4H6O3 HMDB00005 58 C00109 HMDB0000060 6971017 C00164 2-Ketobutyric acid/acetoacetate-3 C4H6O3 HMDB00005 58 C00109 HMDB0000060 6971017 C00164 2-Ketobutyric acid/acetoacetate-4 C4H6O3 HMDB00005 58 C00109 HMDB0000060 6971017 C00164 5-oxoproline/L-1-Pyrroline-3-hydroxy-5-carboxylate C5H7NO3 HMDB00267 4992 C01879 HMDB01369 1059 C04281 5-oxoproline/L-1-Pyrroline-3-hydroxy-5-carboxylate-1 C5H7NO3 HMDB00267 4992 C01879 HMDB01369 1059 C04281 5-oxoproline/L-1-Pyrroline-3-hydroxy-5-carboxylate-2 C5H7NO3 HMDB00267 4992 C01879 HMDB01369 1059 C04281 5-oxoproline/L-1-Pyrroline-3-hydroxy-5-carboxylate-3 C5H7NO3 HMDB00267 4992 C01879 HMDB01369 1059 C04281 5-oxoproline/L-1-Pyrroline-3-hydroxy-5-carboxylate-4 C5H7NO3 HMDB00267 4992 C01879 HMDB01369 1059 C04281 5-oxoproline/L-1-Pyrroline-3-hydroxy-5-carboxylate-5 C5H7NO3 HMDB00267 4992 C01879 HMDB01369 1059 C04281 L-2-aminoadipate C6H11NO4 HMDB00510 469 C00956 L-2-aminoadipate-1 C6H11NO4 HMDB00510 469 C00956 L-2-aminoadipate-2 C6H11NO4 HMDB00510 469 C00956 L-2-aminoadipate-3 C6H11NO4 HMDB00510 469 C00956 L-2-aminoadipate-4 C6H11NO4 HMDB00510 469 C00956 L-2-aminoadipate-5 C6H11NO4 HMDB00510 469 C00956 L-2-aminoadipate-6 C6H11NO4 HMDB00510 469 C00956 N-acetyl-L-aspartate C6H9NO5 HMDB00812 65065 C01042 N-acetyl-L-aspartate-1 C6H9NO5 HMDB00812 65065 C01042 N-acetyl-L-aspartate-2 C6H9NO5 HMDB00812 65065 C01042 N-acetyl-L-aspartate-3 C6H9NO5 HMDB00812 65065 C01042 N-acetyl-L-aspartate-4 C6H9NO5 HMDB00812 65065 C01042 N-acetyl-L-aspartate-5 C6H9NO5 HMDB00812 65065 C01042 N-acetyl-L-aspartate-6 C6H9NO5 HMDB00812 65065 C01042 METABOLITES_END #END