#METABOLOMICS WORKBENCH wpathmasiri_20230627_102831 DATATRACK_ID:4122 STUDY_ID:ST002762 ANALYSIS_ID:AN004491 VERSION 1 CREATED_ON 06-29-2023 #PROJECT PR:PROJECT_TITLE The ECHO Cohort Exposome: First Steps using HHEAR Analysis – An Opportunity PR:PROJECT_TITLE for ALL ECHO Cohorts to Contribute Type A Samples – Untargeted Analysis PR:PROJECT_TITLE (ECHO-NOVI Cohort) PR:PROJECT_TYPE C18 Reversed-Phase Broad Spectrum Metabolomics PR:PROJECT_SUMMARY This project was funded by the NIH Environmental influences on Child Health PR:PROJECT_SUMMARY Outcomes (ECHO) Program. Untargeted metabolomics profiling data was acquired PR:PROJECT_SUMMARY from urine samples provided by 14 ECHO cohorts. PR:INSTITUTE NC HHEAR Hub PR:DEPARTMENT Untargeted Analysis PR:LABORATORY Sumner Lab PR:LAST_NAME Rushing PR:FIRST_NAME Blake PR:ADDRESS Nutrition Research Institute , University of North Carolina at Chapel Hill, 500 PR:ADDRESS Laureate Way Kannapolis, NC 28081 PR:EMAIL blake_rushing@unc.edu PR:PHONE (704) 282-9838 PR:FUNDING_SOURCE This research was supported by the Environmental influences on Child Health PR:FUNDING_SOURCE Outcomes (ECHO) program, Office of The Director, National Institutes of Health. PR:FUNDING_SOURCE The content is solely the responsibility of the authors and does not necessarily PR:FUNDING_SOURCE represent the official views of the National Institutes of Health. The ECHO-NOVI PR:FUNDING_SOURCE Cohort is supported by the following ECHO Program Collaborators: ECHO PR:FUNDING_SOURCE Coordinating Center: Duke Clinical Research Institute, Durham, North Carolina: PR:FUNDING_SOURCE Smith PB, Newby KL, Benjamin DK; U2C OD023375; ECHO Data Analysis Center: Johns PR:FUNDING_SOURCE Hopkins University Bloomberg School of Public Health, Baltimore, Maryland: PR:FUNDING_SOURCE Jacobson LP; Research Triangle Institute, Durham, North Carolina: Catellier.D PR:FUNDING_SOURCE U24 OD023382; North Carolina Human Health Exposure Analysis Resource Hub: PR:FUNDING_SOURCE Research Triangle Institute: Fennell T, University of North Carolina at Chapel PR:FUNDING_SOURCE Hill: Sumner S, University of North Carolina at Charlotte: Du X; U2C ES030857; PR:FUNDING_SOURCE Human Health Exposure Analysis Resource Coordinating Center: Westat, Inc., PR:FUNDING_SOURCE Rockville, Maryland: O’Brien B; U24 ES026539 PR:DOI http://dx.doi.org/10.21228/M8CM6S #STUDY ST:STUDY_TITLE The ECHO Cohort Exposome: First Steps using HHEAR Analysis – An Opportunity ST:STUDY_TITLE for ALL ECHO Cohorts to Contribute Type A Samples – Untargeted Analysis ST:STUDY_TITLE (ECHO-NOVI Cohort) ST:STUDY_TYPE Prospective Cohort Study ST:STUDY_SUMMARY The Neonatal Neurobehavior and Outcomes in Very Preterm Infants cohort is a ST:STUDY_SUMMARY prospective study of infants born <30 weeks postmenstrual age who through ST:STUDY_SUMMARY ECHO are being followed from age 2 to 7 to understand the neurobehavioral and ST:STUDY_SUMMARY other health outcomes of very preterm infants. The goal is to identify ST:STUDY_SUMMARY environmental factors and behaviors that can place these children at greater ST:STUDY_SUMMARY risk for or provide protection from adverse developmental outcomes. Please ST:STUDY_SUMMARY contact Carmen Marsit at carmen.j.marsit@emory.edu for questions related to the ST:STUDY_SUMMARY subject characteristics and outcomes. This research was supported by the ST:STUDY_SUMMARY Environmental influences on Child Health Outcomes (ECHO) Program, Office of The ST:STUDY_SUMMARY Director, National Institutes of Health. The content is solely the ST:STUDY_SUMMARY responsibility of the authors and does not necessarily represent the official ST:STUDY_SUMMARY views of the National Institutes of Health. ECHO-NOVI is an ECHO cohort which is ST:STUDY_SUMMARY supported by the following ECHO Program Collaborators: ECHO-NOVI Cohort Award, ST:STUDY_SUMMARY UH3OD023347 to mPIs Barry Lester, Women and Infants Hospital, Providence, RI and ST:STUDY_SUMMARY Carmen Marsit, Emory University, Atlanta, GA. ECHO Coordinating Center: Duke ST:STUDY_SUMMARY Clinical Research Institute, Durham, North Carolina: Smith PB, Newby KL, ST:STUDY_SUMMARY Benjamin DK; U2C OD023375 ECHO Data Analysis Center: Johns Hopkins University ST:STUDY_SUMMARY Bloomberg School of Public Health, Baltimore, Maryland: Jacobson LP; Research ST:STUDY_SUMMARY Triangle Institute, Durham, North Carolina: Catellier.D U24 OD023382 North ST:STUDY_SUMMARY Carolina Human Health Exposure Analysis Resource Hub: Research Triangle ST:STUDY_SUMMARY Institute: Fennell T, University of North Carolina at Chapel Hill: Sumner S, ST:STUDY_SUMMARY University of North Carolina at Charlotte: Du X; U2C ES030857 Human Health ST:STUDY_SUMMARY Exposure Analysis Resource Coordinating Center: Westat, Inc., Rockville, ST:STUDY_SUMMARY Maryland: O’Brien B; U24 ES026539 ST:INSTITUTE Emory University ST:DEPARTMENT Rollins School of Public Health ST:LAST_NAME Marsit ST:FIRST_NAME Carmen ST:ADDRESS 1518 Clifton Road, NE 8008 Claudia Nance Rollins Building Atlanta, GA 30322 ST:EMAIL carmen.j.marsit@emory.edu ST:PHONE (404) 712-8912 ST:SUBMIT_DATE 2023-06-27 #SUBJECT SU:SUBJECT_TYPE Human SU:SUBJECT_SPECIES Homo sapiens SU:TAXONOMY_ID 9606 #SUBJECT_SAMPLE_FACTORS: SUBJECT(optional)[tab]SAMPLE[tab]FACTORS(NAME:VALUE pairs separated by |)[tab]Additional sample data SUBJECT_SAMPLE_FACTORS - NOVI_B_1 Sample Type:Blank | Batch:1 Duplicate Pair=-; Analysis Order=12; RAW_FILE_NAME=NOVI_B_1 SUBJECT_SAMPLE_FACTORS - NOVI_B_2 Sample Type:Blank | Batch:1 Duplicate Pair=-; Analysis Order=26; RAW_FILE_NAME=NOVI_B_2 SUBJECT_SAMPLE_FACTORS - NOVI_B_3 Sample Type:Blank | Batch:1 Duplicate Pair=-; Analysis Order=39; RAW_FILE_NAME=NOVI_B_3 SUBJECT_SAMPLE_FACTORS - NOVI_B_4 Sample Type:Blank | Batch:1 Duplicate Pair=-; Analysis Order=53; RAW_FILE_NAME=NOVI_B_4 SUBJECT_SAMPLE_FACTORS - NOVI_B_5 Sample Type:Blank | Batch:1 Duplicate Pair=-; Analysis Order=67; RAW_FILE_NAME=NOVI_B_5 SUBJECT_SAMPLE_FACTORS - NOVI_B_6 Sample Type:Blank | Batch:1 Duplicate Pair=-; Analysis Order=81; RAW_FILE_NAME=NOVI_B_6 SUBJECT_SAMPLE_FACTORS - NOVI_B_7 Sample Type:Blank | Batch:1 Duplicate Pair=-; Analysis Order=94; RAW_FILE_NAME=NOVI_B_7 SUBJECT_SAMPLE_FACTORS - NOVI_B_8 Sample Type:Blank | Batch:1 Duplicate Pair=-; Analysis Order=108; RAW_FILE_NAME=NOVI_B_8 SUBJECT_SAMPLE_FACTORS - NOVI_B_10 Sample Type:Blank | Batch:2 Duplicate Pair=-; Analysis Order=137; RAW_FILE_NAME=NOVI_B_10 SUBJECT_SAMPLE_FACTORS - NOVI_B_11 Sample Type:Blank | Batch:2 Duplicate Pair=-; Analysis Order=150; RAW_FILE_NAME=NOVI_B_11 SUBJECT_SAMPLE_FACTORS - NOVI_B_12 Sample Type:Blank | Batch:2 Duplicate Pair=-; Analysis Order=164; RAW_FILE_NAME=NOVI_B_12 SUBJECT_SAMPLE_FACTORS - NOVI_B_13 Sample Type:Blank | Batch:2 Duplicate Pair=-; Analysis Order=178; RAW_FILE_NAME=NOVI_B_13 SUBJECT_SAMPLE_FACTORS - NOVI_B_14 Sample Type:Blank | Batch:2 Duplicate Pair=-; Analysis Order=192; RAW_FILE_NAME=NOVI_B_14 SUBJECT_SAMPLE_FACTORS - NOVI_B_15 Sample Type:Blank | Batch:2 Duplicate Pair=-; Analysis Order=205; RAW_FILE_NAME=NOVI_B_15 SUBJECT_SAMPLE_FACTORS - NOVI_B_16 Sample Type:Blank | Batch:2 Duplicate Pair=-; Analysis Order=219; RAW_FILE_NAME=NOVI_B_16 SUBJECT_SAMPLE_FACTORS - NOVI_B_9 Sample Type:Blank | Batch:2 Duplicate Pair=-; Analysis Order=123; RAW_FILE_NAME=NOVI_B_9 SUBJECT_SAMPLE_FACTORS - NOVI_B_17 Sample Type:Blank | Batch:3 Duplicate Pair=-; Analysis Order=234; RAW_FILE_NAME=NOVI_B_17 SUBJECT_SAMPLE_FACTORS - NOVI_B_18 Sample Type:Blank | Batch:3 Duplicate Pair=-; Analysis Order=248; RAW_FILE_NAME=NOVI_B_18 SUBJECT_SAMPLE_FACTORS - NOVI_B_19 Sample Type:Blank | Batch:3 Duplicate Pair=-; Analysis Order=261; RAW_FILE_NAME=NOVI_B_19 SUBJECT_SAMPLE_FACTORS - NOVI_B_20 Sample Type:Blank | Batch:3 Duplicate Pair=-; Analysis Order=275; RAW_FILE_NAME=NOVI_B_20 SUBJECT_SAMPLE_FACTORS - NOVI_B_21 Sample Type:Blank | Batch:3 Duplicate Pair=-; Analysis Order=288; RAW_FILE_NAME=NOVI_B_21 SUBJECT_SAMPLE_FACTORS - NOVI_B_22 Sample Type:Blank | Batch:3 Duplicate Pair=-; Analysis Order=303; RAW_FILE_NAME=NOVI_B_22 SUBJECT_SAMPLE_FACTORS - NOVI_B_23 Sample Type:Blank | Batch:3 Duplicate Pair=-; Analysis Order=316; RAW_FILE_NAME=NOVI_B_23 SUBJECT_SAMPLE_FACTORS - NOVI_B_24 Sample Type:Blank | Batch:3 Duplicate Pair=-; Analysis Order=330; RAW_FILE_NAME=NOVI_B_24 SUBJECT_SAMPLE_FACTORS - NOVI_B_25 Sample Type:Blank | Batch:3 Duplicate Pair=-; Analysis Order=343; RAW_FILE_NAME=NOVI_B_25 SUBJECT_SAMPLE_FACTORS - NOVI_B_26 Sample Type:Blank | Batch:3 Duplicate Pair=-; Analysis Order=357; RAW_FILE_NAME=NOVI_B_26 SUBJECT_SAMPLE_FACTORS - NOVI_B_27 Sample Type:Blank | Batch:3 Duplicate Pair=-; Analysis Order=365; RAW_FILE_NAME=NOVI_B_27 SUBJECT_SAMPLE_FACTORS - NOVI_CHEAR_U_1 Sample Type:CHEAR | Batch:1 Duplicate Pair=-; Analysis Order=14; RAW_FILE_NAME=NOVI_CHEAR_U_1 SUBJECT_SAMPLE_FACTORS - NOVI_CHEAR_U_2 Sample Type:CHEAR | Batch:1 Duplicate Pair=-; Analysis Order=41; RAW_FILE_NAME=NOVI_CHEAR_U_2 SUBJECT_SAMPLE_FACTORS - NOVI_CHEAR_U_3 Sample Type:CHEAR | Batch:1 Duplicate Pair=-; Analysis Order=69; RAW_FILE_NAME=NOVI_CHEAR_U_3 SUBJECT_SAMPLE_FACTORS - NOVI_CHEAR_U_4 Sample Type:CHEAR | Batch:1 Duplicate Pair=-; Analysis Order=96; RAW_FILE_NAME=NOVI_CHEAR_U_4 SUBJECT_SAMPLE_FACTORS - NOVI_CHEAR_U_5 Sample Type:CHEAR | Batch:2 Duplicate Pair=-; Analysis Order=125; RAW_FILE_NAME=NOVI_CHEAR_U_5 SUBJECT_SAMPLE_FACTORS - NOVI_CHEAR_U_6 Sample Type:CHEAR | Batch:2 Duplicate Pair=-; Analysis Order=152; RAW_FILE_NAME=NOVI_CHEAR_U_6 SUBJECT_SAMPLE_FACTORS - NOVI_CHEAR_U_7 Sample Type:CHEAR | Batch:2 Duplicate Pair=-; Analysis Order=180; RAW_FILE_NAME=NOVI_CHEAR_U_7 SUBJECT_SAMPLE_FACTORS - NOVI_CHEAR_U_8 Sample Type:CHEAR | Batch:2 Duplicate Pair=-; Analysis Order=207; RAW_FILE_NAME=NOVI_CHEAR_U_8 SUBJECT_SAMPLE_FACTORS - NOVI_CHEAR_U_10 Sample Type:CHEAR | Batch:3 Duplicate Pair=-; Analysis Order=263; RAW_FILE_NAME=NOVI_CHEAR_U_10 SUBJECT_SAMPLE_FACTORS - NOVI_CHEAR_U_11 Sample Type:CHEAR | Batch:3 Duplicate Pair=-; Analysis Order=290; RAW_FILE_NAME=NOVI_CHEAR_U_11 SUBJECT_SAMPLE_FACTORS - NOVI_CHEAR_U_12 Sample Type:CHEAR | Batch:3 Duplicate Pair=-; Analysis Order=318; RAW_FILE_NAME=NOVI_CHEAR_U_12 SUBJECT_SAMPLE_FACTORS - NOVI_CHEAR_U_13 Sample Type:CHEAR | Batch:3 Duplicate Pair=-; Analysis Order=345; RAW_FILE_NAME=NOVI_CHEAR_U_13 SUBJECT_SAMPLE_FACTORS - NOVI_CHEAR_U_14 Sample Type:CHEAR | Batch:3 Duplicate Pair=-; Analysis Order=367; RAW_FILE_NAME=NOVI_CHEAR_U_14 SUBJECT_SAMPLE_FACTORS - NOVI_CHEAR_U_9 Sample Type:CHEAR | Batch:3 Duplicate Pair=-; Analysis Order=236; RAW_FILE_NAME=NOVI_CHEAR_U_9 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U1_1 Sample Type:HHEAR U1 | Batch:1 Duplicate Pair=-; Analysis Order=13; RAW_FILE_NAME=NOVI_HHEAR_U1_1 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U1_2 Sample Type:HHEAR U1 | Batch:1 Duplicate Pair=-; Analysis Order=40; RAW_FILE_NAME=NOVI_HHEAR_U1_2 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U1_3 Sample Type:HHEAR U1 | Batch:1 Duplicate Pair=-; Analysis Order=68; RAW_FILE_NAME=NOVI_HHEAR_U1_3 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U1_4 Sample Type:HHEAR U1 | Batch:1 Duplicate Pair=-; Analysis Order=95; RAW_FILE_NAME=NOVI_HHEAR_U1_4 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U1_5 Sample Type:HHEAR U1 | Batch:2 Duplicate Pair=-; Analysis Order=124; RAW_FILE_NAME=NOVI_HHEAR_U1_5 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U1_6 Sample Type:HHEAR U1 | Batch:2 Duplicate Pair=-; Analysis Order=151; RAW_FILE_NAME=NOVI_HHEAR_U1_6 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U1_7 Sample Type:HHEAR U1 | Batch:2 Duplicate Pair=-; Analysis Order=179; RAW_FILE_NAME=NOVI_HHEAR_U1_7 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U1_8 Sample Type:HHEAR U1 | Batch:2 Duplicate Pair=-; Analysis Order=206; RAW_FILE_NAME=NOVI_HHEAR_U1_8 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U1_10 Sample Type:HHEAR U1 | Batch:3 Duplicate Pair=-; Analysis Order=262; RAW_FILE_NAME=NOVI_HHEAR_U1_10 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U1_11 Sample Type:HHEAR U1 | Batch:3 Duplicate Pair=-; Analysis Order=289; RAW_FILE_NAME=NOVI_HHEAR_U1_11 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U1_12 Sample Type:HHEAR U1 | Batch:3 Duplicate Pair=-; Analysis Order=317; RAW_FILE_NAME=NOVI_HHEAR_U1_12 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U1_13 Sample Type:HHEAR U1 | Batch:3 Duplicate Pair=-; Analysis Order=344; RAW_FILE_NAME=NOVI_HHEAR_U1_13 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U1_14 Sample Type:HHEAR U1 | Batch:3 Duplicate Pair=-; Analysis Order=366; RAW_FILE_NAME=NOVI_HHEAR_U1_14 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U1_9 Sample Type:HHEAR U1 | Batch:3 Duplicate Pair=-; Analysis Order=235; RAW_FILE_NAME=NOVI_HHEAR_U1_9 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U2_1 Sample Type:HHEAR U2 | Batch:1 Duplicate Pair=-; Analysis Order=27; RAW_FILE_NAME=NOVI_HHEAR_U2_1 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U2_2 Sample Type:HHEAR U2 | Batch:1 Duplicate Pair=-; Analysis Order=54; RAW_FILE_NAME=NOVI_HHEAR_U2_2 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U2_3 Sample Type:HHEAR U2 | Batch:1 Duplicate Pair=-; Analysis Order=82; RAW_FILE_NAME=NOVI_HHEAR_U2_3 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U2_4 Sample Type:HHEAR U2 | Batch:1 Duplicate Pair=-; Analysis Order=109; RAW_FILE_NAME=NOVI_HHEAR_U2_4 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U2_5 Sample Type:HHEAR U2 | Batch:2 Duplicate Pair=-; Analysis Order=138; RAW_FILE_NAME=NOVI_HHEAR_U2_5 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U2_6 Sample Type:HHEAR U2 | Batch:2 Duplicate Pair=-; Analysis Order=165; RAW_FILE_NAME=NOVI_HHEAR_U2_6 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U2_7 Sample Type:HHEAR U2 | Batch:2 Duplicate Pair=-; Analysis Order=193; RAW_FILE_NAME=NOVI_HHEAR_U2_7 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U2_8 Sample Type:HHEAR U2 | Batch:2 Duplicate Pair=-; Analysis Order=220; RAW_FILE_NAME=NOVI_HHEAR_U2_8 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U2_10 Sample Type:HHEAR U2 | Batch:3 Duplicate Pair=-; Analysis Order=276; RAW_FILE_NAME=NOVI_HHEAR_U2_10 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U2_11 Sample Type:HHEAR U2 | Batch:3 Duplicate Pair=-; Analysis Order=304; RAW_FILE_NAME=NOVI_HHEAR_U2_11 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U2_12 Sample Type:HHEAR U2 | Batch:3 Duplicate Pair=-; Analysis Order=331; RAW_FILE_NAME=NOVI_HHEAR_U2_12 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U2_13 Sample Type:HHEAR U2 | Batch:3 Duplicate Pair=-; Analysis Order=358; RAW_FILE_NAME=NOVI_HHEAR_U2_13 SUBJECT_SAMPLE_FACTORS - NOVI_HHEAR_U2_9 Sample Type:HHEAR U2 | Batch:3 Duplicate Pair=-; Analysis Order=249; RAW_FILE_NAME=NOVI_HHEAR_U2_9 SUBJECT_SAMPLE_FACTORS - NOVI_NIST_3672_1 Sample Type:NIST | Batch:1 Duplicate Pair=-; Analysis Order=1; RAW_FILE_NAME=NOVI_NIST_3672_1 SUBJECT_SAMPLE_FACTORS - NOVI_NIST_3672_2 Sample Type:NIST | Batch:1 Duplicate Pair=-; Analysis Order=56; RAW_FILE_NAME=NOVI_NIST_3672_2 SUBJECT_SAMPLE_FACTORS - NOVI_NIST_3672_3 Sample Type:NIST | Batch:1 Duplicate Pair=-; Analysis Order=111; RAW_FILE_NAME=NOVI_NIST_3672_3 SUBJECT_SAMPLE_FACTORS - NOVI_NIST_3672_4 Sample Type:NIST | Batch:2 Duplicate Pair=-; Analysis Order=112; RAW_FILE_NAME=NOVI_NIST_3672_4 SUBJECT_SAMPLE_FACTORS - NOVI_NIST_3672_5 Sample Type:NIST | Batch:2 Duplicate Pair=-; Analysis Order=167; RAW_FILE_NAME=NOVI_NIST_3672_5 SUBJECT_SAMPLE_FACTORS - NOVI_NIST_3672_6 Sample Type:NIST | Batch:2 Duplicate Pair=-; Analysis Order=222; RAW_FILE_NAME=NOVI_NIST_3672_6 SUBJECT_SAMPLE_FACTORS - NOVI_NIST_3672_7 Sample Type:NIST | Batch:3 Duplicate Pair=-; Analysis Order=223; RAW_FILE_NAME=NOVI_NIST_3672_7 SUBJECT_SAMPLE_FACTORS - NOVI_NIST_3672_8 Sample Type:NIST | Batch:3 Duplicate Pair=-; Analysis Order=292; RAW_FILE_NAME=NOVI_NIST_3672_8 SUBJECT_SAMPLE_FACTORS - NOVI_NIST_3672_9 Sample Type:NIST | Batch:3 Duplicate Pair=-; Analysis Order=369; RAW_FILE_NAME=NOVI_NIST_3672_9 SUBJECT_SAMPLE_FACTORS - NOVI_SP_1 Sample Type:Study pool | Batch:1 Duplicate Pair=-; Analysis Order=15; RAW_FILE_NAME=NOVI_SP_1 SUBJECT_SAMPLE_FACTORS - NOVI_SP_2 Sample Type:Study pool | Batch:1 Duplicate Pair=-; Analysis Order=28; RAW_FILE_NAME=NOVI_SP_2 SUBJECT_SAMPLE_FACTORS - NOVI_SP_3 Sample Type:Study pool | Batch:1 Duplicate Pair=-; Analysis Order=42; RAW_FILE_NAME=NOVI_SP_3 SUBJECT_SAMPLE_FACTORS - NOVI_SP_4 Sample Type:Study pool | Batch:1 Duplicate Pair=-; Analysis Order=55; RAW_FILE_NAME=NOVI_SP_4 SUBJECT_SAMPLE_FACTORS - NOVI_SP_5 Sample Type:Study pool | Batch:1 Duplicate Pair=-; Analysis Order=70; RAW_FILE_NAME=NOVI_SP_5 SUBJECT_SAMPLE_FACTORS - NOVI_SP_6 Sample Type:Study pool | Batch:1 Duplicate Pair=-; Analysis Order=83; RAW_FILE_NAME=NOVI_SP_6 SUBJECT_SAMPLE_FACTORS - NOVI_SP_7 Sample Type:Study pool | Batch:1 Duplicate Pair=-; Analysis Order=97; RAW_FILE_NAME=NOVI_SP_7 SUBJECT_SAMPLE_FACTORS - NOVI_SP_8 Sample Type:Study pool | Batch:1 Duplicate Pair=-; Analysis Order=110; RAW_FILE_NAME=NOVI_SP_8 SUBJECT_SAMPLE_FACTORS - NOVI_SP_10 Sample Type:Study pool | Batch:2 Duplicate Pair=-; Analysis Order=139; RAW_FILE_NAME=NOVI_SP_10 SUBJECT_SAMPLE_FACTORS - NOVI_SP_11 Sample Type:Study pool | Batch:2 Duplicate Pair=-; Analysis Order=153; RAW_FILE_NAME=NOVI_SP_11 SUBJECT_SAMPLE_FACTORS - NOVI_SP_12 Sample Type:Study pool | Batch:2 Duplicate Pair=-; Analysis Order=166; RAW_FILE_NAME=NOVI_SP_12 SUBJECT_SAMPLE_FACTORS - NOVI_SP_13 Sample Type:Study pool | Batch:2 Duplicate Pair=-; Analysis Order=181; RAW_FILE_NAME=NOVI_SP_13 SUBJECT_SAMPLE_FACTORS - NOVI_SP_14 Sample Type:Study pool | Batch:2 Duplicate Pair=-; Analysis Order=194; RAW_FILE_NAME=NOVI_SP_14 SUBJECT_SAMPLE_FACTORS - NOVI_SP_15 Sample Type:Study pool | Batch:2 Duplicate Pair=-; Analysis Order=208; RAW_FILE_NAME=NOVI_SP_15 SUBJECT_SAMPLE_FACTORS - NOVI_SP_16 Sample Type:Study pool | Batch:2 Duplicate Pair=-; Analysis Order=221; RAW_FILE_NAME=NOVI_SP_16 SUBJECT_SAMPLE_FACTORS - NOVI_SP_9 Sample Type:Study pool | Batch:2 Duplicate Pair=-; Analysis Order=126; RAW_FILE_NAME=NOVI_SP_9 SUBJECT_SAMPLE_FACTORS - NOVI_SP_17 Sample Type:Study pool | Batch:3 Duplicate Pair=-; Analysis Order=237; RAW_FILE_NAME=NOVI_SP_17 SUBJECT_SAMPLE_FACTORS - NOVI_SP_18 Sample Type:Study pool | Batch:3 Duplicate Pair=-; Analysis Order=250; RAW_FILE_NAME=NOVI_SP_18 SUBJECT_SAMPLE_FACTORS - NOVI_SP_19 Sample Type:Study pool | Batch:3 Duplicate Pair=-; Analysis Order=264; RAW_FILE_NAME=NOVI_SP_19 SUBJECT_SAMPLE_FACTORS - NOVI_SP_20 Sample Type:Study pool | Batch:3 Duplicate Pair=-; Analysis Order=277; RAW_FILE_NAME=NOVI_SP_20 SUBJECT_SAMPLE_FACTORS - NOVI_SP_21 Sample Type:Study pool | Batch:3 Duplicate Pair=-; Analysis Order=291; RAW_FILE_NAME=NOVI_SP_21 SUBJECT_SAMPLE_FACTORS - NOVI_SP_22 Sample Type:Study pool | Batch:3 Duplicate Pair=-; Analysis Order=305; RAW_FILE_NAME=NOVI_SP_22 SUBJECT_SAMPLE_FACTORS - NOVI_SP_23 Sample Type:Study pool | Batch:3 Duplicate Pair=-; Analysis Order=319; RAW_FILE_NAME=NOVI_SP_23 SUBJECT_SAMPLE_FACTORS - NOVI_SP_24 Sample Type:Study pool | Batch:3 Duplicate Pair=-; Analysis Order=332; RAW_FILE_NAME=NOVI_SP_24 SUBJECT_SAMPLE_FACTORS - NOVI_SP_25 Sample Type:Study pool | Batch:3 Duplicate Pair=-; Analysis Order=346; RAW_FILE_NAME=NOVI_SP_25 SUBJECT_SAMPLE_FACTORS - NOVI_SP_26 Sample Type:Study pool | Batch:3 Duplicate Pair=-; Analysis Order=359; RAW_FILE_NAME=NOVI_SP_26 SUBJECT_SAMPLE_FACTORS - NOVI_SP_27 Sample Type:Study pool | Batch:3 Duplicate Pair=-; Analysis Order=368; RAW_FILE_NAME=NOVI_SP_27 SUBJECT_SAMPLE_FACTORS EM-478R9-U-00-12001 NOVI_S_1 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=2; RAW_FILE_NAME=NOVI_S_1 SUBJECT_SAMPLE_FACTORS EM-48LG1-U-00-12001 NOVI_S_10 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=11; RAW_FILE_NAME=NOVI_S_10 SUBJECT_SAMPLE_FACTORS EM-483F8-U-00-12001 NOVI_S_11 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=16; RAW_FILE_NAME=NOVI_S_11 SUBJECT_SAMPLE_FACTORS EM-5CXX6-U-00-12001 NOVI_S_12 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=17; RAW_FILE_NAME=NOVI_S_12 SUBJECT_SAMPLE_FACTORS EM-5CYD9-U-00-12001 NOVI_S_13 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=18; RAW_FILE_NAME=NOVI_S_13 SUBJECT_SAMPLE_FACTORS EM-481B9-U-00-12001 NOVI_S_14 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=19; RAW_FILE_NAME=NOVI_S_14 SUBJECT_SAMPLE_FACTORS EM-48JF5-U-00-12001 NOVI_S_15 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=20; RAW_FILE_NAME=NOVI_S_15 SUBJECT_SAMPLE_FACTORS EM-47C36-U-00-12001 NOVI_S_16 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=21; RAW_FILE_NAME=NOVI_S_16 SUBJECT_SAMPLE_FACTORS EM-48256-U-00-12001 NOVI_S_17 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=22; RAW_FILE_NAME=NOVI_S_17 SUBJECT_SAMPLE_FACTORS EM-5D0C0-U-00-12001 NOVI_S_18 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=23; RAW_FILE_NAME=NOVI_S_18 SUBJECT_SAMPLE_FACTORS EM-5CZ51-U-00-12001 NOVI_S_19 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=24; RAW_FILE_NAME=NOVI_S_19 SUBJECT_SAMPLE_FACTORS EM-48306-U-00-12001 NOVI_S_2 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=3; RAW_FILE_NAME=NOVI_S_2 SUBJECT_SAMPLE_FACTORS EM-47WG2-U-00-12001 NOVI_S_20 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=25; RAW_FILE_NAME=NOVI_S_20 SUBJECT_SAMPLE_FACTORS EM-47NQ9-U-00-12001 NOVI_S_21 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=29; RAW_FILE_NAME=NOVI_S_21 SUBJECT_SAMPLE_FACTORS EM-47JL4-U-00-12001 NOVI_S_22 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=30; RAW_FILE_NAME=NOVI_S_22 SUBJECT_SAMPLE_FACTORS EM-48918-U-00-12001 NOVI_S_23 Sample Type:Study sample | Batch:1 Duplicate Pair=A; Analysis Order=31; RAW_FILE_NAME=NOVI_S_23 SUBJECT_SAMPLE_FACTORS EM-48A85-U-00-12001 NOVI_S_24 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=32; RAW_FILE_NAME=NOVI_S_24 SUBJECT_SAMPLE_FACTORS EM-47MB3-U-00-12001 NOVI_S_25 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=33; RAW_FILE_NAME=NOVI_S_25 SUBJECT_SAMPLE_FACTORS EM-5CRD6-U-00-12001 NOVI_S_26 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=34; RAW_FILE_NAME=NOVI_S_26 SUBJECT_SAMPLE_FACTORS EM-47A38-U-00-12001 NOVI_S_27 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=35; RAW_FILE_NAME=NOVI_S_27 SUBJECT_SAMPLE_FACTORS EM-48EL7-U-00-12001 NOVI_S_28 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=36; RAW_FILE_NAME=NOVI_S_28 SUBJECT_SAMPLE_FACTORS EM-5D191-U-00-12001 NOVI_S_29 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=37; RAW_FILE_NAME=NOVI_S_29 SUBJECT_SAMPLE_FACTORS EM-47W85-U-00-12001 NOVI_S_3 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=4; RAW_FILE_NAME=NOVI_S_3 SUBJECT_SAMPLE_FACTORS EM-47PT0-U-00-12001 NOVI_S_30 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=38; RAW_FILE_NAME=NOVI_S_30 SUBJECT_SAMPLE_FACTORS EM-47YL9-U-00-12001 NOVI_S_31 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=43; RAW_FILE_NAME=NOVI_S_31 SUBJECT_SAMPLE_FACTORS EM-48090-U-00-12001 NOVI_S_32 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=44; RAW_FILE_NAME=NOVI_S_32 SUBJECT_SAMPLE_FACTORS EM-47928-U-00-12001 NOVI_S_33 Sample Type:Study sample | Batch:1 Duplicate Pair=B; Analysis Order=45; RAW_FILE_NAME=NOVI_S_33 SUBJECT_SAMPLE_FACTORS EM-48025-U-00-12001 NOVI_S_34 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=46; RAW_FILE_NAME=NOVI_S_34 SUBJECT_SAMPLE_FACTORS EM-47852-U-00-12001 NOVI_S_35 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=47; RAW_FILE_NAME=NOVI_S_35 SUBJECT_SAMPLE_FACTORS EM-5D0L0-U-00-12001 NOVI_S_36 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=48; RAW_FILE_NAME=NOVI_S_36 SUBJECT_SAMPLE_FACTORS EM-47CM9-U-00-12001 NOVI_S_37 Sample Type:Study sample | Batch:1 Duplicate Pair=C; Analysis Order=49; RAW_FILE_NAME=NOVI_S_37 SUBJECT_SAMPLE_FACTORS EM-47W51-U-00-12001 NOVI_S_38 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=50; RAW_FILE_NAME=NOVI_S_38 SUBJECT_SAMPLE_FACTORS EM-47V11-U-00-12001 NOVI_S_39 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=51; RAW_FILE_NAME=NOVI_S_39 SUBJECT_SAMPLE_FACTORS EM-48PV4-U-00-12001 NOVI_S_4 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=5; RAW_FILE_NAME=NOVI_S_4 SUBJECT_SAMPLE_FACTORS EM-47BH1-U-00-12001 NOVI_S_40 Sample Type:Study sample | Batch:1 Duplicate Pair.D Analysis Order=52; RAW_FILE_NAME=NOVI_S_40 SUBJECT_SAMPLE_FACTORS EM-47HA0-U-00-12001 NOVI_S_41 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=57; RAW_FILE_NAME=NOVI_S_41 SUBJECT_SAMPLE_FACTORS EM-477Y4-U-00-12001 NOVI_S_42 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=58; RAW_FILE_NAME=NOVI_S_42 SUBJECT_SAMPLE_FACTORS EM-47M02-U-00-12001 NOVI_S_43 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=59; RAW_FILE_NAME=NOVI_S_43 SUBJECT_SAMPLE_FACTORS EM-487A5-U-00-12001 NOVI_S_44 Sample Type:Study sample | Batch:1 Duplicate Pair=E; Analysis Order=60; RAW_FILE_NAME=NOVI_S_44 SUBJECT_SAMPLE_FACTORS EM-47QT9-U-00-12001 NOVI_S_45 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=61; RAW_FILE_NAME=NOVI_S_45 SUBJECT_SAMPLE_FACTORS EM-47GF0-U-00-12001 NOVI_S_46 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=62; RAW_FILE_NAME=NOVI_S_46 SUBJECT_SAMPLE_FACTORS EM-484D1-U-00-12001 NOVI_S_47 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=63; RAW_FILE_NAME=NOVI_S_47 SUBJECT_SAMPLE_FACTORS EM-482V4-U-00-12001 NOVI_S_48 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=64; RAW_FILE_NAME=NOVI_S_48 SUBJECT_SAMPLE_FACTORS EM-488V8-U-00-12001 NOVI_S_49 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=65; RAW_FILE_NAME=NOVI_S_49 SUBJECT_SAMPLE_FACTORS EM-478Y3-U-00-12001 NOVI_S_5 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=6; RAW_FILE_NAME=NOVI_S_5 SUBJECT_SAMPLE_FACTORS EM-48H39-U-00-12001 NOVI_S_50 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=66; RAW_FILE_NAME=NOVI_S_50 SUBJECT_SAMPLE_FACTORS EM-5CSA2-U-00-12001 NOVI_S_51 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=71; RAW_FILE_NAME=NOVI_S_51 SUBJECT_SAMPLE_FACTORS EM-47TD1-U-00-12001 NOVI_S_52 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=72; RAW_FILE_NAME=NOVI_S_52 SUBJECT_SAMPLE_FACTORS EM-48LT2-U-00-12001 NOVI_S_53 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=73; RAW_FILE_NAME=NOVI_S_53 SUBJECT_SAMPLE_FACTORS EM-47JR1-U-00-12001 NOVI_S_54 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=74; RAW_FILE_NAME=NOVI_S_54 SUBJECT_SAMPLE_FACTORS EM-47A53-U-00-12001 NOVI_S_55 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=75; RAW_FILE_NAME=NOVI_S_55 SUBJECT_SAMPLE_FACTORS EM-47C02-U-00-12001 NOVI_S_56 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=76; RAW_FILE_NAME=NOVI_S_56 SUBJECT_SAMPLE_FACTORS EM-478A6-U-00-12001 NOVI_S_57 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=77; RAW_FILE_NAME=NOVI_S_57 SUBJECT_SAMPLE_FACTORS EM-48967-U-00-12001 NOVI_S_58 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=78; RAW_FILE_NAME=NOVI_S_58 SUBJECT_SAMPLE_FACTORS EM-48C18-U-00-12001 NOVI_S_59 Sample Type:Study sample | Batch:1 Duplicate Pair=F; Analysis Order=79; RAW_FILE_NAME=NOVI_S_59 SUBJECT_SAMPLE_FACTORS EM-5CWU4-U-00-12001 NOVI_S_6 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=7; RAW_FILE_NAME=NOVI_S_6 SUBJECT_SAMPLE_FACTORS EM-47WE6-U-00-12001 NOVI_S_60 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=80; RAW_FILE_NAME=NOVI_S_60 SUBJECT_SAMPLE_FACTORS EM-486U2-U-00-12001 NOVI_S_61 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=84; RAW_FILE_NAME=NOVI_S_61 SUBJECT_SAMPLE_FACTORS EM-47J54-U-00-12001 NOVI_S_62 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=85; RAW_FILE_NAME=NOVI_S_62 SUBJECT_SAMPLE_FACTORS EM-479D8-U-00-12001 NOVI_S_63 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=86; RAW_FILE_NAME=NOVI_S_63 SUBJECT_SAMPLE_FACTORS EM-48892-U-00-12001 NOVI_S_64 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=87; RAW_FILE_NAME=NOVI_S_64 SUBJECT_SAMPLE_FACTORS EM-48GD2-U-00-12001 NOVI_S_65 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=88; RAW_FILE_NAME=NOVI_S_65 SUBJECT_SAMPLE_FACTORS EM-47Z66-U-00-12001 NOVI_S_66 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=89; RAW_FILE_NAME=NOVI_S_66 SUBJECT_SAMPLE_FACTORS EM-484G5-U-00-12001 NOVI_S_67 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=90; RAW_FILE_NAME=NOVI_S_67 SUBJECT_SAMPLE_FACTORS EM-48CK1-U-00-12001 NOVI_S_68 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=91; RAW_FILE_NAME=NOVI_S_68 SUBJECT_SAMPLE_FACTORS EM-48PK8-U-00-12001 NOVI_S_69 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=92; RAW_FILE_NAME=NOVI_S_69 SUBJECT_SAMPLE_FACTORS EM-5CTA1-U-00-12001 NOVI_S_7 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=8; RAW_FILE_NAME=NOVI_S_7 SUBJECT_SAMPLE_FACTORS EM-5CWL4-U-00-12001 NOVI_S_70 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=93; RAW_FILE_NAME=NOVI_S_70 SUBJECT_SAMPLE_FACTORS EM-483W1-U-00-12001 NOVI_S_71 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=98; RAW_FILE_NAME=NOVI_S_71 SUBJECT_SAMPLE_FACTORS EM-48314-U-00-12001 NOVI_S_72 Sample Type:Study sample | Batch:1 Duplicate Pair=G; Analysis Order=99; RAW_FILE_NAME=NOVI_S_72 SUBJECT_SAMPLE_FACTORS EM-48HU4-U-00-12001 NOVI_S_73 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=100; RAW_FILE_NAME=NOVI_S_73 SUBJECT_SAMPLE_FACTORS EM-47JA8-U-00-12001 NOVI_S_74 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=101; RAW_FILE_NAME=NOVI_S_74 SUBJECT_SAMPLE_FACTORS EM-48LU0-U-00-12001 NOVI_S_75 Sample Type:Study sample | Batch:1 Duplicate Pair=H; Analysis Order=102; RAW_FILE_NAME=NOVI_S_75 SUBJECT_SAMPLE_FACTORS EM-48678-U-00-12001 NOVI_S_76 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=103; RAW_FILE_NAME=NOVI_S_76 SUBJECT_SAMPLE_FACTORS EM-489R6-U-00-12001 NOVI_S_77 Sample Type:Study sample | Batch:1 Duplicate Pair=I; Analysis Order=104; RAW_FILE_NAME=NOVI_S_77 SUBJECT_SAMPLE_FACTORS EM-478V0-U-00-12001 NOVI_S_78 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=105; RAW_FILE_NAME=NOVI_S_78 SUBJECT_SAMPLE_FACTORS EM-48J11-U-00-12001 NOVI_S_79 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=106; RAW_FILE_NAME=NOVI_S_79 SUBJECT_SAMPLE_FACTORS EM-489U9-U-00-12001 NOVI_S_8 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=9; RAW_FILE_NAME=NOVI_S_8 SUBJECT_SAMPLE_FACTORS EM-48652-U-00-12001 NOVI_S_80 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=107; RAW_FILE_NAME=NOVI_S_80 SUBJECT_SAMPLE_FACTORS EM-47QH6-U-00-12001 NOVI_S_9 Sample Type:Study sample | Batch:1 Duplicate Pair=-; Analysis Order=10; RAW_FILE_NAME=NOVI_S_9 SUBJECT_SAMPLE_FACTORS EM-5CQV8-U-00-12001 NOVI_S_100 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=136; RAW_FILE_NAME=NOVI_S_100 SUBJECT_SAMPLE_FACTORS EM-47VE7-U-00-12001 NOVI_S_101 Sample Type:Study sample | Batch:2 Duplicate Pair=G; Analysis Order=140; RAW_FILE_NAME=NOVI_S_101 SUBJECT_SAMPLE_FACTORS EM-48645-U-00-12001 NOVI_S_102 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=141; RAW_FILE_NAME=NOVI_S_102 SUBJECT_SAMPLE_FACTORS EM-48371-U-00-12001 NOVI_S_103 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=142; RAW_FILE_NAME=NOVI_S_103 SUBJECT_SAMPLE_FACTORS EM-5CRU9-U-00-12001 NOVI_S_104 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=143; RAW_FILE_NAME=NOVI_S_104 SUBJECT_SAMPLE_FACTORS EM-47QN2-U-00-12001 NOVI_S_105 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=144; RAW_FILE_NAME=NOVI_S_105 SUBJECT_SAMPLE_FACTORS EM-489V7-U-00-12001 NOVI_S_106 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=145; RAW_FILE_NAME=NOVI_S_106 SUBJECT_SAMPLE_FACTORS EM-47FD5-U-00-12001 NOVI_S_107 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=146; RAW_FILE_NAME=NOVI_S_107 SUBJECT_SAMPLE_FACTORS EM-48HM2-U-00-12001 NOVI_S_108 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=147; RAW_FILE_NAME=NOVI_S_108 SUBJECT_SAMPLE_FACTORS EM-5CVX8-U-00-12001 NOVI_S_109 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=148; RAW_FILE_NAME=NOVI_S_109 SUBJECT_SAMPLE_FACTORS EM-48DG9-U-00-12001 NOVI_S_110 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=149; RAW_FILE_NAME=NOVI_S_110 SUBJECT_SAMPLE_FACTORS EM-47RH5-U-00-12001 NOVI_S_111 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=154; RAW_FILE_NAME=NOVI_S_111 SUBJECT_SAMPLE_FACTORS EM-480N3-U-00-12001 NOVI_S_112 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=155; RAW_FILE_NAME=NOVI_S_112 SUBJECT_SAMPLE_FACTORS EM-5CNQ2-U-00-12001 NOVI_S_113 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=156; RAW_FILE_NAME=NOVI_S_113 SUBJECT_SAMPLE_FACTORS EM-47Y59-U-00-12001 NOVI_S_114 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=157; RAW_FILE_NAME=NOVI_S_114 SUBJECT_SAMPLE_FACTORS EM-5CQL0-U-00-12001 NOVI_S_115 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=158; RAW_FILE_NAME=NOVI_S_115 SUBJECT_SAMPLE_FACTORS EM-47803-U-00-12001 NOVI_S_116 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=159; RAW_FILE_NAME=NOVI_S_116 SUBJECT_SAMPLE_FACTORS EM-481U7-U-00-12001 NOVI_S_117 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=160; RAW_FILE_NAME=NOVI_S_117 SUBJECT_SAMPLE_FACTORS EM-5CP93-U-00-12001 NOVI_S_118 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=161; RAW_FILE_NAME=NOVI_S_118 SUBJECT_SAMPLE_FACTORS EM-48SS7-U-00-12001 NOVI_S_119 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=162; RAW_FILE_NAME=NOVI_S_119 SUBJECT_SAMPLE_FACTORS EM-485V1-U-00-12001 NOVI_S_120 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=163; RAW_FILE_NAME=NOVI_S_120 SUBJECT_SAMPLE_FACTORS EM-47BQ1-U-00-12001 NOVI_S_121 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=168; RAW_FILE_NAME=NOVI_S_121 SUBJECT_SAMPLE_FACTORS EM-48751-U-00-12001 NOVI_S_122 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=169; RAW_FILE_NAME=NOVI_S_122 SUBJECT_SAMPLE_FACTORS EM-47837-U-00-12001 NOVI_S_123 Sample Type:Study sample | Batch:2 Duplicate Pair=J; Analysis Order=170; RAW_FILE_NAME=NOVI_S_123 SUBJECT_SAMPLE_FACTORS EM-5CSJ2-U-00-12001 NOVI_S_124 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=171; RAW_FILE_NAME=NOVI_S_124 SUBJECT_SAMPLE_FACTORS EM-5CNJ7-U-00-12001 NOVI_S_125 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=172; RAW_FILE_NAME=NOVI_S_125 SUBJECT_SAMPLE_FACTORS EM-47TG5-U-00-12001 NOVI_S_126 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=173; RAW_FILE_NAME=NOVI_S_126 SUBJECT_SAMPLE_FACTORS EM-5CP85-U-00-12001 NOVI_S_127 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=174; RAW_FILE_NAME=NOVI_S_127 SUBJECT_SAMPLE_FACTORS EM-47K04-U-00-12001 NOVI_S_128 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=175; RAW_FILE_NAME=NOVI_S_128 SUBJECT_SAMPLE_FACTORS EM-47P25-U-00-12001 NOVI_S_129 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=176; RAW_FILE_NAME=NOVI_S_129 SUBJECT_SAMPLE_FACTORS EM-47BB4-U-00-12001 NOVI_S_130 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=177; RAW_FILE_NAME=NOVI_S_130 SUBJECT_SAMPLE_FACTORS EM-47N68-U-00-12001 NOVI_S_131 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=182; RAW_FILE_NAME=NOVI_S_131 SUBJECT_SAMPLE_FACTORS EM-5CY86-U-00-12001 NOVI_S_132 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=183; RAW_FILE_NAME=NOVI_S_132 SUBJECT_SAMPLE_FACTORS EM-48P80-U-00-12001 NOVI_S_133 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=184; RAW_FILE_NAME=NOVI_S_133 SUBJECT_SAMPLE_FACTORS EM-48S38-U-00-12001 NOVI_S_134 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=185; RAW_FILE_NAME=NOVI_S_134 SUBJECT_SAMPLE_FACTORS EM-47JS8-U-00-12001 NOVI_S_135 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=186; RAW_FILE_NAME=NOVI_S_135 SUBJECT_SAMPLE_FACTORS EM-47MK3-U-00-12001 NOVI_S_136 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=187; RAW_FILE_NAME=NOVI_S_136 SUBJECT_SAMPLE_FACTORS EM-47QF0-U-00-12001 NOVI_S_137 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=188; RAW_FILE_NAME=NOVI_S_137 SUBJECT_SAMPLE_FACTORS EM-48199-U-00-12001 NOVI_S_138 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=189; RAW_FILE_NAME=NOVI_S_138 SUBJECT_SAMPLE_FACTORS EM-47H07-U-00-12001 NOVI_S_139 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=190; RAW_FILE_NAME=NOVI_S_139 SUBJECT_SAMPLE_FACTORS EM-47GC7-U-00-12001 NOVI_S_140 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=191; RAW_FILE_NAME=NOVI_S_140 SUBJECT_SAMPLE_FACTORS EM-480Y9-U-00-12001 NOVI_S_141 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=195; RAW_FILE_NAME=NOVI_S_141 SUBJECT_SAMPLE_FACTORS EM-47KB5-U-00-12001 NOVI_S_142 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=196; RAW_FILE_NAME=NOVI_S_142 SUBJECT_SAMPLE_FACTORS EM-47H64-U-00-12001 NOVI_S_143 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=197; RAW_FILE_NAME=NOVI_S_143 SUBJECT_SAMPLE_FACTORS EM-48L43-U-00-12001 NOVI_S_144 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=198; RAW_FILE_NAME=NOVI_S_144 SUBJECT_SAMPLE_FACTORS EM-47G81-U-00-12001 NOVI_S_145 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=199; RAW_FILE_NAME=NOVI_S_145 SUBJECT_SAMPLE_FACTORS EM-5CZV9-U-00-12001 NOVI_S_146 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=200; RAW_FILE_NAME=NOVI_S_146 SUBJECT_SAMPLE_FACTORS EM-48835-U-00-12001 NOVI_S_147 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=201; RAW_FILE_NAME=NOVI_S_147 SUBJECT_SAMPLE_FACTORS EM-483M3-U-00-12001 NOVI_S_148 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=202; RAW_FILE_NAME=NOVI_S_148 SUBJECT_SAMPLE_FACTORS EM-47D19-U-00-12001 NOVI_S_149 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=203; RAW_FILE_NAME=NOVI_S_149 SUBJECT_SAMPLE_FACTORS EM-5CTB9-U-00-12001 NOVI_S_150 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=204; RAW_FILE_NAME=NOVI_S_150 SUBJECT_SAMPLE_FACTORS EM-47CY2-U-00-12001 NOVI_S_151 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=209; RAW_FILE_NAME=NOVI_S_151 SUBJECT_SAMPLE_FACTORS EM-477T5-U-00-12001 NOVI_S_152 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=210; RAW_FILE_NAME=NOVI_S_152 SUBJECT_SAMPLE_FACTORS EM-47XC0-U-00-12001 NOVI_S_153 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=211; RAW_FILE_NAME=NOVI_S_153 SUBJECT_SAMPLE_FACTORS EM-47B52-U-00-12001 NOVI_S_154 Sample Type:Study sample | Batch:2 Duplicate Pair=J; Analysis Order=212; RAW_FILE_NAME=NOVI_S_154 SUBJECT_SAMPLE_FACTORS EM-5D0G1-U-00-12001 NOVI_S_155 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=213; RAW_FILE_NAME=NOVI_S_155 SUBJECT_SAMPLE_FACTORS EM-47FS2-U-00-12001 NOVI_S_156 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=214; RAW_FILE_NAME=NOVI_S_156 SUBJECT_SAMPLE_FACTORS EM-47KM1-U-00-12001 NOVI_S_157 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=215; RAW_FILE_NAME=NOVI_S_157 SUBJECT_SAMPLE_FACTORS EM-47B60-U-00-12001 NOVI_S_158 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=216; RAW_FILE_NAME=NOVI_S_158 SUBJECT_SAMPLE_FACTORS EM-48JD9-U-00-12001 NOVI_S_159 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=217; RAW_FILE_NAME=NOVI_S_159 SUBJECT_SAMPLE_FACTORS EM-5CUU6-U-00-12001 NOVI_S_160 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=218; RAW_FILE_NAME=NOVI_S_160 SUBJECT_SAMPLE_FACTORS EM-47QC7-U-00-12001 NOVI_S_81 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=113; RAW_FILE_NAME=NOVI_S_81 SUBJECT_SAMPLE_FACTORS EM-47UG4-U-00-12001 NOVI_S_82 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=114; RAW_FILE_NAME=NOVI_S_82 SUBJECT_SAMPLE_FACTORS EM-5CT24-U-00-12001 NOVI_S_83 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=115; RAW_FILE_NAME=NOVI_S_83 SUBJECT_SAMPLE_FACTORS EM-47EC9-U-00-12001 NOVI_S_84 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=116; RAW_FILE_NAME=NOVI_S_84 SUBJECT_SAMPLE_FACTORS EM-47EG0-U-00-12001 NOVI_S_85 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=117; RAW_FILE_NAME=NOVI_S_85 SUBJECT_SAMPLE_FACTORS EM-48LH9-U-00-12001 NOVI_S_86 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=118; RAW_FILE_NAME=NOVI_S_86 SUBJECT_SAMPLE_FACTORS EM-482K8-U-00-12001 NOVI_S_87 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=119; RAW_FILE_NAME=NOVI_S_87 SUBJECT_SAMPLE_FACTORS EM-5CTH6-U-00-12001 NOVI_S_88 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=120; RAW_FILE_NAME=NOVI_S_88 SUBJECT_SAMPLE_FACTORS EM-48HE9-U-00-12001 NOVI_S_89 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=121; RAW_FILE_NAME=NOVI_S_89 SUBJECT_SAMPLE_FACTORS EM-48DE3-U-00-12001 NOVI_S_90 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=122; RAW_FILE_NAME=NOVI_S_90 SUBJECT_SAMPLE_FACTORS EM-47FW4-U-00-12001 NOVI_S_91 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=127; RAW_FILE_NAME=NOVI_S_91 SUBJECT_SAMPLE_FACTORS EM-482U6-U-00-12001 NOVI_S_92 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=128; RAW_FILE_NAME=NOVI_S_92 SUBJECT_SAMPLE_FACTORS EM-48CL9-U-00-12001 NOVI_S_93 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=129; RAW_FILE_NAME=NOVI_S_93 SUBJECT_SAMPLE_FACTORS EM-47BY3-U-00-12001 NOVI_S_94 Sample Type:Study sample | Batch:2 Duplicate Pair=H; Analysis Order=130; RAW_FILE_NAME=NOVI_S_94 SUBJECT_SAMPLE_FACTORS EM-48595-U-00-12001 NOVI_S_95 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=131; RAW_FILE_NAME=NOVI_S_95 SUBJECT_SAMPLE_FACTORS EM-47ZB0-U-00-12001 NOVI_S_96 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=132; RAW_FILE_NAME=NOVI_S_96 SUBJECT_SAMPLE_FACTORS EM-47QQ6-U-00-12001 NOVI_S_97 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=133; RAW_FILE_NAME=NOVI_S_97 SUBJECT_SAMPLE_FACTORS EM-5CPR8-U-00-12001 NOVI_S_98 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=134; RAW_FILE_NAME=NOVI_S_98 SUBJECT_SAMPLE_FACTORS EM-47A87-U-00-12001 NOVI_S_99 Sample Type:Study sample | Batch:2 Duplicate Pair=-; Analysis Order=135; RAW_FILE_NAME=NOVI_S_99 SUBJECT_SAMPLE_FACTORS EM-5CSC8-U-00-12001 NOVI_S_161 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=224; RAW_FILE_NAME=NOVI_S_161 SUBJECT_SAMPLE_FACTORS EM-48LN5-U-00-12001 NOVI_S_162 Sample Type:Study sample | Batch:3 Duplicate Pair=A; Analysis Order=225; RAW_FILE_NAME=NOVI_S_162 SUBJECT_SAMPLE_FACTORS EM-5CYJ6-U-00-12001 NOVI_S_163 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=226; RAW_FILE_NAME=NOVI_S_163 SUBJECT_SAMPLE_FACTORS EM-48NN3-U-00-12001 NOVI_S_164 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=227; RAW_FILE_NAME=NOVI_S_164 SUBJECT_SAMPLE_FACTORS EM-487D8-U-00-12001 NOVI_S_165 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=228; RAW_FILE_NAME=NOVI_S_165 SUBJECT_SAMPLE_FACTORS EM-5CUY7-U-00-12001 NOVI_S_166 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=229; RAW_FILE_NAME=NOVI_S_166 SUBJECT_SAMPLE_FACTORS EM-47CX4-U-00-12001 NOVI_S_167 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=230; RAW_FILE_NAME=NOVI_S_167 SUBJECT_SAMPLE_FACTORS EM-5CS90-U-00-12001 NOVI_S_168 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=231; RAW_FILE_NAME=NOVI_S_168 SUBJECT_SAMPLE_FACTORS EM-48B01-U-00-12001 NOVI_S_169 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=232; RAW_FILE_NAME=NOVI_S_169 SUBJECT_SAMPLE_FACTORS EM-489H8-U-00-12001 NOVI_S_170 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=233; RAW_FILE_NAME=NOVI_S_170 SUBJECT_SAMPLE_FACTORS EM-47JD1-U-00-12001 NOVI_S_171 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=238; RAW_FILE_NAME=NOVI_S_171 SUBJECT_SAMPLE_FACTORS EM-5CS66-U-00-12001 NOVI_S_172 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=239; RAW_FILE_NAME=NOVI_S_172 SUBJECT_SAMPLE_FACTORS EM-48BY1-U-00-12001 NOVI_S_173 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=240; RAW_FILE_NAME=NOVI_S_173 SUBJECT_SAMPLE_FACTORS EM-47P66-U-00-12001 NOVI_S_174 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=241; RAW_FILE_NAME=NOVI_S_174 SUBJECT_SAMPLE_FACTORS EM-47G08-U-00-12001 NOVI_S_175 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=242; RAW_FILE_NAME=NOVI_S_175 SUBJECT_SAMPLE_FACTORS EM-5CNP4-U-00-12001 NOVI_S_176 Sample Type:Study sample | Batch:3 Duplicate Pair=K; Analysis Order=243; RAW_FILE_NAME=NOVI_S_176 SUBJECT_SAMPLE_FACTORS EM-48801-U-00-12001 NOVI_S_177 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=244; RAW_FILE_NAME=NOVI_S_177 SUBJECT_SAMPLE_FACTORS EM-47QK9-U-00-12001 NOVI_S_178 Sample Type:Study sample | Batch:3 Duplicate Pair=C; Analysis Order=245; RAW_FILE_NAME=NOVI_S_178 SUBJECT_SAMPLE_FACTORS EM-5CRK1-U-00-12001 NOVI_S_179 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=246; RAW_FILE_NAME=NOVI_S_179 SUBJECT_SAMPLE_FACTORS EM-5CX61-U-00-12001 NOVI_S_180 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=247; RAW_FILE_NAME=NOVI_S_180 SUBJECT_SAMPLE_FACTORS EM-5CRF2-U-00-12001 NOVI_S_181 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=251; RAW_FILE_NAME=NOVI_S_181 SUBJECT_SAMPLE_FACTORS EM-48HF7-U-00-12001 NOVI_S_182 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=252; RAW_FILE_NAME=NOVI_S_182 SUBJECT_SAMPLE_FACTORS EM-47LX5-U-00-12001 NOVI_S_183 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=253; RAW_FILE_NAME=NOVI_S_183 SUBJECT_SAMPLE_FACTORS EM-48FM4-U-00-12001 NOVI_S_184 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=254; RAW_FILE_NAME=NOVI_S_184 SUBJECT_SAMPLE_FACTORS EM-48ET9-U-00-12001 NOVI_S_185 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=255; RAW_FILE_NAME=NOVI_S_185 SUBJECT_SAMPLE_FACTORS EM-48488-U-00-12001 NOVI_S_186 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=256; RAW_FILE_NAME=NOVI_S_186 SUBJECT_SAMPLE_FACTORS EM-487K3-U-00-12001 NOVI_S_187 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=257; RAW_FILE_NAME=NOVI_S_187 SUBJECT_SAMPLE_FACTORS EM-48HK6-U-00-12001 NOVI_S_188 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=258; RAW_FILE_NAME=NOVI_S_188 SUBJECT_SAMPLE_FACTORS EM-47K79-U-00-12001 NOVI_S_189 Sample Type:Study sample | Batch:3 Duplicate Pair=L; Analysis Order=259; RAW_FILE_NAME=NOVI_S_189 SUBJECT_SAMPLE_FACTORS EM-47YF2-U-00-12001 NOVI_S_190 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=260; RAW_FILE_NAME=NOVI_S_190 SUBJECT_SAMPLE_FACTORS EM-48CG0-U-00-12001 NOVI_S_191 Sample Type:Study sample | Batch:3 Duplicate Pair=F; Analysis Order=265; RAW_FILE_NAME=NOVI_S_191 SUBJECT_SAMPLE_FACTORS EM-47ZM6-U-00-12001 NOVI_S_192 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=266; RAW_FILE_NAME=NOVI_S_192 SUBJECT_SAMPLE_FACTORS EM-47HU6-U-00-12001 NOVI_S_193 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=267; RAW_FILE_NAME=NOVI_S_193 SUBJECT_SAMPLE_FACTORS EM-48JT4-U-00-12001 NOVI_S_194 Sample Type:Study sample | Batch:3 Duplicate Pair.D Analysis Order=268; RAW_FILE_NAME=NOVI_S_194 SUBJECT_SAMPLE_FACTORS EM-48LR7-U-00-12001 NOVI_S_195 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=269; RAW_FILE_NAME=NOVI_S_195 SUBJECT_SAMPLE_FACTORS EM-5CNE8-U-00-12001 NOVI_S_196 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=270; RAW_FILE_NAME=NOVI_S_196 SUBJECT_SAMPLE_FACTORS EM-48FW2-U-00-12001 NOVI_S_197 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=271; RAW_FILE_NAME=NOVI_S_197 SUBJECT_SAMPLE_FACTORS EM-48CA3-U-00-12001 NOVI_S_198 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=272; RAW_FILE_NAME=NOVI_S_198 SUBJECT_SAMPLE_FACTORS EM-47CE6-U-00-12001 NOVI_S_199 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=273; RAW_FILE_NAME=NOVI_S_199 SUBJECT_SAMPLE_FACTORS EM-48J78-U-00-12001 NOVI_S_200 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=274; RAW_FILE_NAME=NOVI_S_200 SUBJECT_SAMPLE_FACTORS EM-48HD1-U-00-12001 NOVI_S_201 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=278; RAW_FILE_NAME=NOVI_S_201 SUBJECT_SAMPLE_FACTORS EM-48R05-U-00-12001 NOVI_S_202 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=279; RAW_FILE_NAME=NOVI_S_202 SUBJECT_SAMPLE_FACTORS EM-48J94-U-00-12001 NOVI_S_203 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=280; RAW_FILE_NAME=NOVI_S_203 SUBJECT_SAMPLE_FACTORS EM-480B0-U-00-12001 NOVI_S_204 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=281; RAW_FILE_NAME=NOVI_S_204 SUBJECT_SAMPLE_FACTORS EM-48MF2-U-00-12001 NOVI_S_205 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=282; RAW_FILE_NAME=NOVI_S_205 SUBJECT_SAMPLE_FACTORS EM-487S5-U-00-12001 NOVI_S_206 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=283; RAW_FILE_NAME=NOVI_S_206 SUBJECT_SAMPLE_FACTORS EM-5CR34-U-00-12001 NOVI_S_207 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=284; RAW_FILE_NAME=NOVI_S_207 SUBJECT_SAMPLE_FACTORS EM-48FN1-U-00-12001 NOVI_S_208 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=285; RAW_FILE_NAME=NOVI_S_208 SUBJECT_SAMPLE_FACTORS EM-488N5-U-00-12001 NOVI_S_209 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=286; RAW_FILE_NAME=NOVI_S_209 SUBJECT_SAMPLE_FACTORS EM-5CUH5-U-00-12001 NOVI_S_210 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=287; RAW_FILE_NAME=NOVI_S_210 SUBJECT_SAMPLE_FACTORS EM-48EA1-U-00-12001 NOVI_S_211 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=293; RAW_FILE_NAME=NOVI_S_211 SUBJECT_SAMPLE_FACTORS EM-47FT0-U-00-12001 NOVI_S_212 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=294; RAW_FILE_NAME=NOVI_S_212 SUBJECT_SAMPLE_FACTORS EM-47JH3-U-00-12001 NOVI_S_213 Sample Type:Study sample | Batch:3 Duplicate Pair=K; Analysis Order=295; RAW_FILE_NAME=NOVI_S_213 SUBJECT_SAMPLE_FACTORS EM-47EP0-U-00-12001 NOVI_S_214 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=296; RAW_FILE_NAME=NOVI_S_214 SUBJECT_SAMPLE_FACTORS EM-48G55-U-00-12001 NOVI_S_215 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=297; RAW_FILE_NAME=NOVI_S_215 SUBJECT_SAMPLE_FACTORS EM-5CNM1-U-00-12001 NOVI_S_216 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=298; RAW_FILE_NAME=NOVI_S_216 SUBJECT_SAMPLE_FACTORS EM-47TN9-U-00-12001 NOVI_S_217 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=299; RAW_FILE_NAME=NOVI_S_217 SUBJECT_SAMPLE_FACTORS EM-5CRR6-U-00-12001 NOVI_S_218 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=300; RAW_FILE_NAME=NOVI_S_218 SUBJECT_SAMPLE_FACTORS EM-47DJ4-U-00-12001 NOVI_S_219 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=301; RAW_FILE_NAME=NOVI_S_219 SUBJECT_SAMPLE_FACTORS EM-48JP3-U-00-12001 NOVI_S_220 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=302; RAW_FILE_NAME=NOVI_S_220 SUBJECT_SAMPLE_FACTORS EM-5CNT5-U-00-12001 NOVI_S_221 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=306; RAW_FILE_NAME=NOVI_S_221 SUBJECT_SAMPLE_FACTORS EM-5CR75-U-00-12001 NOVI_S_222 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=307; RAW_FILE_NAME=NOVI_S_222 SUBJECT_SAMPLE_FACTORS EM-5CT32-U-00-12001 NOVI_S_223 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=308; RAW_FILE_NAME=NOVI_S_223 SUBJECT_SAMPLE_FACTORS EM-480A2-U-00-12001 NOVI_S_224 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=309; RAW_FILE_NAME=NOVI_S_224 SUBJECT_SAMPLE_FACTORS EM-481S1-U-00-12001 NOVI_S_225 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=310; RAW_FILE_NAME=NOVI_S_225 SUBJECT_SAMPLE_FACTORS EM-47YG0-U-00-12001 NOVI_S_226 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=311; RAW_FILE_NAME=NOVI_S_226 SUBJECT_SAMPLE_FACTORS EM-5CRN4-U-00-12001 NOVI_S_227 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=312; RAW_FILE_NAME=NOVI_S_227 SUBJECT_SAMPLE_FACTORS EM-479L1-U-00-12001 NOVI_S_228 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=313; RAW_FILE_NAME=NOVI_S_228 SUBJECT_SAMPLE_FACTORS EM-47DS4-U-00-12001 NOVI_S_229 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=314; RAW_FILE_NAME=NOVI_S_229 SUBJECT_SAMPLE_FACTORS EM-47J47-U-00-12001 NOVI_S_230 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=315; RAW_FILE_NAME=NOVI_S_230 SUBJECT_SAMPLE_FACTORS EM-48934-U-00-12001 NOVI_S_231 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=320; RAW_FILE_NAME=NOVI_S_231 SUBJECT_SAMPLE_FACTORS EM-48FC6-U-00-12001 NOVI_S_232 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=321; RAW_FILE_NAME=NOVI_S_232 SUBJECT_SAMPLE_FACTORS EM-48PH5-U-00-12001 NOVI_S_233 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=322; RAW_FILE_NAME=NOVI_S_233 SUBJECT_SAMPLE_FACTORS EM-47FV6-U-00-12001 NOVI_S_234 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=323; RAW_FILE_NAME=NOVI_S_234 SUBJECT_SAMPLE_FACTORS EM-48RP5-U-00-12001 NOVI_S_235 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=324; RAW_FILE_NAME=NOVI_S_235 SUBJECT_SAMPLE_FACTORS EM-48QR2-U-00-12001 NOVI_S_236 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=325; RAW_FILE_NAME=NOVI_S_236 SUBJECT_SAMPLE_FACTORS EM-47MM9-U-00-12001 NOVI_S_237 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=326; RAW_FILE_NAME=NOVI_S_237 SUBJECT_SAMPLE_FACTORS EM-48C42-U-00-12001 NOVI_S_238 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=327; RAW_FILE_NAME=NOVI_S_238 SUBJECT_SAMPLE_FACTORS EM-47MX4-U-00-12001 NOVI_S_239 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=328; RAW_FILE_NAME=NOVI_S_239 SUBJECT_SAMPLE_FACTORS EM-5CNU3-U-00-12001 NOVI_S_240 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=329; RAW_FILE_NAME=NOVI_S_240 SUBJECT_SAMPLE_FACTORS EM-5CQE5-U-00-12001 NOVI_S_241 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=333; RAW_FILE_NAME=NOVI_S_241 SUBJECT_SAMPLE_FACTORS EM-477P4-U-00-12001 NOVI_S_242 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=334; RAW_FILE_NAME=NOVI_S_242 SUBJECT_SAMPLE_FACTORS EM-48PF9-U-00-12001 NOVI_S_243 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=335; RAW_FILE_NAME=NOVI_S_243 SUBJECT_SAMPLE_FACTORS EM-47XA4-U-00-12001 NOVI_S_244 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=336; RAW_FILE_NAME=NOVI_S_244 SUBJECT_SAMPLE_FACTORS EM-47W93-U-00-12001 NOVI_S_245 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=337; RAW_FILE_NAME=NOVI_S_245 SUBJECT_SAMPLE_FACTORS EM-48MK1-U-00-12001 NOVI_S_246 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=338; RAW_FILE_NAME=NOVI_S_246 SUBJECT_SAMPLE_FACTORS EM-47GS1-U-00-12001 NOVI_S_247 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=339; RAW_FILE_NAME=NOVI_S_247 SUBJECT_SAMPLE_FACTORS EM-47QD4-U-00-12001 NOVI_S_248 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=340; RAW_FILE_NAME=NOVI_S_248 SUBJECT_SAMPLE_FACTORS EM-47UT5-U-00-12001 NOVI_S_249 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=341; RAW_FILE_NAME=NOVI_S_249 SUBJECT_SAMPLE_FACTORS EM-48JU2-U-00-12001 NOVI_S_250 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=342; RAW_FILE_NAME=NOVI_S_250 SUBJECT_SAMPLE_FACTORS EM-5CWX7-U-00-12001 NOVI_S_251 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=347; RAW_FILE_NAME=NOVI_S_251 SUBJECT_SAMPLE_FACTORS EM-48AD8-U-00-12001 NOVI_S_252 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=348; RAW_FILE_NAME=NOVI_S_252 SUBJECT_SAMPLE_FACTORS EM-47P41-U-00-12001 NOVI_S_253 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=349; RAW_FILE_NAME=NOVI_S_253 SUBJECT_SAMPLE_FACTORS EM-47Q24-U-00-12001 NOVI_S_254 Sample Type:Study sample | Batch:3 Duplicate Pair=L; Analysis Order=350; RAW_FILE_NAME=NOVI_S_254 SUBJECT_SAMPLE_FACTORS EM-47FR5-U-00-12001 NOVI_S_255 Sample Type:Study sample | Batch:3 Duplicate Pair=E; Analysis Order=351; RAW_FILE_NAME=NOVI_S_255 SUBJECT_SAMPLE_FACTORS EM-47HP7-U-00-12001 NOVI_S_256 Sample Type:Study sample | Batch:3 Duplicate Pair=B; Analysis Order=352; RAW_FILE_NAME=NOVI_S_256 SUBJECT_SAMPLE_FACTORS EM-48JV0-U-00-12001 NOVI_S_257 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=353; RAW_FILE_NAME=NOVI_S_257 SUBJECT_SAMPLE_FACTORS EM-47UE8-U-00-12001 NOVI_S_258 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=354; RAW_FILE_NAME=NOVI_S_258 SUBJECT_SAMPLE_FACTORS EM-48C00-U-00-12001 NOVI_S_259 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=355; RAW_FILE_NAME=NOVI_S_259 SUBJECT_SAMPLE_FACTORS EM-48G71-U-00-12001 NOVI_S_260 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=356; RAW_FILE_NAME=NOVI_S_260 SUBJECT_SAMPLE_FACTORS EM-48KC1-U-00-12001 NOVI_S_261 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=360; RAW_FILE_NAME=NOVI_S_261 SUBJECT_SAMPLE_FACTORS EM-48HY5-U-00-12001 NOVI_S_262 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=361; RAW_FILE_NAME=NOVI_S_262 SUBJECT_SAMPLE_FACTORS EM-47UB5-U-00-12001 NOVI_S_263 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=362; RAW_FILE_NAME=NOVI_S_263 SUBJECT_SAMPLE_FACTORS EM-48RU4-U-00-12001 NOVI_S_264 Sample Type:Study sample | Batch:3 Duplicate Pair=-; Analysis Order=363; RAW_FILE_NAME=NOVI_S_264 SUBJECT_SAMPLE_FACTORS EM-48SG4-U-00-12001 NOVI_S_265 Sample Type:Study sample | Batch:3 Duplicate Pair=I; Analysis Order=364; RAW_FILE_NAME=NOVI_S_265 #COLLECTION CO:COLLECTION_SUMMARY N/A CO:SAMPLE_TYPE Urine CO:STORAGE_CONDITIONS -80℃ #TREATMENT TR:TREATMENT_SUMMARY N/A #SAMPLEPREP SP:SAMPLEPREP_SUMMARY Study samples were shipped from the Emory University Rollins School of Public SP:SAMPLEPREP_SUMMARY Health to the NC HHEAR Hub on dry ice. The NC HHEAR Hub thawed and transferred SP:SAMPLEPREP_SUMMARY 50 µL of the study samples to a new set of tubes and used them for the SP:SAMPLEPREP_SUMMARY analysis. An additional 10 µL was taken from the original study sample and SP:SAMPLEPREP_SUMMARY transferred to another tube to make the total study pool for this project, and SP:SAMPLEPREP_SUMMARY then distributed with 50 µL per aliquot, used as quality control study pools SP:SAMPLEPREP_SUMMARY (QC study pools) throughout the whole analysis. All sample aliquots (50 µL SP:SAMPLEPREP_SUMMARY each) and QC study pools (50 µL each) were stored at -80° C until the day of SP:SAMPLEPREP_SUMMARY sample preparation. HHEAR Urine Pool 1 (50 µL each), HHEAR Urine Pool 2 (50 µL SP:SAMPLEPREP_SUMMARY each), CHEAR reference urine (50 µL each) and NIST urine (SRM 3672) reference SP:SAMPLEPREP_SUMMARY material (50 µL each) were provided by the NC HHEAR Hub. LC-MS grade water (50 SP:SAMPLEPREP_SUMMARY µL) was used as blanks. All samples were thawed at 4°C overnight before the SP:SAMPLEPREP_SUMMARY preparation. Samples, including study samples, study pool samples, HHEAR SP:SAMPLEPREP_SUMMARY reference urine, CHEAR reference urine, NIST reference urine, and blanks were SP:SAMPLEPREP_SUMMARY mixed with 400 µL methanol containing 500 ng/mL tryptophan-d5 as internal SP:SAMPLEPREP_SUMMARY standard and vortexed by a multiple tube vortex mixer for 2 min at 5000 rpm at SP:SAMPLEPREP_SUMMARY room temperature. All samples were centrifuged at 16,000 rcf for 10 min at 4°C. SP:SAMPLEPREP_SUMMARY The supernatant (350 µL) was transferred into a pre-labeled 2.0 mL Lo-bind SP:SAMPLEPREP_SUMMARY Eppendorf tube, dried by a SpeedVac overnight, and stored at -80° C. For SP:SAMPLEPREP_SUMMARY immediate analysis, 100 µL of water-methanol solution (95:5, v/v) was used to SP:SAMPLEPREP_SUMMARY reconstitute the dried extracts. Samples were thoroughly mixed on a multiple SP:SAMPLEPREP_SUMMARY tube vortex mixer for 10 min at 5000 rpm at room temperature and then SP:SAMPLEPREP_SUMMARY centrifuged at 4°C for 10 min at 16,000 rcf. The supernatant was transferred to SP:SAMPLEPREP_SUMMARY pre-labeled autosampler vials for data acquisition by LC-MS. SP:PROCESSING_STORAGE_CONDITIONS 4℃ SP:EXTRACTION_METHOD Vortex with methanol containing 500ng/ml tryptophan-d5 as internal standard SP:EXTRACT_STORAGE -80℃ SP:SAMPLE_RESUSPENSION Water-Methanol (95:5, v/v) SP:SAMPLE_SPIKING Tryptophan-d5 stock solution at 500 ng/mL #CHROMATOGRAPHY CH:CHROMATOGRAPHY_SUMMARY Reversed phase CH:INSTRUMENT_NAME Thermo Vanquish CH:COLUMN_NAME Waters ACQUITY UPLC HSS T3 (100 x 2.1mm,1.8um) CH:COLUMN_PRESSURE 6000-10000 psi CH:COLUMN_TEMPERATURE 50 ℃ CH:FLOW_GRADIENT Time(min) Flow Rate %A %B Curve 1. 0 0.4 99.0 1.0 5 2. 1.00 0.4 99.0 1.0 5 3. CH:FLOW_GRADIENT 16.00 0.4 1.0 99.0 5 4. 19.00 0.4 1.0 99.0 5 5. 19.50 0.4 99.0 1.0 5 6. 22.00 CH:FLOW_GRADIENT 0.4 99.0 1.0 5 CH:FLOW_RATE 0.4 mL/min CH:INJECTION_TEMPERATURE 8 ℃ CH:INTERNAL_STANDARD Tryptophan-d5 CH:SOLVENT_A 100% water; 0.1% formic acid CH:SOLVENT_B 100% methanol; 0.1% formic acid CH:ANALYTICAL_TIME 22 min CH:WEAK_WASH_SOLVENT_NAME 10% methanol/90% water; 0.1% formic acid CH:STRONG_WASH_SOLVENT_NAME 75% 2-Propanol/25% Water; 0.1% formic acid CH:CHROMATOGRAPHY_TYPE Reversed phase #ANALYSIS AN:ANALYSIS_TYPE MS AN:ACQUISITION_DATE 1/3/2023-1/14/2023 AN:SOFTWARE_VERSION Xcalibur 4.1.31.9 AN:DETECTOR_TYPE Orbitrap AN:DATA_FORMAT Profile #MS MS:INSTRUMENT_NAME Thermo Q Exactive HF-X Orbitrap MS:INSTRUMENT_TYPE Orbitrap MS:MS_TYPE ESI MS:MS_COMMENTS Instrument: Thermo Q Exactive HFx Software: Xcalibur 4.1.31.9 for data MS:MS_COMMENTS acquisition; Progenesis QI 2.4 for data preprocessing MS:ION_MODE POSITIVE MS:CAPILLARY_TEMPERATURE 320 °C MS:CAPILLARY_VOLTAGE 3.5 KV MS:COLLISION_ENERGY 20-45, ramp MS:COLLISION_GAS N2 MS:FRAGMENTATION_METHOD CID MS:ION_SPRAY_VOLTAGE 3.5kV MS:IONIZATION ES+ MS:MASS_ACCURACY 5 ppm MS:DATAFORMAT Profile MS:DESOLVATION_GAS_FLOW 55 MS:DESOLVATION_TEMPERATURE 400 ℃ MS:MS_RESULTS_FILE ST002762_AN004491_Results.txt UNITS:Normalized intensity Has m/z:Yes Has RT:Yes RT units:Minutes #END