{
"METABOLOMICS WORKBENCH":{"STUDY_ID":"ST001200","ANALYSIS_ID":"AN001996","VERSION":"1","CREATED_ON":"June 19, 2019, 12:51 pm"},

"PROJECT":{"PROJECT_TITLE":"Biological Responses to Tobacco Smoke Exposure in III Children: Inflammatory Processes and the Oral Microbiome","PROJECT_TYPE":"NIH/NIEHS 1U2CES026560-01","PROJECT_SUMMARY":"This project evaluates the biological response to overall tobacco smoke (OTS) exposure among pediatric emergency patients enrolled in a randomized-controlled intervention trial aimed at reducing secondhand smoke exposure. The effects of OTS as measured by salivary continine on salivary metabolic profiles are measured by untargeted high resolution metabolomics, comparing higher and lower levels of OTS.","INSTITUTE":"Emory University","DEPARTMENT":"School of Medicine","LABORATORY":"Clinical Biomarkers Laboratory","LAST_NAME":"Tran","FIRST_NAME":"ViLinh","ADDRESS":"NA","EMAIL":"vtran6@emory.edu","PHONE":"(404) 727 5027","FUNDING_SOURCE":"NIEHS ES026560"},

"STUDY":{"STUDY_TITLE":"Biological Responses to Tobacco Smoke Exposure in III Children: Inflammatory Processes and the Oral Microbiome","STUDY_SUMMARY":"This project evaluates the biological response to overall tobacco smoke (OTS) exposure among pediatric emergency patients enrolled in a randomized-controlled intervention trial aimed at reducing secondhand smoke exposure. The effects of OTS as measured by salivary continine on salivary metabolic profiles are measured by untargeted high resolution metabolomics, comparing higher and lower levels of OTS.","INSTITUTE":"Emory University","DEPARTMENT":"School of Medicine","LABORATORY":"Clincal Biomarkers Laboratory","LAST_NAME":"Uppal","FIRST_NAME":"Karan","ADDRESS":"NA","EMAIL":"kuppal2@emory.edu","PHONE":"(404) 727 5027","TOTAL_SUBJECTS":"284","STUDY_COMMENTS":"Both CHEAR pooled saliva samples and Clinical Biomarker Laboratory pooled plasma samples were used","CHEAR_STUDY":"2017-1762"},

"SUBJECT":{"SUBJECT_TYPE":"Human","SUBJECT_SPECIES":"Homo sapiens","TAXONOMY_ID":"9606","AGE_OR_AGE_RANGE":"Ages 0 to 17 years"},
"SUBJECT_SAMPLE_FACTORS":[
{
"Subject ID":"Quality Control",
"Sample ID":"NIST SRM 1950_1a",
"Factors":{"Plasma":"Plasma"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Plasma","Raw files":"VT_190122_M371_002,VT_190122_M371_004,VT_190122_M371_006"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"Q-Std Plasma pool_1a_1",
"Factors":{"Plasma":"Plasma"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Plasma","Raw files":"VT_190122_M371_008,VT_190122_M371_010,VT_190122_M371_012"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"Q-Std Plasma pool_1b_1",
"Factors":{"Plasma":"Plasma"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Plasma","Raw files":"VT_190122_M371_014,VT_190122_M371_016,VT_190122_M371_018"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"salivapool_1a_1",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_020,VT_190122_M371_022,VT_190122_M371_024"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"salivapool_1b_1",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_026,VT_190122_M371_028,VT_190122_M371_030"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GBF3-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_032,VT_190122_M371_034,VT_190122_M371_036"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GBG1-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_038,VT_190122_M371_040,VT_190122_M371_042"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GBH9-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_044,VT_190122_M371_046,VT_190122_M371_048"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GBL0-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_050,VT_190122_M371_052,VT_190122_M371_054"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GBN5-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_056,VT_190122_M371_058,VT_190122_M371_060"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GBP1-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_062,VT_190122_M371_064,VT_190122_M371_066"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GBQ9-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_068,VT_190122_M371_070,VT_190122_M371_072"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GBR7-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_074,VT_190122_M371_076,VT_190122_M371_078"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GBT2-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_080,VT_190122_M371_082,VT_190122_M371_084"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GBX3-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_086,VT_190122_M371_088,VT_190122_M371_090"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GBY1-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_092,VT_190122_M371_094,VT_190122_M371_096"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GC18-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_098,VT_190122_M371_100,VT_190122_M371_102"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GC26-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_104,VT_190122_M371_106,VT_190122_M371_108"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GC59-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_110,VT_190122_M371_112,VT_190122_M371_114"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GC75-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_116,VT_190122_M371_118,VT_190122_M371_120"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GC83-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_122,VT_190122_M371_124,VT_190122_M371_126"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GCB1-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_128,VT_190122_M371_130,VT_190122_M371_132"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GCF2-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_134,VT_190122_M371_136,VT_190122_M371_138"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GCL9-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_140,VT_190122_M371_142,VT_190122_M371_144"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GCM7-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_146,VT_190122_M371_148,VT_190122_M371_150"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"Q-Std Plasma pool_1c_1",
"Factors":{"Plasma":"Plasma"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Plasma","Raw files":"VT_190122_M371_152,VT_190122_M371_154,VT_190122_M371_156"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"Q-Std Plasma pool_1d_1",
"Factors":{"Plasma":"Plasma"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Plasma","Raw files":"VT_190122_M371_158,VT_190122_M371_160,VT_190122_M371_162"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"salivapool_1c_1",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_164,VT_190122_M371_166,VT_190122_M371_168"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"salivapool_1d_1",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_170,VT_190122_M371_172,VT_190122_M371_174"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GCN4-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_176,VT_190122_M371_178,VT_190122_M371_180"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GCP0-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_182,VT_190122_M371_184,VT_190122_M371_186"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GCQ8-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_188,VT_190122_M371_190,VT_190122_M371_192"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GD25-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_194,VT_190122_M371_196,VT_190122_M371_198"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GD33-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_200,VT_190122_M371_202,VT_190122_M371_204"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GD41-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_206,VT_190122_M371_208,VT_190122_M371_210"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GD58-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_212,VT_190122_M371_214,VT_190122_M371_216"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GD66-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_218,VT_190122_M371_220,VT_190122_M371_222"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GD74-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_224,VT_190122_M371_226,VT_190122_M371_228"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GDA2-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_230,VT_190122_M371_232,VT_190122_M371_234"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GDB0-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_236,VT_190122_M371_238,VT_190122_M371_240"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GDE3-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_242,VT_190122_M371_244,VT_190122_M371_246"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GDF1-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_248,VT_190122_M371_250,VT_190122_M371_252"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-XALJ8-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_254,VT_190122_M371_256,VT_190122_M371_258"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GDG9-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_260,VT_190122_M371_262,VT_190122_M371_264"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GDH7-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_266,VT_190122_M371_268,VT_190122_M371_270"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GDJ2-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_272,VT_190122_M371_274,VT_190122_M371_276"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GDM6-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_278,VT_190122_M371_280,VT_190122_M371_282"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GDP9-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_284,VT_190122_M371_286,VT_190122_M371_288"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GDQ7-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_290,VT_190122_M371_292,VT_190122_M371_294"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"Q-Std Plasma pool_1e_1",
"Factors":{"Plasma":"Plasma"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Plasma","Raw files":"VT_190122_M371_296,VT_190122_M371_298,VT_190122_M371_300"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"Q-Std Plasma pool_1f_1",
"Factors":{"Plasma":"Plasma"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Plasma","Raw files":"VT_190122_M371_302,VT_190122_M371_304,VT_190122_M371_306"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"salivapool_1e_1",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_308,VT_190122_M371_310,VT_190122_M371_312"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"salivapool_1f_1",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190122","Batch":"1","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190122_M371_314,VT_190122_M371_316,VT_190122_M371_318"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"Q-Std Plasma pool_2a_1",
"Factors":{"Plasma":"Plasma"},
"Additional sample data":{"Date Analyzed":"190123","Batch":"2","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Plasma","Raw files":"VT_190123_M371_002,VT_190123_M371_004,VT_190123_M371_006"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"Q-Std Plasma pool_2b_1",
"Factors":{"Plasma":"Plasma"},
"Additional sample data":{"Date Analyzed":"190123","Batch":"2","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Plasma","Raw files":"VT_190123_M371_008,VT_190123_M371_010,VT_190123_M371_012"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"salivapool_2a_1",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190123","Batch":"2","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190123_M371_014,VT_190123_M371_016,VT_190123_M371_018"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"salivapool_2b_1",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190123","Batch":"2","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190123_M371_020,VT_190123_M371_022,VT_190123_M371_024"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GDR5-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190123","Batch":"2","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190123_M371_026,VT_190123_M371_028,VT_190123_M371_030"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GE16-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190123","Batch":"2","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190123_M371_032,VT_190123_M371_034,VT_190123_M371_036"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GE24-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190123","Batch":"2","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190123_M371_038,VT_190123_M371_040,VT_190123_M371_042"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GE40-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190123","Batch":"2","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190123_M371_044,VT_190123_M371_046,VT_190123_M371_048"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GE65-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190123","Batch":"2","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190123_M371_050,VT_190123_M371_052,VT_190123_M371_054"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GE73-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190123","Batch":"2","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190123_M371_056,VT_190123_M371_058,VT_190123_M371_060"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GEB9-SL-01_2",
"Factors":{"Plasma":"Saliva"},
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GEC7-SL-01_2",
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"Additional sample data":{"Date Analyzed":"190123","Batch":"2","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190123_M371_068,VT_190123_M371_070,VT_190123_M371_072"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GEE2-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GEF0-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GEK9-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-JWM67-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GEL7-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-G2T98-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Quality Control",
"Sample ID":"Q-Std Plasma pool_2c_1",
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},
{
"Subject ID":"Quality Control",
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},
{
"Subject ID":"Quality Control",
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},
{
"Subject ID":"Quality Control",
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},
{
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},
{
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
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},
{
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},
{
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},
{
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},
{
"Subject ID":"Quality Control",
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"Additional sample data":{"Date Analyzed":"190124","Batch":"3","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Plasma","Raw files":"VT_190124_M371_002,VT_190124_M371_004,VT_190124_M371_006"}
},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GGN0-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
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},
{
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},
{
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
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"Sample ID":"C-1GGY6-SL-01_2",
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},
{
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
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},
{
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},
{
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
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},
{
"Subject ID":"Quality Control",
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},
{
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},
{
"Subject ID":"Quality Control",
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},
{
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"Sample ID":"salivapool_3d_1",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GHA8-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GHF7-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GHG5-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GHK6-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GHL4-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GHM2-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GHR1-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GHS8-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GHT6-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
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},
{
"Subject ID":"Quality Control",
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},
{
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},
{
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},
{
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},
{
"Subject ID":"Quality Control",
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},
{
"Subject ID":"Quality Control",
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},
{
"Subject ID":"Quality Control",
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Quality Control",
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},
{
"Subject ID":"Quality Control",
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},
{
"Subject ID":"Quality Control",
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},
{
"Subject ID":"Quality Control",
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GL76-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190125","Batch":"4","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190125_M371_284,VT_190125_M371_286,VT_190125_M371_288"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"Q-Std Plasma pool_4e_1",
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},
{
"Subject ID":"Quality Control",
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},
{
"Subject ID":"Quality Control",
"Sample ID":"salivapool_4e_1",
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},
{
"Subject ID":"Quality Control",
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},
{
"Subject ID":"Quality Control",
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"Additional sample data":{"Date Analyzed":"190126","Batch":"5","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Plasma","Raw files":"VT_190126_M371_002,VT_190126_M371_004,VT_190126_M371_006"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"Q-Std Plasma pool_5b_1",
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},
{
"Subject ID":"Quality Control",
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},
{
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GL92-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GLA4-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GLD7-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GLS4-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GLT2-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GMC9-SL-01_2",
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},
{
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
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},
{
"Subject ID":"Quality Control",
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},
{
"Subject ID":"Quality Control",
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},
{
"Subject ID":"Quality Control",
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},
{
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},
{
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"Sample ID":"C-1GMP0-SL-01_2",
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},
{
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},
{
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"Sample ID":"C-1GMR6-SL-01_2",
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},
{
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"Sample ID":"C-1GMV7-SL-01_2",
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},
{
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GN17-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GN25-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
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},
{
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GN74-SL-01_2",
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},
{
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GN90-SL-01_2",
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},
{
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"Sample ID":"C-1GNE3-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GNL8-SL-01_2",
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},
{
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"Sample ID":"C-1GNM6-SL-01_2",
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GNN3-SL-01_2",
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},
{
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"Sample ID":"C-1GNU8-SL-01_2",
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},
{
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"Sample ID":"C-1GNV6-SL-01_2",
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},
{
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"Sample ID":"C-1GP07-SL-01_2",
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},
{
"Subject ID":"Quality Control",
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},
{
"Subject ID":"Quality Control",
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},
{
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},
{
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},
{
"Subject ID":"Quality Control",
"Sample ID":"Q-Std Plasma pool_6a_1",
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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"Sample ID":"C-1GPD3-SL-01_2",
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},
{
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},
{
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},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GPK8-SL-01_2",
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},
{
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"Sample ID":"C-1GPM4-SL-01_2",
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"Additional sample data":{"Date Analyzed":"190127","Batch":"6","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190127_M371_068,VT_190127_M371_070,VT_190127_M371_072"}
},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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},
{
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"Sample ID":"salivapool_7c_1",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_152,VT_190128_M371_154,VT_190128_M371_156"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"salivapool_7d_1",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_158,VT_190128_M371_160,VT_190128_M371_162"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GT03-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_164,VT_190128_M371_166,VT_190128_M371_168"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GT60-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_170,VT_190128_M371_172,VT_190128_M371_174"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GT86-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_176,VT_190128_M371_178,VT_190128_M371_180"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GTA6-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_182,VT_190128_M371_184,VT_190128_M371_186"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GTB4-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_188,VT_190128_M371_190,VT_190128_M371_192"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GTC2-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_194,VT_190128_M371_196,VT_190128_M371_198"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GTD9-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_200,VT_190128_M371_202,VT_190128_M371_204"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GTE7-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_206,VT_190128_M371_208,VT_190128_M371_210"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GTG3-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_212,VT_190128_M371_214,VT_190128_M371_216"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1GTH1-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_218,VT_190128_M371_220,VT_190128_M371_222"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-WM3X7-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_224,VT_190128_M371_226,VT_190128_M371_228"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-1MW80-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_230,VT_190128_M371_232,VT_190128_M371_234"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-3GWU7-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_236,VT_190128_M371_238,VT_190128_M371_240"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-67TF5-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_242,VT_190128_M371_244,VT_190128_M371_246"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-6TPR9-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_248,VT_190128_M371_250,VT_190128_M371_252"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-8ERN6-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_254,VT_190128_M371_256,VT_190128_M371_258"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-LGR24-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_260,VT_190128_M371_262,VT_190128_M371_264"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-C60S1-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_266,VT_190128_M371_268,VT_190128_M371_270"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-CJ186-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_272,VT_190128_M371_274,VT_190128_M371_276"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-F02V3-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_278,VT_190128_M371_280,VT_190128_M371_282"}
},
{
"Subject ID":"Saliva Study Sample",
"Sample ID":"C-FKBQ9-SL-01_2",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_284,VT_190128_M371_286,VT_190128_M371_288"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"Q-Std Plasma pool_7e_1",
"Factors":{"Plasma":"Plasma"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Plasma","Raw files":"VT_190128_M371_290,VT_190128_M371_292,VT_190128_M371_294"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"Q-Std Plasma pool_7f_1",
"Factors":{"Plasma":"Plasma"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Plasma","Raw files":"VT_190128_M371_296,VT_190128_M371_298,VT_190128_M371_300"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"salivapool_7e_1",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_302,VT_190128_M371_304,VT_190128_M371_306"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"salivapool_7f_1",
"Factors":{"Plasma":"Saliva"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Saliva","Raw files":"VT_190128_M371_308,VT_190128_M371_310,VT_190128_M371_312"}
},
{
"Subject ID":"Quality Control",
"Sample ID":"NIST SRM 1950_2a",
"Factors":{"Plasma":"Plasma"},
"Additional sample data":{"Date Analyzed":"190128","Batch":"7","CHEAR_Project_ID":"2017-1762","Sample.Matrix":"Plasma","Raw files":"VT_190128_M371_314,VT_190128_M371_316,VT_190128_M371_318"}
}
],
"COLLECTION":{"COLLECTION_SUMMARY":"Saliva samples were collected from participants in the randomized controlled trial, An Intervention to Reduce Secondhand Smoke Exposure among Pediatric Emergency Patients, at baseline and a six-week follow up visit. Saliva samples were collected at baseline and a six-week follow up visit by standard protocol using oral swab collection, centrifugation and aliquots trasnferred to 1.8ml freezer tubes and stored in a -70 degree C freezer. The samples were shipped on dry ice from the Cincinnati Children's Hospital Medical Center biorepository storage facility and subsequently to the metabolomics analysis lab at Emory University.","SAMPLE_TYPE":"plasma","STORAGE_CONDITIONS":"Described in summary"},

"TREATMENT":{"TREATMENT_SUMMARY":"Samples were received frozen in aliquouts of <250uL. Prior to analysis, samples were thawed and prepared for HRM analysis using the standard protocols described in the Sample Preparation section."},

"SAMPLEPREP":{"SAMPLEPREP_SUMMARY":"Samples were prepared for metabolomics analysis using established methods(Johnson et al. (2010). Analyst; Go et al. (2015). Tox Sci). Prior to analysis, plasma aliquots were removed from storage at -80 degrees C and thawed on ice. Each cryotube was then vortexed briefly to ensure homogeneity, and 50 microliters was transferred to a clean microfuge tube. Immediately after, the plasma was treated with 100 microliters of ice-cold LC-MS grade acetonitrile (Sigma Aldrich) containing 2.5 microliters of internal standard solution with eight stable isotopic chemicals selected to cover a range of chemical properties. Following addition of acetonitrile, urine was equilibrated for 30 min on ice, upon which precipitated proteins were removed by centrifuge (14,000 rpm at 4 degrees C for 10 min). The resulting supernatant (100 microliters) was removed, added to a low volume autosampler vial and maintained at 4 degrees C until analysis (<22 h).","SAMPLEPREP_PROTOCOL_ID":"HRM_SP_082016_01","SAMPLEPREP_PROTOCOL_FILENAME":"EmoryUniversity_HRM_SP_082016_01.pdf","SAMPLEPREP_PROTOCOL_COMMENTS":"Date effective: 30 July 2016","EXTRACTION_METHOD":"2:1 acetonitrile: sample followed by vortexing and centrifugation"},

"CHROMATOGRAPHY":{"CHROMATOGRAPHY_SUMMARY":"The HILIC column is operated parallel to reverse phase column for simultaneous analytical separation and column flushing through the use of a dual head HPLC pump equipped with 10-port and 6-port switching valves. During operation of HILIC separation method, the MS is operated in positive ion mode and 10 microliters of sample is injected onto the HILIC column while the reverse phase column is flushing with wash solution. Flow rate is maintained at 0.35 mL/min until 1.5 min, increased to 0.4 mL/min at 4 min and held for 1 min. Solvent A is 100% LC-MS grade water, solvent B is 100% LC-MS grade acetonitrile and solvent C is 2% formic acid (v/v) in LC-MS grade water. Initial mobile phase conditions are 22.5% A, 75% B, 2.5% C hold for 1.5 min, with linear gradient to 77.5% A, 20% B, 2.5% C at 4 min, hold for 1 min, resulting in a total analytical run time of 5 min. During the flushing phase (reverse phase analytical separation), the HILIC column is equilibrated with a wash solution of 77.5% A, 20% B, 2.5% C.","CHROMATOGRAPHY_TYPE":"HILIC","INSTRUMENT_NAME":"Thermo Dionex Ultimate 3000","COLUMN_NAME":"Waters XBridge BEH Amide XP HILIC column. 2.1mm x 50mm x 2.5μm particle size with Thermo Accucore HILIC guard column with Thermo Accucore HILIC guard column","COLUMN_TEMPERATURE":"60 C","METHODS_FILENAME":"20160920_posHILIC120kres5min_ESI_c18negwash.meth","SOLVENT_A":"LC-MS grade water","SOLVENT_B":"LC-MS grade acetonitrile","METHODS_ID":"2% formic acid in LC-MS grade water","SAMPLE_INJECTION":"10 uL","ANALYTICAL_TIME":"5 min","SAMPLE_LOOP_SIZE":"15 uL","SAMPLE_SYRINGE_SIZE":"100 uL","CHROMATOGRAPHY_COMMENTS":"Triplicate injections for each chromatography mode"},

"ANALYSIS":{"ANALYSIS_TYPE":"MS","LABORATORY_NAME":"Clinical Biomarkers Laboratory","OPERATOR_NAME":"ViLinh Tran","DETECTOR_TYPE":"Orbitrap","SOFTWARE_VERSION":"Xcalibur 3.0.63","ACQUISITION_DATE":"1/23/19-2/1/19","ANALYSIS_PROTOCOL_FILE":"EmoryUniversity_HRM_QEHF-MS_092017_v1.pdf","DATA_FORMAT":"Profile"},

"MS":{"INSTRUMENT_NAME":"Thermo Q Exactive HF hybrid Orbitrap","INSTRUMENT_TYPE":"Orbitrap","MS_TYPE":"ESI","ION_MODE":"POSITIVE","MS_COMMENTS":"NA","ACQUISITION_DATE":"1/23/19-2/1/19","CAPILLARY_TEMPERATURE":"250C","COLLISION_GAS":"N2","DRY_GAS_FLOW":"45","DRY_GAS_TEMP":"150C","MASS_ACCURACY":"< 3ppm","SPRAY_VOLTAGE":"3500","ACTIVATION_PARAMETER":"5.00E+05","ACTIVATION_TIME":"118ms","INTERFACE_VOLTAGE":"S-Lens RF level= 55","SCANNING_RANGE":"85-1275"},

"MS_METABOLITE_DATA":{
"Units":"peak area",

"Data":[{"Metabolite":"Aniline","NIST SRM 1950_1a":"21614806.3","Q-Std Plasma pool_1a_1":"20366024.9","Q-Std Plasma pool_1b_1":"18683769.8","salivapool_1a_1":"25795029.4","salivapool_1b_1":"28074157.7","C-1GBF3-SL-01_2":"695175.7","C-1GBG1-SL-01_2":"989370.7","C-1GBH9-SL-01_2":"599288.6","C-1GBL0-SL-01_2":"0","C-1GBN5-SL-01_2":"725505.3","C-1GBP1-SL-01_2":"558249.5","C-1GBQ9-SL-01_2":"0","C-1GBR7-SL-01_2":"490927.2","C-1GBT2-SL-01_2":"615241.4","C-1GBX3-SL-01_2":"727125.2","C-1GBY1-SL-01_2":"9149437.1","C-1GC18-SL-01_2":"795334.7","C-1GC26-SL-01_2":"698223.6","C-1GC59-SL-01_2":"662165.8","C-1GC75-SL-01_2":"8290.5","C-1GC83-SL-01_2":"651380.6","C-1GCB1-SL-01_2":"597958.8","C-1GCF2-SL-01_2":"650774.2","C-1GCL9-SL-01_2":"0","C-1GCM7-SL-01_2":"842092.6","Q-Std Plasma pool_1c_1":"19683484.8","Q-Std Plasma pool_1d_1":"20272010.5","salivapool_1c_1":"26802117.7","salivapool_1d_1":"26673481","C-1GCN4-SL-01_2":"741317.8","C-1GCP0-SL-01_2":"157583.4","C-1GCQ8-SL-01_2":"801427.8","C-1GD25-SL-01_2":"849201","C-1GD33-SL-01_2":"1039299.1","C-1GD41-SL-01_2":"1187944.4","C-1GD58-SL-01_2":"1229110.8","C-1GD66-SL-01_2":"5188099.5","C-1GD74-SL-01_2":"2909222","C-1GDA2-SL-01_2":"525564.4","C-1GDB0-SL-01_2":"764705.6","C-1GDE3-SL-01_2":"878072.7","C-1GDF1-SL-01_2":"913806.7","C-XALJ8-SL-01_2":"858576","C-1GDG9-SL-01_2":"661753.1","C-1GDH7-SL-01_2":"772321.2","C-1GDJ2-SL-01_2":"954803.6","C-1GDM6-SL-01_2":"810512.6","C-1GDP9-SL-01_2":"2058283.3","C-1GDQ7-SL-01_2":"769562.4","Q-Std Plasma pool_1e_1":"18892770.3","Q-Std Plasma pool_1f_1":"19418926","salivapool_1e_1":"29030580.2","salivapool_1f_1":"29810006.9","Q-Std Plasma pool_2a_1":"18790362.4","Q-Std Plasma pool_2b_1":"17854149.1","salivapool_2a_1":"27733424.3","salivapool_2b_1":"27602963.9","C-1GDR5-SL-01_2":"750227.2","C-1GE16-SL-01_2":"738817.8","C-1GE24-SL-01_2":"703000.9","C-1GE40-SL-01_2":"584065","C-1GE65-SL-01_2":"694107.1","C-1GE73-SL-01_2":"475531.7","C-1GEB9-SL-01_2":"459434.8","C-1GEC7-SL-01_2":"15737027.3","C-1GEE2-SL-01_2":"772557.4","C-1GEF0-SL-01_2":"425454.1","C-1GEH6-SL-01_2":"718123.4","C-1GEK9-SL-01_2":"870384","C-JWM67-SL-01_2":"971260.7","C-1GEL7-SL-01_2":"1042292.7","C-G2T98-SL-01_2":"937191.8","C-1GEP8-SL-01_2":"469880.5","C-1GER4-SL-01_2":"919148.8","C-1GET9-SL-01_2":"9614878.4","C-1GEU7-SL-01_2":"966394.1","C-1GEX0-SL-01_2":"760696.3","Q-Std Plasma pool_2c_1":"19305627.9","Q-Std Plasma pool_2d_1":"19992406.2","salivapool_2c_1":"28994436.7","salivapool_2d_1":"27885733.5","C-1GEY8-SL-01_2":"808021.6","C-1GF15-SL-01_2":"524127.4","C-1GF23-SL-01_2":"481448.3","C-1GF56-SL-01_2":"814536.5","C-1GF80-SL-01_2":"801600.3","C-1GF98-SL-01_2":"891816.2","C-1GFB8-SL-01_2":"0","C-1GFC6-SL-01_2":"568460.2","C-1GFG7-SL-01_2":"829991","C-1GFJ0-SL-01_2":"543526.3","C-1GFL6-SL-01_2":"506264.4","C-1GFP7-SL-01_2":"1057911.9","C-1GFQ5-SL-01_2":"880337.6","C-1GFS0-SL-01_2":"910238.9","C-1GFW2-SL-01_2":"917230.6","C-1GFX9-SL-01_2":"546479.2","C-1GG48-SL-01_2":"953541.6","C-1GG55-SL-01_2":"0","C-1GG63-SL-01_2":"618388.4","C-1GG89-SL-01_2":"849195.6","Q-Std Plasma pool_2e_1":"20584913.6","Q-Std Plasma pool_2f_1":"21182667.3","salivapool_2e_1":"27734725.2","salivapool_2f_1":"28000841.9","Q-Std Plasma pool_3a_1":"25790904.7","Q-Std Plasma 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time":"75.6","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"Pyridoxal","chemical_ID":"HMDB01545","InChiKey":"InChIKey=RADKZDMFGJYCBB-UHFFFAOYSA-N","quantified m/z":"168.0655","retention time":"40.3","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"3-Methoxytyramine","chemical_ID":"HMDB00022","InChiKey":"InChIKey=DIVQKHQLANKJQO-UHFFFAOYSA-N","quantified m/z":"168.1018","retention time":"37.2","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"Quinaldic acid","chemical_ID":"HMDB00842","InChiKey":"InChIKey=LOAUVZALPPNFOQ-UHFFFAOYSA-N","quantified m/z":"174.055","retention time":"25.7","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"N-Acetylleucine","chemical_ID":"HMDB11756","InChiKey":"InChIKey=WXNXCEHXYPACJF-ZETCQYMHSA-N","quantified m/z":"174.1125","retention time":"35.7","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"Arginine","chemical_ID":"HMDB00517","InChiKey":"InChIKey=ODKSFYDXXFIFQN-BYPYZUCNSA-N","quantified m/z":"175.119","retention time":"103.9","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"Citrulline","chemical_ID":"HMDB00904","InChiKey":"InChIKey=RHGKLRLOHDJJDR-BYPYZUCNSA-N","quantified m/z":"176.103","retention time":"104.2","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"Hippuric acid","chemical_ID":"HMDB00714","InChiKey":"InChIKey=QIAFMBKCNZACKA-UHFFFAOYSA-N","quantified m/z":"180.0656","retention time":"33.3","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"(R)-Salsolinol","chemical_ID":"HMDB05199","InChiKey":"InChIKey=IBRKLUSXDYATLG-UHFFFAOYSA-N","quantified m/z":"180.1017","retention time":"43.4","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"N-Alpha-acetyllysine","chemical_ID":"HMDB00446","InChiKey":"InChIKey=VEYYWZRYIYDQJM-UHFFFAOYSA-N","quantified m/z":"189.1233","retention time":"80.6","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"Diaminopimelic acid","chemical_ID":"HMDB01370","InChiKey":"InChIKey=GMKMEZVLHJARHF-WHFBIAKZSA-N","quantified m/z":"191.1029","retention time":"213.5","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"Selenomethionine","chemical_ID":"HMDB03966","InChiKey":"InChIKey=RJFAYQIBOAGBLC-UHFFFAOYSA-N","quantified m/z":"198.0034","retention time":"38.4","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"Acetylcarnitine","chemical_ID":"HMDB00201","InChiKey":"InChIKey=RDHQFKQIGNGIED-UHFFFAOYSA-N","quantified m/z":"204.123","retention time":"64.5","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"Kynurenine","chemical_ID":"HMDB00684","InChiKey":"InChIKey=YGPSJZOEDVAXAB-QMMMGPOBSA-N","quantified m/z":"209.0916","retention time":"54.7","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"12-Hydroxydodecanoic acid","chemical_ID":"HMDB02059","InChiKey":"InChIKey=ZDHCZVWCTKTBRY-UHFFFAOYSA-N","quantified m/z":"217.1797","retention time":"24.1","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"Pantothenic acid","chemical_ID":"HMDB00210","InChiKey":"InChIKey=GHOKWGTUZJEAQD-UHFFFAOYSA-N","quantified m/z":"220.1182","retention time":"45.3","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"Methyl jasmonate","chemical_ID":"HMDB36583","InChiKey":"InChIKey=GEWDNTWNSAZUDX-LEPXEHPDNA-N","quantified m/z":"225.1484","retention time":"33.5","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"Carnosine","chemical_ID":"HMDB00033","InChiKey":"InChIKey=CQOVPNPJLQNMDC-ZETCQYMHSA-N","quantified m/z":"227.1135","retention time":"99.8","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"Cystine","chemical_ID":"HMDB00192","InChiKey":"InChIKey=LEVWYRKDKASIDU-IMJSIDKUSA-N","quantified m/z":"241.0307","retention time":"214.5","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"Anserine","chemical_ID":"HMDB00194","InChiKey":"InChIKey=MYYIAHXIVFADCU-QMMMGPOBSA-N","quantified m/z":"241.1292","retention time":"114.2","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"Glutathione","chemical_ID":"HMDB00125","InChiKey":"InChIKey=RWSXRVCMGQZWBV-WDSKDSINSA-N","quantified m/z":"308.0919","retention time":"90.5","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"Guanosine monophosphate","chemical_ID":"HMDB01397","InChiKey":"InChIKey=RQFCJASXJCIDSX-UUOKFMHZSA-N","quantified m/z":"364.0644","retention time":"257.1","MSIcategory":"1","Adduct":"M+H"},{"Metabolite":"Stachyose","chemical_ID":"HMDB03553","InChiKey":"InChIKey=UQZIYBXSHAGNOE-XNSRJBNMSA-N","quantified m/z":"667.227","retention time":"252","MSIcategory":"1","Adduct":"M+H"}]
}

}