#METABOLOMICS WORKBENCH kmercier_20160613_095123 DATATRACK_ID:645 STUDY_ID:ST000411 ANALYSIS_ID:AN000651 PROJECT_ID:PR000321 VERSION 1 CREATED_ON June 27, 2016, 12:17 pm #PROJECT PR:PROJECT_TITLE SRM Proficiency PR:PROJECT_SUMMARY Pooled urine samples from smokers (NIST SRM 3672) and non-smokers (NIST SRM PR:PROJECT_SUMMARY 3673) were provided by NIH. PR:INSTITUTE National Institutes of Health PR:DEPARTMENT CHEAR PR:LAST_NAME Sumner PR:FIRST_NAME Su PR:ADDRESS 3040 E. Cornwallis Road PR:EMAIL ssumner@rti.org PR:PHONE 919-541-7479 #STUDY ST:STUDY_TITLE Smoking and urinary metabolomics ST:STUDY_SUMMARY This metabolomics projects was to evaluate the differences between pooled urine ST:STUDY_SUMMARY from smokers and non-smokers from NIST. ST:INSTITUTE RTI International ST:LAST_NAME Sumner ST:FIRST_NAME Susan ST:ADDRESS 3040 E. Cornwallis Road ST:EMAIL ssumner@rti.org ST:PHONE 919-541-7479 #SUBJECT SU:SUBJECT_TYPE Human SU:SUBJECT_SPECIES Homo sapiens SU:TAXONOMY_ID 9606 #SUBJECT_SAMPLE_FACTORS: SUBJECT(optional)[tab]SAMPLE[tab]FACTORS(NAME:VALUE pairs separated by |)[tab]Additional sample data SUBJECT_SAMPLE_FACTORS - N3672-1d Group:Smoker SUBJECT_SAMPLE_FACTORS - N3672-1d1 Group:Smoker SUBJECT_SAMPLE_FACTORS - N3672-1e Group:Smoker SUBJECT_SAMPLE_FACTORS - N3672-1e1 Group:Smoker SUBJECT_SAMPLE_FACTORS - N3672-1f Group:Smoker SUBJECT_SAMPLE_FACTORS - N3672-1f1 Group:Smoker SUBJECT_SAMPLE_FACTORS - N3672-1g Group:Smoker SUBJECT_SAMPLE_FACTORS - N3672-1g1 Group:Smoker SUBJECT_SAMPLE_FACTORS - N3672-1h Group:Smoker SUBJECT_SAMPLE_FACTORS - N3672-1h1 Group:Smoker SUBJECT_SAMPLE_FACTORS - N3673-1d Group:Non-Smoker SUBJECT_SAMPLE_FACTORS - N3673-1d1 Group:Non-Smoker SUBJECT_SAMPLE_FACTORS - N3673-1e Group:Non-Smoker SUBJECT_SAMPLE_FACTORS - N3673-1e1 Group:Non-Smoker SUBJECT_SAMPLE_FACTORS - N3673-1f Group:Non-Smoker SUBJECT_SAMPLE_FACTORS - N3673-1f1 Group:Non-Smoker SUBJECT_SAMPLE_FACTORS - N3673-1g Group:Non-Smoker SUBJECT_SAMPLE_FACTORS - N3673-1g1 Group:Non-Smoker SUBJECT_SAMPLE_FACTORS - N3673-1h Group:Non-Smoker SUBJECT_SAMPLE_FACTORS - N3673-1h1 Group:Non-Smoker SUBJECT_SAMPLE_FACTORS - TotalPool_1 Group:Total Pool SUBJECT_SAMPLE_FACTORS - TotalPool_2 Group:Total Pool SUBJECT_SAMPLE_FACTORS - TotalPool_3 Group:Total Pool SUBJECT_SAMPLE_FACTORS - TotalPool_4 Group:Total Pool SUBJECT_SAMPLE_FACTORS - TotalPool_5 Group:Total Pool #COLLECTION CO:COLLECTION_SUMMARY Pooled urine samples from smokers (NIST SRM 3672) and non-smokers (NIST SRM CO:COLLECTION_SUMMARY 3673) were provided by NIH. #TREATMENT TR:TREATMENT_SUMMARY Pooled urine samples from smokers (NIST SRM 3672) and non-smokers (NIST SRM TR:TREATMENT_SUMMARY 3673) were provided by NIH. #SAMPLEPREP SP:SAMPLEPREP_SUMMARY Vials of pooled urine (smoker and non-smoker) were shipped the NIH RTI-RCMRC on SP:SAMPLEPREP_SUMMARY dry ice and immediately stored at -80 °C after being logged in for metabolomics SP:SAMPLEPREP_SUMMARY analysis. Five 1 mL aliquots of each pool were taken for NMR analysis. A total SP:SAMPLEPREP_SUMMARY of 10 study samples were thawed on ice for sample preparation. Two aliquots (400 SP:SAMPLEPREP_SUMMARY μl) of thawed urine from each sample was mixed with 230 μl of 0.5 mM phosphate SP:SAMPLEPREP_SUMMARY buffer (pH 7.5) and 70 uL of Chenomx ISTD solution. A total study pool was SP:SAMPLEPREP_SUMMARY created by mixing 150 μl of urine from each sample. Additionally, two random QC SP:SAMPLEPREP_SUMMARY pools were created. The tubes were vortexed for 2 min on a multi-tube vortexer. SP:SAMPLEPREP_SUMMARY A 600 µl aliquot of the supernatant was transferred into pre-labeled 5 mm SP:SAMPLEPREP_SUMMARY (7”) NMR tubes for data acquisition on a 700 MHz spectrometer. 1H NMR spectra SP:SAMPLEPREP_SUMMARY of urine samples were acquired on a Bruker 700 MHz NMR spectrometer (located at SP:SAMPLEPREP_SUMMARY North Carolina State University, Raleigh, NC, USA) using a 5 mm cryogenically SP:SAMPLEPREP_SUMMARY cooled ATMA inverse probe and ambient temperature of 25 ℃. A 1D NOESY SP:SAMPLEPREP_SUMMARY presaturation pulse sequence (noesypr1d, [recycle delay SP:SAMPLEPREP_SUMMARY (RD)-90°-t1-90°-tm-90°-acquire free induction decay (FID) was used for data SP:SAMPLEPREP_SUMMARY acquisition. For each sample 16 transients were collected into 65k data points SP:SAMPLEPREP_SUMMARY using a spectral width of 12.02 ppm, 2 s relaxation delay, 100 ms mixing time, SP:SAMPLEPREP_SUMMARY and an acquisition time of 3.89 s per FID. The water resonance was suppressed SP:SAMPLEPREP_SUMMARY using resonance irradiation during the relaxation delay and mixing time. NMR SP:SAMPLEPREP_SUMMARY spectra were processed using TopSpin 3.2 software (Bruker-Biospin, Germany). SP:SAMPLEPREP_SUMMARY Spectra were zero filled, and Fourier transformed after exponential SP:SAMPLEPREP_SUMMARY multiplication with line broadening factor of 0.5. Phase and baseline of the SP:SAMPLEPREP_SUMMARY spectra were manually corrected for each spectrum. Spectra were referenced SP:SAMPLEPREP_SUMMARY internally to the DSS-d6 signal. The quality of each NMR spectrum was assessed SP:SAMPLEPREP_SUMMARY for the level of noise and alignment of identified markers. Spectra were SP:SAMPLEPREP_SUMMARY assessed for missing data and underwent quality checks. NMR bins (0.7-9.50 ppm) SP:SAMPLEPREP_SUMMARY were created excluding water and urea (4.25- 6.5 ppm) using intelligent bucket SP:SAMPLEPREP_SUMMARY integration of 0.04 ppm bucket width with 50% looseness using ACD NMR Processor SP:SAMPLEPREP_SUMMARY (ACD Labs Inc, Toronto, Canada). Integrals of each of the bins were normalized SP:SAMPLEPREP_SUMMARY to total integral of each of the spectrum. #CHROMATOGRAPHY CH:CHROMATOGRAPHY_TYPE - CH:INSTRUMENT_NAME - CH:COLUMN_NAME - #ANALYSIS AN:ANALYSIS_TYPE NMR #NMR NM:INSTRUMENT_NAME Bruker Avance III NM:INSTRUMENT_TYPE FT-NMR NM:NMR_EXPERIMENT_TYPE 1D-1H NM:SPECTROMETER_FREQUENCY 700.13 MHz #NMR_BINNED_DATA NMR_BINNED_DATA:UNITS Peak area NMR_BINNED_DATA_START Bin range(ppm) N3672-1d N3672-1d1 N3672-1e N3672-1e1 N3672-1f N3672-1f1 N3672-1g N3672-1g1 N3672-1h N3672-1h1 N3673-1d N3673-1d1 N3673-1e N3673-1e1 N3673-1f N3673-1f1 N3673-1g N3673-1g1 N3673-1h N3673-1h1 TotalPool_1 TotalPool_2 TotalPool_3 TotalPool_4 TotalPool_5 [0.70 .. 0.72] 0.22 0.22 0.14 0.23 0.09 0.19 0.28 0.22 0.19 0.22 0.04 0.04 0.00 0.06 0.03 0.04 0.03 0.04 0.02 0.05 0.06 0.12 0.09 0.12 0.08 [0.72 .. 0.77] 0.69 0.71 0.55 0.66 0.45 0.66 0.88 0.71 0.59 0.70 0.18 0.18 0.13 0.23 0.16 0.18 0.17 0.19 0.15 0.21 0.28 0.39 0.34 0.40 0.29 [0.77 .. 0.80] 0.26 0.29 0.20 0.25 0.09 0.27 0.39 0.28 0.24 0.30 0.05 0.07 0.03 0.07 0.04 0.07 0.06 0.06 0.05 0.07 0.09 0.16 0.14 0.16 0.10 [0.80 .. 0.82] 0.33 0.34 0.26 0.31 0.22 0.34 0.40 0.33 0.28 0.32 0.07 0.09 0.06 0.09 0.06 0.07 0.08 0.09 0.07 0.10 0.12 0.19 0.16 0.18 0.14 [0.82 .. 0.84] 0.58 0.64 0.58 0.61 0.50 0.61 0.72 0.64 0.54 0.61 0.16 0.18 0.16 0.18 0.17 0.17 0.18 0.18 0.17 0.19 0.27 0.32 0.32 0.32 0.28 [0.84 .. 0.90] 6.17 6.22 6.18 6.21 5.95 6.29 6.41 6.10 6.10 6.25 1.92 1.93 1.89 1.97 1.89 1.90 1.92 1.95 1.91 1.98 3.19 3.31 3.28 3.35 3.19 [0.90 .. 0.96] 3.91 3.89 3.80 3.81 3.59 3.91 4.02 3.83 3.84 3.85 1.20 1.22 1.16 1.28 1.20 1.19 1.21 1.21 1.19 1.27 1.98 2.11 2.07 2.12 2.03 [0.96 .. 1.01] 2.66 2.62 2.41 2.54 2.28 2.63 2.87 2.66 2.49 2.53 0.77 0.80 0.73 0.85 0.76 0.77 0.78 0.78 0.74 0.81 1.25 1.43 1.36 1.44 1.31 [1.01 .. 1.04] 1.23 1.23 1.14 1.24 1.05 1.21 1.39 1.22 1.11 1.18 0.38 0.39 0.36 0.42 0.38 0.38 0.38 0.39 0.38 0.41 0.60 0.68 0.66 0.69 0.62 [1.04 .. 1.08] 3.25 3.25 3.18 3.23 3.07 3.27 3.36 3.23 3.19 3.21 0.97 0.98 0.94 1.01 0.95 0.97 0.96 0.96 0.97 0.99 1.64 1.74 1.70 1.76 1.65 [1.08 .. 1.12] 2.51 2.50 2.41 2.49 2.29 2.53 2.66 2.50 2.38 2.48 1.05 1.07 1.01 1.09 1.04 1.04 1.04 1.03 1.02 1.10 1.42 1.56 1.50 1.55 1.45 [1.12 .. 1.15] 2.75 2.79 2.79 2.82 2.62 2.81 2.95 2.75 2.67 2.78 1.09 1.10 1.08 1.12 1.07 1.08 1.09 1.09 1.07 1.11 1.57 1.63 1.63 1.67 1.55 [1.15 .. 1.17] 2.50 2.53 2.54 2.58 2.38 2.55 2.67 2.48 2.42 2.56 0.68 0.70 0.69 0.71 0.68 0.69 0.69 0.70 0.67 0.72 1.23 1.29 1.28 1.29 1.22 [1.17 .. 1.21] 7.43 7.37 7.46 7.43 7.21 7.50 7.55 7.30 7.35 7.43 1.95 1.95 1.93 1.99 1.95 1.96 1.94 1.96 1.94 1.99 3.65 3.72 3.70 3.75 3.62 [1.21 .. 1.25] 7.09 6.98 7.06 7.03 6.85 7.11 7.18 6.98 7.06 7.01 2.23 2.24 2.20 2.28 2.21 2.21 2.21 2.23 2.18 2.25 3.92 4.02 3.96 4.01 3.92 [1.25 .. 1.28] 4.23 4.19 4.24 4.23 4.07 4.25 4.35 4.15 4.17 4.21 1.20 1.20 1.19 1.23 1.18 1.19 1.21 1.20 1.19 1.23 2.11 2.19 2.16 2.18 2.10 [1.28 .. 1.34] 9.08 9.00 9.01 9.02 8.77 9.13 9.30 8.99 9.05 9.06 2.72 2.75 2.68 2.79 2.69 2.69 2.73 2.73 2.69 2.77 4.64 4.79 4.73 4.81 4.65 [1.34 .. 1.36] 2.84 2.82 2.78 2.82 2.71 2.85 2.92 2.83 2.83 2.82 0.84 0.86 0.84 0.88 0.83 0.84 0.83 0.84 0.84 0.87 1.43 1.50 1.48 1.52 1.44 [1.36 .. 1.40] 5.18 5.15 5.02 5.12 4.91 5.16 5.30 5.14 5.11 5.13 1.33 1.32 1.30 1.38 1.29 1.30 1.29 1.31 1.31 1.37 2.44 2.56 2.54 2.58 2.47 [1.40 .. 1.43] 2.30 2.26 2.17 2.24 2.10 2.27 2.35 2.25 2.21 2.25 0.65 0.66 0.65 0.70 0.65 0.66 0.64 0.67 0.63 0.68 1.13 1.20 1.18 1.20 1.13 [1.43 .. 1.46] 2.85 2.82 2.72 2.86 2.69 2.85 2.97 2.86 2.74 2.82 0.91 0.94 0.91 0.97 0.91 0.91 0.90 0.92 0.89 0.96 1.47 1.57 1.53 1.58 1.47 [1.46 .. 1.49] 6.41 6.31 6.37 6.36 6.18 6.41 6.52 6.29 6.32 6.34 1.50 1.52 1.48 1.55 1.48 1.51 1.48 1.50 1.48 1.54 2.98 3.08 3.06 3.11 2.99 [1.49 .. 1.53] 4.20 4.10 3.98 4.10 3.92 4.19 4.31 4.14 4.07 4.09 1.12 1.14 1.10 1.17 1.09 1.10 1.09 1.10 1.08 1.16 2.02 2.13 2.10 2.15 2.01 [1.53 .. 1.57] 3.88 3.84 3.63 3.79 3.56 3.84 4.05 3.86 3.81 3.74 1.14 1.17 1.13 1.22 1.12 1.14 1.14 1.14 1.11 1.20 1.91 2.03 2.01 2.08 1.92 [1.57 .. 1.59] 1.85 1.82 1.71 1.79 1.71 1.82 1.91 1.82 1.76 1.77 0.54 0.55 0.54 0.58 0.54 0.54 0.54 0.54 0.54 0.57 0.91 0.99 0.95 0.99 0.91 [1.59 .. 1.61] 2.29 2.23 2.16 2.26 2.13 2.28 2.42 2.24 2.21 2.24 0.62 0.65 0.64 0.68 0.62 0.63 0.63 0.63 0.62 0.68 1.09 1.18 1.16 1.19 1.10 [1.61 .. 1.67] 6.39 6.37 6.12 6.32 6.07 6.39 6.65 6.41 6.22 6.29 2.08 2.10 2.07 2.20 2.05 2.08 2.06 2.08 2.03 2.16 3.33 3.53 3.46 3.58 3.32 [1.67 .. 1.69] 1.77 1.72 1.63 1.71 1.59 1.73 1.83 1.77 1.66 1.70 0.52 0.53 0.53 0.56 0.51 0.52 0.52 0.51 0.51 0.55 0.86 0.94 0.91 0.96 0.89 [1.69 .. 1.74] 3.87 3.81 3.59 3.81 3.58 3.86 4.05 3.88 3.70 3.80 1.24 1.27 1.25 1.32 1.22 1.23 1.23 1.24 1.22 1.31 1.95 2.13 2.08 2.17 1.99 [1.74 .. 1.79] 5.31 5.25 4.99 5.30 4.87 5.32 5.68 5.27 5.09 5.22 1.62 1.68 1.63 1.77 1.62 1.63 1.60 1.63 1.58 1.71 2.66 2.88 2.82 2.93 2.65 [1.79 .. 1.85] 6.20 6.08 5.84 6.10 5.78 6.26 6.52 6.21 5.97 6.10 2.08 2.14 2.11 2.24 2.05 2.09 2.06 2.07 2.04 2.17 3.21 3.46 3.40 3.54 3.24 [1.85 .. 1.87] 2.04 2.03 1.92 2.00 1.87 2.06 2.20 2.05 1.92 2.00 0.68 0.70 0.69 0.74 0.67 0.69 0.66 0.68 0.65 0.72 1.04 1.14 1.11 1.17 1.05 [1.87 .. 1.89] 2.19 2.19 2.09 2.21 2.04 2.21 2.39 2.21 2.07 2.20 0.72 0.74 0.74 0.78 0.71 0.73 0.71 0.73 0.72 0.77 1.15 1.23 1.22 1.25 1.13 [1.89 .. 1.95] 8.76 8.66 8.43 8.63 8.34 8.80 9.12 8.77 8.52 8.69 3.00 3.07 3.04 3.16 3.01 3.02 3.01 2.98 2.96 3.10 4.65 4.92 4.85 4.99 4.68 [1.95 .. 1.99] 4.21 4.19 4.01 4.17 4.00 4.25 4.46 4.22 4.02 4.16 1.31 1.33 1.34 1.40 1.30 1.31 1.29 1.30 1.28 1.36 2.12 2.28 2.26 2.31 2.14 [1.99 .. 2.01] 2.28 2.28 2.21 2.34 2.16 2.33 2.51 2.33 2.15 2.28 0.69 0.71 0.71 0.75 0.68 0.69 0.69 0.69 0.67 0.74 1.13 1.24 1.21 1.26 1.14 [2.01 .. 2.06] 14.10 14.00 14.10 14.10 13.80 14.30 14.50 14.00 14.00 14.10 4.30 4.37 4.35 4.46 4.30 4.34 4.30 4.30 4.26 4.41 7.25 7.49 7.47 7.54 7.22 [2.06 .. 2.10] 5.22 5.18 5.01 5.18 4.98 5.26 5.42 5.24 5.14 5.19 1.60 1.66 1.63 1.70 1.60 1.62 1.59 1.60 1.58 1.68 2.66 2.80 2.79 2.85 2.66 [2.10 .. 2.13] 5.50 5.52 5.42 5.54 5.33 5.61 5.83 5.48 5.37 5.50 2.11 2.15 2.15 2.20 2.11 2.12 2.11 2.10 2.09 2.19 3.09 3.24 3.24 3.29 3.08 [2.13 .. 2.18] 14.50 14.40 14.40 14.30 14.10 14.50 14.70 14.40 14.40 14.40 8.82 8.89 8.88 8.97 8.84 8.85 8.80 8.82 8.80 8.91 10.50 10.70 10.70 10.70 10.50 [2.18 .. 2.23] 6.15 6.08 5.75 6.08 5.75 6.10 6.40 6.21 5.99 6.00 1.99 2.05 2.02 2.14 1.96 1.99 1.99 1.99 1.96 2.10 3.20 3.40 3.36 3.46 3.20 [2.23 .. 2.28] 8.87 8.77 8.64 8.81 8.50 8.83 9.11 8.89 8.70 8.71 3.45 3.51 3.49 3.58 3.45 3.46 3.43 3.44 3.42 3.56 5.06 5.24 5.20 5.31 5.05 [2.28 .. 2.30] 3.08 3.03 2.85 3.02 2.84 3.03 3.23 3.11 2.98 2.97 1.02 1.06 1.06 1.11 1.03 1.04 1.01 1.03 1.00 1.09 1.61 1.73 1.72 1.76 1.62 [2.30 .. 2.35] 7.27 7.25 6.99 7.21 6.89 7.27 7.54 7.33 7.09 7.20 2.60 2.67 2.66 2.75 2.61 2.62 2.59 2.60 2.56 2.70 3.95 4.17 4.13 4.22 3.97 [2.35 .. 2.37] 3.20 3.19 3.00 3.18 2.97 3.20 3.38 3.26 3.07 3.13 0.79 0.84 0.83 0.89 0.80 0.81 0.79 0.79 0.77 0.85 1.47 1.61 1.59 1.65 1.50 [2.37 .. 2.40] 4.17 4.19 3.91 4.15 3.88 4.18 4.44 4.22 3.99 4.08 1.20 1.26 1.25 1.33 1.21 1.24 1.22 1.22 1.19 1.31 2.07 2.19 2.20 2.27 2.08 [2.40 .. 2.46] 9.10 9.05 8.76 9.03 8.69 9.11 9.53 9.13 8.83 9.02 2.28 2.41 2.36 2.53 2.28 2.31 2.26 2.28 2.26 2.45 4.26 4.57 4.54 4.67 4.28 [2.46 .. 2.48] 3.46 3.46 3.17 3.44 3.20 3.50 3.65 3.51 3.30 3.38 0.97 1.02 1.02 1.10 0.97 1.00 0.96 0.97 0.95 1.06 1.68 1.81 1.79 1.86 1.67 [2.48 .. 2.53] 11.00 10.80 10.70 10.90 10.60 11.00 11.40 10.90 10.70 10.80 4.00 4.11 4.12 4.20 4.03 4.04 4.00 3.99 4.00 4.14 6.02 6.30 6.27 6.40 6.02 [2.53 .. 2.58] 12.00 12.00 11.60 12.00 11.60 12.00 12.10 12.20 12.00 11.90 4.28 4.39 4.36 4.48 4.27 4.29 4.23 4.27 4.23 4.41 6.58 6.84 6.78 6.90 6.60 [2.58 .. 2.62] 2.91 2.89 2.47 2.87 2.55 2.90 3.21 3.09 2.73 2.76 0.69 0.79 0.77 0.89 0.70 0.72 0.69 0.69 0.67 0.83 1.24 1.51 1.47 1.58 1.27 [2.62 .. 2.64] 1.42 1.45 1.22 1.47 1.23 1.50 1.69 1.53 1.28 1.39 0.39 0.45 0.45 0.51 0.40 0.42 0.38 0.39 0.38 0.48 0.64 0.79 0.78 0.84 0.65 [2.64 .. 2.69] 16.20 16.10 16.00 16.20 15.80 16.40 16.70 16.10 16.00 16.10 6.39 6.47 6.50 6.62 6.37 6.38 6.32 6.31 6.32 6.53 9.25 9.59 9.57 9.74 9.24 [2.69 .. 2.73] 7.16 7.19 6.89 7.14 6.81 7.16 7.30 7.27 7.09 7.09 2.19 2.30 2.29 2.37 2.19 2.22 2.16 2.18 2.15 2.31 3.66 3.87 3.84 3.92 3.66 [2.73 .. 2.79] 4.80 4.84 4.00 4.79 4.15 4.76 5.29 5.13 4.42 4.63 1.53 1.70 1.70 1.88 1.53 1.59 1.49 1.49 1.47 1.76 2.32 2.75 2.69 2.86 2.34 [2.79 .. 2.83] 3.38 3.34 2.83 3.35 2.93 3.38 3.81 3.54 3.02 3.21 0.74 0.86 0.87 0.99 0.73 0.78 0.70 0.73 0.69 0.91 1.36 1.69 1.67 1.81 1.38 [2.83 .. 2.88] 3.91 3.99 3.16 3.87 3.27 3.99 4.78 4.20 3.40 3.79 0.83 1.04 1.02 1.21 0.83 0.89 0.78 0.82 0.75 1.11 1.51 2.02 1.99 2.24 1.53 [2.88 .. 2.94] 4.48 4.49 3.54 4.40 3.70 4.65 5.58 4.74 3.83 4.25 0.76 1.06 1.04 1.28 0.79 0.86 0.74 0.74 0.69 1.13 1.59 2.22 2.19 2.50 1.56 [2.94 .. 2.96] 0.91 0.90 0.55 0.88 0.59 0.99 1.45 0.98 0.58 0.83 0.10 0.20 0.20 0.28 0.09 0.13 0.06 0.07 0.05 0.23 0.18 0.46 0.44 0.56 0.17 [2.96 .. 2.98] 1.44 1.41 1.07 1.40 1.12 1.58 2.11 1.44 1.01 1.36 0.25 0.37 0.38 0.47 0.26 0.30 0.22 0.23 0.22 0.40 0.46 0.74 0.75 0.89 0.44 [2.98 .. 3.02] 5.50 5.36 4.84 5.38 4.73 6.06 7.52 5.13 4.15 5.35 1.10 1.38 1.41 1.57 1.15 1.22 1.07 1.05 1.05 1.46 2.03 2.74 2.80 3.10 1.96 [3.02 .. 3.07] 85.50 85.20 87.90 85.80 85.80 86.00 83.90 84.20 86.70 86.10 26.90 27.10 27.10 27.10 26.90 27.00 26.80 26.90 26.80 27.00 45.60 45.40 45.50 45.40 45.30 [3.07 .. 3.09] 1.87 1.94 1.63 1.94 1.67 1.67 1.74 2.13 1.93 1.82 0.32 0.41 0.42 0.50 0.31 0.35 0.31 0.31 0.27 0.44 0.71 0.90 0.89 0.95 0.72 [3.09 .. 3.12] 5.37 5.40 5.10 5.38 5.13 5.26 5.33 5.57 5.33 5.29 1.74 1.88 1.88 1.99 1.75 1.79 1.72 1.72 1.68 1.93 2.75 3.00 2.98 3.08 2.74 [3.12 .. 3.17] 10.80 10.90 10.30 10.90 10.30 10.80 11.00 11.20 10.70 10.70 3.78 4.15 4.16 4.42 3.81 3.91 3.71 3.74 3.66 4.20 5.66 6.32 6.29 6.60 5.65 [3.17 .. 3.20] 8.10 8.08 7.69 8.10 7.69 8.08 8.45 8.25 7.87 8.00 2.20 2.56 2.59 2.80 2.23 2.37 2.12 2.13 2.09 2.60 3.66 4.30 4.34 4.62 3.64 [3.20 .. 3.26] 32.80 32.70 32.90 33.00 32.30 33.10 33.40 32.60 32.50 32.90 79.80 80.40 80.30 80.40 80.10 80.20 79.80 79.90 79.80 80.20 65.00 65.20 65.50 65.40 64.40 [3.26 .. 3.32] 11.40 11.60 10.70 11.50 10.80 11.20 11.10 12.20 11.70 11.30 4.91 5.08 5.02 5.27 4.88 4.88 4.84 4.90 4.78 5.07 6.86 7.27 7.11 7.24 6.94 [3.32 .. 3.35] 3.83 3.94 3.41 3.95 3.48 3.77 4.07 4.14 3.68 3.80 1.44 1.69 1.75 1.91 1.46 1.56 1.41 1.42 1.36 1.77 1.93 2.41 2.40 2.63 1.92 [3.35 .. 3.37] 1.95 1.97 1.53 1.98 1.64 1.90 2.18 2.21 1.82 1.87 0.74 1.00 1.02 1.22 0.77 0.84 0.66 0.65 0.59 1.05 0.84 1.36 1.35 1.61 0.81 [3.37 .. 3.43] 18.80 18.90 18.20 19.00 18.10 19.00 19.80 19.10 18.30 18.80 110.00 111.00 111.00 111.00 111.00 111.00 110.00 110.00 110.00 110.00 81.10 81.40 81.80 81.80 80.40 [3.43 .. 3.48] 16.00 16.10 15.40 16.10 15.40 16.00 16.60 16.20 15.60 15.90 91.00 91.20 91.60 91.10 91.30 91.20 91.20 91.10 91.30 91.30 67.30 67.20 67.60 67.30 66.70 [3.48 .. 3.51] 12.10 12.10 11.70 12.20 11.70 12.10 12.40 12.20 11.80 12.00 52.20 51.90 51.60 51.30 52.20 52.00 52.10 52.00 52.20 51.30 40.00 39.40 39.20 38.90 40.00 [3.51 .. 3.57] 24.80 24.80 24.20 25.00 24.10 24.90 25.50 25.00 24.40 24.70 48.30 47.80 47.90 47.60 48.40 48.20 48.50 48.40 48.60 47.60 41.30 40.50 40.40 40.20 41.20 [3.57 .. 3.59] 6.30 6.39 6.08 6.46 6.05 6.33 6.79 6.43 6.06 6.34 2.78 2.72 2.77 2.71 2.77 2.75 2.82 2.81 2.83 2.78 3.87 3.89 3.88 3.86 3.89 [3.59 .. 3.62] 20.20 20.20 20.00 20.40 19.70 20.40 21.00 20.10 19.70 20.20 10.10 10.10 10.20 10.20 10.10 10.10 10.10 10.10 10.10 10.20 13.20 13.30 13.40 13.40 13.10 [3.62 .. 3.66] 23.10 23.00 23.00 23.20 22.70 23.20 23.20 23.10 23.00 23.10 9.40 9.48 9.47 9.57 9.39 9.39 9.30 9.30 9.31 9.47 13.60 13.80 13.80 13.90 13.60 [3.66 .. 3.68] 19.20 19.20 19.30 19.50 18.90 19.40 19.50 19.20 19.10 19.40 6.30 6.50 6.64 6.72 6.36 6.41 6.30 6.29 6.24 6.67 10.20 10.60 10.60 10.70 10.10 [3.68 .. 3.74] 44.30 44.40 44.40 44.70 43.80 44.30 43.80 44.60 44.70 44.40 126.00 125.00 126.00 125.00 126.00 126.00 126.00 126.00 126.00 125.00 100.00 99.70 100.00 99.60 99.80 [3.74 .. 3.80] 37.30 37.50 37.20 37.70 36.80 37.20 36.50 37.90 37.80 37.40 50.10 49.40 49.50 49.20 50.10 49.80 50.00 49.90 50.10 49.10 46.50 45.50 45.40 45.20 46.40 [3.80 .. 3.85] 33.00 33.50 32.90 33.80 32.50 32.80 32.40 34.00 33.50 33.30 86.40 85.80 86.10 85.60 86.70 86.40 86.60 86.40 86.70 85.40 70.20 69.00 69.10 68.70 69.80 [3.85 .. 3.91] 29.60 30.30 29.10 30.30 29.00 29.40 29.00 30.90 30.10 29.80 74.80 74.00 74.00 73.30 74.90 74.40 74.90 74.60 75.00 73.70 61.30 59.90 60.00 59.20 61.10 [3.91 .. 3.97] 39.60 40.30 39.50 40.40 39.10 39.50 38.90 40.80 40.20 39.90 19.70 18.90 18.90 18.30 19.60 19.30 19.80 19.80 19.90 18.70 26.70 25.40 25.30 24.50 26.80 [3.97 .. 4.02] 14.90 15.60 13.90 15.60 14.20 14.60 14.40 16.50 15.30 15.00 7.05 6.63 6.46 6.29 6.95 6.80 7.03 7.04 7.11 6.56 9.95 9.31 9.18 8.82 10.10 [4.02 .. 4.08] 67.40 67.80 68.40 68.30 67.80 66.50 65.60 68.50 68.30 68.10 23.10 22.60 22.40 22.10 22.90 22.60 22.90 23.00 23.00 22.50 37.60 36.80 36.80 35.90 37.70 [4.08 .. 4.12] 8.99 10.20 8.42 10.20 8.69 8.35 7.38 11.20 10.10 9.45 3.72 3.39 3.38 3.19 3.69 3.58 3.81 3.77 3.79 3.39 5.87 5.22 5.16 4.79 6.02 [4.12 .. 4.16] 6.11 7.02 5.47 6.96 5.75 5.67 5.30 7.83 6.76 6.41 2.65 2.43 2.41 2.30 2.63 2.56 2.71 2.68 2.72 2.47 4.07 3.67 3.63 3.38 4.17 [4.16 .. 4.21] 8.76 10.30 7.30 10.20 7.92 7.99 7.34 11.90 9.78 9.17 3.78 3.47 3.37 3.25 3.74 3.60 3.83 3.81 3.85 3.50 5.83 5.27 5.15 4.81 6.03 [4.21 .. 4.23] 1.58 2.12 0.92 2.07 1.20 1.28 1.18 2.77 1.84 1.69 0.66 0.58 0.56 0.52 0.66 0.62 0.70 0.68 0.70 0.60 1.09 0.94 0.89 0.79 1.17 [4.23 .. 4.25] 1.43 1.87 0.89 1.86 1.11 1.22 1.15 2.41 1.60 1.54 0.68 0.61 0.61 0.57 0.69 0.66 0.71 0.69 0.70 0.64 1.02 0.91 0.87 0.79 1.07 [6.50 .. 6.56] 0.65 0.22 1.37 0.12 1.36 0.67 0.32 0.00 0.72 0.52 0.24 0.18 0.16 0.13 0.18 0.21 0.23 0.26 0.24 0.18 0.41 0.25 0.25 0.25 0.47 [6.56 .. 6.61] 0.69 0.35 1.35 0.26 1.34 0.78 0.54 0.00 0.83 0.59 0.24 0.21 0.19 0.17 0.21 0.24 0.25 0.27 0.26 0.22 0.43 0.32 0.31 0.32 0.46 [6.61 .. 6.65] 0.94 0.67 1.26 0.66 1.24 0.95 0.82 0.42 0.95 0.83 0.24 0.25 0.23 0.21 0.24 0.24 0.26 0.28 0.26 0.23 0.46 0.40 0.42 0.42 0.50 [6.65 .. 6.68] 0.71 0.43 1.08 0.33 1.07 0.72 0.53 0.10 0.71 0.60 0.27 0.24 0.24 0.24 0.25 0.26 0.27 0.29 0.28 0.26 0.43 0.36 0.36 0.36 0.45 [6.68 .. 6.72] 0.41 0.15 0.79 0.07 0.75 0.39 0.30 0.00 0.42 0.32 0.15 0.12 0.13 0.12 0.12 0.15 0.15 0.16 0.15 0.14 0.24 0.19 0.19 0.18 0.28 [6.72 .. 6.74] 0.24 0.06 0.40 0.00 0.39 0.21 0.16 0.00 0.19 0.14 0.08 0.06 0.07 0.06 0.06 0.07 0.08 0.07 0.08 0.07 0.11 0.10 0.08 0.10 0.13 [6.74 .. 6.80] 1.17 0.72 1.69 0.62 1.69 1.18 1.10 0.25 1.11 0.95 0.41 0.39 0.41 0.42 0.39 0.43 0.42 0.46 0.44 0.44 0.65 0.62 0.63 0.63 0.74 [6.80 .. 6.82] 0.40 0.17 0.57 0.16 0.61 0.41 0.40 0.00 0.39 0.29 0.12 0.11 0.12 0.11 0.11 0.12 0.12 0.12 0.13 0.13 0.18 0.19 0.19 0.18 0.22 [6.82 .. 6.87] 2.26 1.77 2.63 1.74 2.67 2.25 2.23 1.36 2.08 2.04 0.71 0.70 0.71 0.71 0.68 0.70 0.73 0.74 0.74 0.73 1.17 1.16 1.14 1.16 1.21 [6.87 .. 6.92] 2.11 1.66 2.44 1.65 2.42 2.09 2.01 1.34 2.00 1.94 0.76 0.77 0.77 0.76 0.73 0.74 0.76 0.79 0.76 0.78 1.16 1.15 1.11 1.15 1.19 [6.92 .. 6.94] 0.61 0.43 0.77 0.43 0.76 0.64 0.63 0.28 0.56 0.58 0.24 0.24 0.26 0.25 0.22 0.24 0.25 0.26 0.23 0.25 0.34 0.35 0.35 0.36 0.36 [6.94 .. 6.98] 2.40 2.05 2.74 2.01 2.71 2.47 2.39 1.71 2.28 2.25 0.92 0.91 0.92 0.93 0.86 0.89 0.90 0.92 0.90 0.93 1.35 1.33 1.36 1.38 1.37 [6.98 .. 7.03] 2.38 2.03 2.75 1.96 2.76 2.46 2.41 1.74 2.34 2.27 2.18 2.18 2.18 2.16 2.15 2.17 2.18 2.19 2.19 2.18 2.22 2.21 2.20 2.23 2.25 [7.03 .. 7.05] 1.04 0.77 1.12 0.74 1.17 1.03 1.05 0.62 0.91 0.92 0.48 0.47 0.48 0.48 0.46 0.47 0.49 0.50 0.48 0.49 0.62 0.63 0.62 0.64 0.63 [7.05 .. 7.10] 4.62 4.25 4.98 4.15 4.97 4.71 4.66 3.84 4.48 4.44 1.35 1.35 1.35 1.35 1.32 1.33 1.34 1.36 1.37 1.37 2.34 2.34 2.35 2.40 2.38 [7.10 .. 7.12] 0.69 0.52 0.80 0.51 0.84 0.69 0.68 0.41 0.65 0.61 0.22 0.22 0.23 0.24 0.20 0.23 0.21 0.22 0.22 0.24 0.34 0.37 0.38 0.38 0.35 [7.12 .. 7.17] 4.56 4.20 4.98 4.13 4.96 4.66 4.60 3.80 4.44 4.45 3.20 3.18 3.20 3.17 3.16 3.18 3.18 3.20 3.19 3.19 3.57 3.58 3.57 3.61 3.60 [7.17 .. 7.21] 4.76 4.47 5.18 4.47 5.17 4.87 4.76 4.11 4.73 4.68 1.86 1.86 1.86 1.85 1.84 1.85 1.85 1.89 1.87 1.86 2.78 2.77 2.76 2.73 2.79 [7.21 .. 7.23] 1.41 1.29 1.62 1.26 1.60 1.42 1.41 1.15 1.42 1.38 0.64 0.64 0.64 0.63 0.62 0.64 0.63 0.64 0.64 0.64 0.85 0.87 0.86 0.87 0.89 [7.23 .. 7.29] 6.25 5.79 6.67 5.80 6.71 6.33 6.30 5.33 6.11 6.06 2.46 2.45 2.45 2.47 2.40 2.42 2.44 2.45 2.45 2.47 3.61 3.61 3.63 3.66 3.62 [7.29 .. 7.33] 4.13 3.77 4.37 3.79 4.35 4.17 4.22 3.51 4.01 3.97 1.92 1.94 1.96 1.98 1.91 1.92 1.92 1.94 1.93 1.96 2.56 2.61 2.61 2.65 2.61 [7.33 .. 7.39] 10.90 10.60 11.70 10.70 11.60 10.90 10.20 10.20 11.20 11.00 5.93 5.90 5.86 5.81 5.90 5.93 5.94 5.96 5.95 5.86 7.63 7.39 7.42 7.35 7.61 [7.39 .. 7.43] 4.98 4.82 5.46 4.86 5.44 5.00 4.64 4.56 5.14 5.01 2.35 2.35 2.36 2.31 2.34 2.36 2.39 2.39 2.37 2.36 3.24 3.12 3.17 3.09 3.26 [7.43 .. 7.48] 2.86 2.80 3.41 2.71 3.46 2.88 2.61 2.55 3.12 2.94 2.84 2.81 2.81 2.76 2.82 2.83 2.86 2.87 2.87 2.79 2.94 2.77 2.83 2.77 2.96 [7.48 .. 7.51] 1.31 1.18 1.47 1.16 1.56 1.35 1.32 1.02 1.31 1.25 0.71 0.70 0.68 0.67 0.70 0.70 0.72 0.70 0.70 0.69 0.93 0.87 0.87 0.89 0.94 [7.51 .. 7.57] 12.00 11.80 12.80 11.80 12.70 12.10 11.50 11.40 12.20 12.10 6.23 6.17 6.16 6.07 6.18 6.20 6.22 6.22 6.23 6.15 8.13 7.91 7.97 7.86 8.15 [7.57 .. 7.59] 0.39 0.45 0.71 0.37 0.75 0.39 0.12 0.34 0.60 0.48 0.24 0.20 0.19 0.15 0.23 0.24 0.26 0.24 0.25 0.19 0.38 0.24 0.25 0.20 0.37 [7.59 .. 7.65] 5.58 5.50 6.27 5.50 6.31 5.61 5.10 5.21 5.85 5.70 2.94 2.88 2.89 2.83 2.92 2.92 2.95 2.95 2.96 2.88 3.86 3.70 3.71 3.63 3.88 [7.65 .. 7.71] 3.14 3.16 3.82 3.12 3.89 3.19 2.63 2.91 3.50 3.30 1.13 1.04 1.05 0.97 1.08 1.11 1.13 1.15 1.15 1.03 1.91 1.67 1.70 1.60 1.91 [7.71 .. 7.76] 1.42 1.37 1.82 1.24 2.04 1.39 1.12 1.11 1.58 1.47 0.44 0.42 0.43 0.38 0.43 0.44 0.44 0.45 0.47 0.40 0.80 0.69 0.68 0.70 0.86 [7.76 .. 7.80] 0.85 0.60 0.95 0.59 1.09 0.87 0.96 0.46 0.70 0.71 1.00 1.01 1.03 1.02 0.96 1.00 0.99 1.01 0.99 1.05 0.90 0.93 0.97 0.97 0.93 [7.80 .. 7.85] 11.60 11.60 12.50 11.60 12.30 11.70 10.90 11.20 12.00 11.80 6.09 6.07 6.03 5.93 6.09 6.11 6.11 6.14 6.13 6.01 7.99 7.71 7.81 7.64 8.00 [7.85 .. 7.91] 2.29 2.49 3.05 2.43 3.13 2.28 1.60 2.29 2.80 2.60 0.86 0.81 0.79 0.67 0.85 0.88 0.90 0.90 0.90 0.77 1.54 1.23 1.27 1.15 1.58 [7.91 .. 7.93] 0.55 0.63 0.87 0.58 0.93 0.57 0.29 0.53 0.76 0.64 0.29 0.27 0.26 0.23 0.28 0.29 0.30 0.30 0.29 0.25 0.44 0.33 0.35 0.31 0.47 [7.93 .. 7.99] 2.66 2.73 3.21 2.67 3.35 2.70 2.24 2.52 2.97 2.83 0.91 0.85 0.85 0.77 0.89 0.91 0.91 0.91 0.92 0.82 1.59 1.36 1.42 1.36 1.65 [7.99 .. 8.05] 2.01 2.11 2.48 2.08 2.74 1.99 1.49 1.88 2.28 2.21 0.92 0.92 0.89 0.82 0.90 0.93 0.94 0.97 0.95 0.90 1.39 1.19 1.24 1.18 1.44 [8.05 .. 8.11] 1.55 1.64 2.09 1.63 2.27 1.52 1.02 1.48 1.93 1.72 0.66 0.62 0.61 0.53 0.62 0.67 0.68 0.68 0.71 0.60 1.07 0.86 0.89 0.85 1.15 [8.11 .. 8.15] 0.47 0.55 0.87 0.53 1.02 0.50 0.14 0.48 0.74 0.62 0.22 0.18 0.20 0.13 0.19 0.21 0.23 0.22 0.24 0.18 0.37 0.25 0.27 0.23 0.43 [8.15 .. 8.21] 0.65 0.67 0.99 0.62 1.22 0.60 0.34 0.55 0.84 0.74 0.32 0.27 0.30 0.22 0.29 0.31 0.32 0.33 0.33 0.29 0.48 0.37 0.39 0.34 0.55 [8.21 .. 8.24] 0.23 0.28 0.45 0.27 0.62 0.24 0.07 0.19 0.41 0.33 0.12 0.10 0.10 0.07 0.10 0.13 0.13 0.12 0.14 0.10 0.20 0.13 0.14 0.13 0.24 [8.24 .. 8.28] 0.34 0.34 0.59 0.30 0.78 0.34 0.09 0.28 0.47 0.41 0.19 0.17 0.17 0.14 0.17 0.19 0.20 0.19 0.19 0.18 0.27 0.17 0.19 0.17 0.29 [8.28 .. 8.31] 0.33 0.35 0.51 0.30 0.66 0.35 0.20 0.25 0.46 0.39 0.15 0.14 0.15 0.13 0.15 0.15 0.18 0.16 0.17 0.14 0.22 0.18 0.20 0.20 0.26 [8.31 .. 8.37] 0.81 0.81 1.17 0.78 1.40 0.79 0.55 0.72 0.99 0.92 0.31 0.29 0.30 0.25 0.29 0.32 0.35 0.32 0.32 0.28 0.57 0.42 0.47 0.43 0.62 [8.37 .. 8.42] 0.31 0.34 0.60 0.27 0.83 0.28 0.10 0.16 0.45 0.37 0.13 0.10 0.13 0.06 0.12 0.14 0.15 0.15 0.15 0.12 0.22 0.12 0.16 0.15 0.27 [8.42 .. 8.46] 0.62 0.61 0.80 0.59 0.99 0.64 0.47 0.52 0.72 0.64 0.20 0.20 0.20 0.18 0.19 0.20 0.22 0.22 0.20 0.20 0.35 0.29 0.31 0.31 0.39 [8.46 .. 8.48] 0.11 0.12 0.22 0.11 0.38 0.11 0.01 0.07 0.19 0.15 0.04 0.04 0.05 0.03 0.04 0.05 0.05 0.05 0.06 0.03 0.09 0.05 0.05 0.06 0.12 [8.48 .. 8.53] 0.56 0.59 0.75 0.50 1.02 0.57 0.41 0.46 0.63 0.65 0.16 0.16 0.17 0.13 0.16 0.18 0.18 0.16 0.16 0.16 0.30 0.25 0.29 0.28 0.38 [8.53 .. 8.59] 0.93 0.97 1.22 0.92 1.52 0.96 0.67 0.91 1.04 1.05 0.45 0.43 0.43 0.40 0.41 0.47 0.46 0.44 0.44 0.43 0.65 0.54 0.59 0.58 0.70 [8.59 .. 8.62] 0.07 0.12 0.24 0.10 0.33 0.09 0.00 0.06 0.15 0.13 0.07 0.04 0.05 0.02 0.04 0.06 0.05 0.06 0.06 0.05 0.09 0.05 0.06 0.06 0.13 [8.62 .. 8.66] 0.23 0.26 0.38 0.18 0.60 0.23 0.06 0.13 0.31 0.25 0.06 0.05 0.08 0.03 0.04 0.07 0.08 0.08 0.07 0.07 0.14 0.09 0.08 0.10 0.17 [8.66 .. 8.72] 0.13 0.19 0.43 0.10 0.68 0.16 0.00 0.02 0.24 0.16 0.08 0.07 0.08 0.06 0.03 0.09 0.08 0.09 0.09 0.09 0.14 0.07 0.06 0.07 0.20 [8.72 .. 8.76] 0.07 0.07 0.20 0.00 0.45 0.08 0.00 0.00 0.09 0.11 0.05 0.04 0.05 0.03 0.04 0.06 0.05 0.06 0.04 0.04 0.07 0.04 0.04 0.04 0.11 [8.76 .. 8.81] 0.42 0.42 0.61 0.35 0.82 0.45 0.36 0.30 0.47 0.41 0.15 0.15 0.17 0.12 0.11 0.14 0.14 0.17 0.13 0.16 0.25 0.20 0.23 0.23 0.28 [8.81 .. 8.86] 1.29 1.39 1.57 1.32 1.86 1.34 1.13 1.26 1.44 1.37 0.58 0.58 0.61 0.56 0.57 0.59 0.59 0.60 0.61 0.60 0.83 0.79 0.81 0.80 0.90 [8.86 .. 8.91] 0.08 0.14 0.26 0.11 0.51 0.12 0.00 0.04 0.20 0.13 0.05 0.05 0.08 0.03 0.05 0.06 0.07 0.08 0.07 0.07 0.11 0.07 0.06 0.09 0.16 [8.91 .. 8.94] 0.05 0.05 0.12 0.01 0.35 0.02 0.00 0.02 0.09 0.05 0.03 0.02 0.04 0.01 0.01 0.03 0.02 0.03 0.03 0.02 0.04 0.01 0.01 0.05 0.06 [8.94 .. 9.00] 0.09 0.19 0.30 0.09 0.62 0.12 0.03 0.06 0.24 0.17 0.06 0.07 0.10 0.06 0.05 0.06 0.07 0.08 0.07 0.08 0.13 0.08 0.07 0.10 0.16 [9.00 .. 9.04] 0.06 0.04 0.14 0.01 0.33 0.05 0.00 0.01 0.05 0.05 0.02 0.01 0.06 0.02 0.02 0.02 0.03 0.01 0.03 0.03 0.04 0.00 0.03 0.03 0.08 [9.04 .. 9.08] 0.15 0.14 0.23 0.07 0.53 0.15 0.09 0.10 0.20 0.18 0.06 0.04 0.09 0.05 0.04 0.06 0.06 0.06 0.05 0.08 0.07 0.04 0.06 0.10 0.13 [9.08 .. 9.14] 0.72 0.76 0.84 0.66 1.24 0.72 0.67 0.65 0.75 0.73 0.29 0.30 0.33 0.28 0.24 0.32 0.29 0.29 0.30 0.30 0.42 0.39 0.41 0.44 0.52 [9.14 .. 9.18] 0.02 0.06 0.15 0.03 0.42 0.01 0.00 0.00 0.07 0.08 0.02 0.03 0.04 0.00 0.00 0.03 0.03 0.02 0.03 0.04 0.04 0.00 0.00 0.04 0.09 [9.18 .. 9.24] 0.00 0.05 0.13 0.01 0.54 0.00 0.00 0.01 0.05 0.05 0.03 0.03 0.07 0.02 0.00 0.02 0.04 0.03 0.02 0.03 0.02 0.01 0.00 0.03 0.06 [9.24 .. 9.30] 0.07 0.13 0.15 0.04 0.62 0.09 0.08 0.13 0.16 0.15 0.05 0.06 0.08 0.04 0.01 0.07 0.05 0.06 0.06 0.09 0.06 0.03 0.04 0.10 0.12 [9.30 .. 9.32] 0.00 0.03 0.03 0.00 0.19 0.01 0.00 0.00 0.02 0.01 0.00 0.01 0.02 0.00 0.00 0.00 0.01 0.00 0.01 0.01 0.00 0.00 0.00 0.02 0.02 [9.32 .. 9.37] 0.02 0.10 0.11 0.05 0.50 0.07 0.03 0.00 0.06 0.06 0.02 0.02 0.08 0.04 0.00 0.03 0.05 0.03 0.05 0.03 0.04 0.01 0.03 0.06 0.09 [9.37 .. 9.40] 0.00 0.01 0.01 0.00 0.21 0.00 0.00 0.00 0.00 0.05 0.00 0.01 0.03 0.01 0.00 0.02 0.02 0.00 0.01 0.01 0.01 0.00 0.01 0.03 0.04 [9.40 .. 9.45] 0.00 0.06 0.07 0.00 0.43 0.00 0.01 0.04 0.00 0.03 0.01 0.01 0.06 0.01 0.00 0.02 0.02 0.00 0.00 0.03 0.00 0.00 0.03 0.04 0.05 [9.45 .. 9.48] 0.01 0.00 0.01 0.00 0.14 0.00 0.01 0.00 0.00 0.00 0.00 0.00 0.03 0.01 0.00 0.01 0.01 0.00 0.00 0.01 0.00 0.00 0.00 0.02 0.03 [9.48 .. 9.50] 0.02 0.00 0.04 0.00 0.17 0.02 0.02 0.00 0.01 0.02 0.00 0.01 0.02 0.01 0.00 0.00 0.01 0.00 0.00 0.02 0.00 0.00 0.00 0.02 0.02 NMR_BINNED_DATA_END #END