#METABOLOMICS WORKBENCH douglas_walker_20180821_140312 DATATRACK_ID:1480 STUDY_ID:ST001040 ANALYSIS_ID:AN001702 PROJECT_ID:PR000696
VERSION             	1
CREATED_ON             	August 22, 2018, 4:03 pm
#PROJECT
PR:PROJECT_TITLE                 	Pregnancy Eating and Postpartum Diapers (PEAPOD)
PR:PROJECT_TYPE                  	Pilot Study
PR:PROJECT_SUMMARY               	This was a pilot study (n=27), to assess the feasibility, acceptability, and
PR:PROJECT_SUMMARY               	preliminary efficacy of implementing a randomized controlled trial of a diet
PR:PROJECT_SUMMARY               	intervention in pregnancy designed to test the effect of maternal diet on the
PR:PROJECT_SUMMARY               	maternal and infant gut microbiome. Our specific aims were to: 1) test
PR:PROJECT_SUMMARY               	feasibility of enrollment and implementation; 2) assess acceptability of weekly
PR:PROJECT_SUMMARY               	food deliveries; and 3) estimate the preliminary effect size of the intervention
PR:PROJECT_SUMMARY               	relative to the usual care group on (a) maternal gut butyrate composition
PR:PROJECT_SUMMARY               	measured in three maternal stool samples collected at two time points during
PR:PROJECT_SUMMARY               	pregnancy (pre- and post-diet intervention phase) and also collected at 6 weeks
PR:PROJECT_SUMMARY               	postpartum; and (b) infant gut butyrate composition measured in infant stool
PR:PROJECT_SUMMARY               	samples collected at 6 weeks of age. The overall goal of PEAPOD was to gather
PR:PROJECT_SUMMARY               	pilot data to effectively refine the intervention so that it can be tested in a
PR:PROJECT_SUMMARY               	larger, longer study using a factorial design. For this pilot, we employed a
PR:PROJECT_SUMMARY               	2-arm RCT with a total sample size of 27 mother-child pairs. We enrolled women
PR:PROJECT_SUMMARY               	in mid-pregnancy who were intending to breastfeed, randomized them to the diet
PR:PROJECT_SUMMARY               	intervention (n=13) or to a usual care group (n=14) and followed them to 6 weeks
PR:PROJECT_SUMMARY               	postpartum. Data collection included surveys of detailed maternal dietary
PR:PROJECT_SUMMARY               	information, as well as collection of maternal blood, urine, and stool at three
PR:PROJECT_SUMMARY               	time points (25 and 36 weeks gestation, and 6 weeks postpartum), and an infant
PR:PROJECT_SUMMARY               	stool sample at 6 weeks of age along with information about infant feeding
PR:PROJECT_SUMMARY               	practices. The diet intervention was initiated at 32 weeks gestation and
PR:PROJECT_SUMMARY               	continued until birth of the baby; thus the 25 week gestation biospecimens are
PR:PROJECT_SUMMARY               	pre-intervention and the 36 week gestation biospecimens are after 4 weeks of
PR:PROJECT_SUMMARY               	receiving the diet intervention. We chose to collect the second set of
PR:PROJECT_SUMMARY               	biospecimens at 36 weeks gestation to avoid missing post-intervention samples in
PR:PROJECT_SUMMARY               	instances where women delivered preterm. We partnered with the hospital catering
PR:PROJECT_SUMMARY               	service and the diet intervention including either legumes (e.g. minestrone with
PR:PROJECT_SUMMARY               	white beans) or whole grains (e.g. beef barley), and 5 pieces of fresh fruit
PR:PROJECT_SUMMARY               	(e.g. apples, oranges). In addition, in the first week, participants received a
PR:PROJECT_SUMMARY               	collection of non-perishable high fiber foods (whole wheat breakfast cereal,
PR:PROJECT_SUMMARY               	oatmeal, dried fruit, and canned beans) as well as upscale olive oil and vinegar
PR:PROJECT_SUMMARY               	from a local store along with recipes for salad dressing, side dishes, and some
PR:PROJECT_SUMMARY               	general information about the health benefits of the Mediterranean diet. We
PR:PROJECT_SUMMARY               	anticipated that participants would likely share the food with their families
PR:PROJECT_SUMMARY               	but our intent was to provide enough supplementary food to increase the fiber
PR:PROJECT_SUMMARY               	consumption of the pregnant women.
PR:INSTITUTE                     	Michigan State University
PR:DEPARTMENT                    	Department of Epidemiology and Biostatistics
PR:LAST_NAME                     	Kerver
PR:FIRST_NAME                    	Jean
PR:ADDRESS                       	314 Munson Professional Building, MSU/CHM Research, 1105 Sixth Street, Traverse
PR:ADDRESS                       	City, MI 49684
PR:EMAIL                         	kerverje@msu.edu
PR:PHONE                         	231-392-8227
PR:CONTRIBUTORS                  	Jean Kerver, Sarah Comstock, Joseph Gardiner, Robert Wright, Lauren Petrick,
PR:CONTRIBUTORS                  	Douglas Walker
#STUDY
ST:STUDY_TITLE                   	Maternal gut microbiome, pregnancy exposure to environmental contaminants, and
ST:STUDY_TITLE                   	child health outcomes: A pilot study exploring potential effect modifications by
ST:STUDY_TITLE                   	diet
ST:STUDY_TYPE                    	CHEAR Pilot Study
ST:STUDY_SUMMARY                 	Using specimens collected as part of a pilot RCT of a diet intervention in
ST:STUDY_SUMMARY                 	pregnancy, we propose to ship our time 2 blood and urine samples (collected
ST:STUDY_SUMMARY                 	post-diet intervention or usual care at 36 weeks gestation) to: 1) Assess
ST:STUDY_SUMMARY                 	biomarker confirmation of the diet intervention effect via: (a) carotenoids
ST:STUDY_SUMMARY                 	and/or other antioxidants (which have been shown to be a good marker of fruit
ST:STUDY_SUMMARY                 	and vegetable intake); and (b) untargeted metabolomics. 2) Assess pregnancy
ST:STUDY_SUMMARY                 	exposure to metals and/or other environmental contaminants. 3) Combine the
ST:STUDY_SUMMARY                 	biomarker data proposed here in aims 1 and 2 with the data being analyzed at MSU
ST:STUDY_SUMMARY                 	(diet survey data and butyrate composition of stool) to explore potential
ST:STUDY_SUMMARY                 	bi-directional effects on gut microbiome, environmental contaminants, and
ST:STUDY_SUMMARY                 	dietary factors.
ST:INSTITUTE                     	Icahn School of Medicine at Mount Sinai
ST:DEPARTMENT                    	Department of Environmental Medicine and Public Health
ST:LABORATORY                    	Mount Sinai CHEAR Untargeted Laboratory Hub
ST:LAST_NAME                     	Walker
ST:FIRST_NAME                    	Douglas
ST:ADDRESS                       	Atran Building RM AB3-39, 1428 Madison Ave
ST:EMAIL                         	douglas.walker@mssm.edu
ST:PHONE                         	212-241-4392
ST:TOTAL_SUBJECTS                	26
#SUBJECT
SU:SUBJECT_TYPE                  	Human
SU:SUBJECT_SPECIES               	Homo sapiens
SU:TAXONOMY_ID                   	9606
#SUBJECT_SAMPLE_FACTORS:         	SUBJECT(optional)[tab]SAMPLE[tab]FACTORS(NAME:VALUE pairs separated by |)[tab]Additional sample data
SUBJECT_SAMPLE_FACTORS           	-	LQC_1	Sample Type/Matrix:Pooled quality control sample	Project ID=2018-PF05 (Kerver); LIMS ID=NA; Readings SpG=NA; Dilution Factor=NA; ZHP run order=23; RPN run order=23
SUBJECT_SAMPLE_FACTORS           	-	LQC_2	Sample Type/Matrix:Pooled quality control sample	Project ID=2018-PF05 (Kerver); LIMS ID=NA; Readings SpG=NA; Dilution Factor=NA; ZHP run order=24; RPN run order=24
SUBJECT_SAMPLE_FACTORS           	-	LQC_3	Sample Type/Matrix:Pooled quality control sample	Project ID=2018-PF05 (Kerver); LIMS ID=NA; Readings SpG=NA; Dilution Factor=NA; ZHP run order=35; RPN run order=35
SUBJECT_SAMPLE_FACTORS           	-	LQC_4	Sample Type/Matrix:Pooled quality control sample	Project ID=2018-PF05 (Kerver); LIMS ID=NA; Readings SpG=NA; Dilution Factor=NA; ZHP run order=46; RPN run order=46
SUBJECT_SAMPLE_FACTORS           	-	LQC_5	Sample Type/Matrix:Pooled quality control sample	Project ID=2018-PF05 (Kerver); LIMS ID=NA; Readings SpG=NA; Dilution Factor=NA; ZHP run order=53; RPN run order=53
SUBJECT_SAMPLE_FACTORS           	-	matrix_1	Sample Type/Matrix:Water matrix blank	Project ID=2018-PF05 (Kerver); LIMS ID=NA; Readings SpG=NA; Dilution Factor=NA; ZHP run order=14; RPN run order=14
SUBJECT_SAMPLE_FACTORS           	-	matrix_2	Sample Type/Matrix:Water matrix blank	Project ID=2018-PF05 (Kerver); LIMS ID=NA; Readings SpG=NA; Dilution Factor=NA; ZHP run order=15; RPN run order=15
SUBJECT_SAMPLE_FACTORS           	-	matrix_3	Sample Type/Matrix:Water matrix blank	Project ID=2018-PF05 (Kerver); LIMS ID=NA; Readings SpG=NA; Dilution Factor=NA; ZHP run order=16; RPN run order=16
SUBJECT_SAMPLE_FACTORS           	-	TCPP1	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0001; Readings SpG=1.0118; Dilution Factor=5.130434783; ZHP run order=25; RPN run order=25
SUBJECT_SAMPLE_FACTORS           	-	TCPP2	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0002; Readings SpG=1.0153; Dilution Factor=6.652173913; ZHP run order=26; RPN run order=26
SUBJECT_SAMPLE_FACTORS           	-	TCPP3	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0003; Readings SpG=1.0062; Dilution Factor=2.695652174; ZHP run order=27; RPN run order=27
SUBJECT_SAMPLE_FACTORS           	-	TCPP4	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0004; Readings SpG=1.0054; Dilution Factor=2.347826087; ZHP run order=28; RPN run order=28
SUBJECT_SAMPLE_FACTORS           	-	TCPP5	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0005; Readings SpG=1.0074; Dilution Factor=3.217391304; ZHP run order=29; RPN run order=29
SUBJECT_SAMPLE_FACTORS           	-	TCPP6	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0006; Readings SpG=1.0231; Dilution Factor=10.04347826; ZHP run order=30; RPN run order=30
SUBJECT_SAMPLE_FACTORS           	-	TCPP8	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0007; Readings SpG=1.0226; Dilution Factor=9.826086957; ZHP run order=31; RPN run order=31
SUBJECT_SAMPLE_FACTORS           	-	TCPP10	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0008; Readings SpG=1.0256; Dilution Factor=11.13043478; ZHP run order=32; RPN run order=32
SUBJECT_SAMPLE_FACTORS           	-	TCPP11	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0009; Readings SpG=1.0082; Dilution Factor=3.565217391; ZHP run order=33; RPN run order=33
SUBJECT_SAMPLE_FACTORS           	-	TCPP12	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0010; Readings SpG=1.0023; Dilution Factor=1; ZHP run order=34; RPN run order=34
SUBJECT_SAMPLE_FACTORS           	-	TCPP13	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0011; Readings SpG=1.0057; Dilution Factor=2.47826087; ZHP run order=36; RPN run order=36
SUBJECT_SAMPLE_FACTORS           	-	TCPP15	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0012; Readings SpG=1.0086; Dilution Factor=3.739130435; ZHP run order=37; RPN run order=37
SUBJECT_SAMPLE_FACTORS           	-	TCPP16	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0013; Readings SpG=1.0088; Dilution Factor=3.826086957; ZHP run order=38; RPN run order=38
SUBJECT_SAMPLE_FACTORS           	-	TCPP17	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0014; Readings SpG=1.0199; Dilution Factor=8.652173913; ZHP run order=39; RPN run order=39
SUBJECT_SAMPLE_FACTORS           	-	TCPP18	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0015; Readings SpG=1.0044; Dilution Factor=1.913043478; ZHP run order=40; RPN run order=40
SUBJECT_SAMPLE_FACTORS           	-	TCPP19	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0016; Readings SpG=1.0091; Dilution Factor=3.956521739; ZHP run order=41; RPN run order=41
SUBJECT_SAMPLE_FACTORS           	-	TCPP20	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0017; Readings SpG=1.0177; Dilution Factor=7.695652174; ZHP run order=42; RPN run order=42
SUBJECT_SAMPLE_FACTORS           	-	TCPP21	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0018; Readings SpG=1.0089; Dilution Factor=3.869565217; ZHP run order=43; RPN run order=43
SUBJECT_SAMPLE_FACTORS           	-	TCPP22	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0019; Readings SpG=1.0268; Dilution Factor=11.65217391; ZHP run order=44; RPN run order=44
SUBJECT_SAMPLE_FACTORS           	-	TCPP23	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0020; Readings SpG=1.0076; Dilution Factor=3.304347826; ZHP run order=45; RPN run order=45
SUBJECT_SAMPLE_FACTORS           	-	TCPP24	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0021; Readings SpG=1.0098; Dilution Factor=4.260869565; ZHP run order=47; RPN run order=47
SUBJECT_SAMPLE_FACTORS           	-	TCPP25	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0022; Readings SpG=1.0082; Dilution Factor=3.565217391; ZHP run order=48; RPN run order=48
SUBJECT_SAMPLE_FACTORS           	-	TCPP26	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0023; Readings SpG=1.0177; Dilution Factor=7.695652174; ZHP run order=49; RPN run order=49
SUBJECT_SAMPLE_FACTORS           	-	TCPP27	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0024; Readings SpG=1.0095; Dilution Factor=4.130434783; ZHP run order=50; RPN run order=50
SUBJECT_SAMPLE_FACTORS           	-	TCPP28	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0025; Readings SpG=1.0081; Dilution Factor=3.52173913; ZHP run order=51; RPN run order=51
SUBJECT_SAMPLE_FACTORS           	-	TCPP29	Sample Type/Matrix:urine	Project ID=2018-PF05 (Kerver); LIMS ID=18S071UR0026; Readings SpG=1.0025; Dilution Factor=1.086956522; ZHP run order=52; RPN run order=52
#COLLECTION
CO:COLLECTION_SUMMARY            	For this pilot, we employed a 2-arm RCT with a total sample size of 27
CO:COLLECTION_SUMMARY            	mother-child pairs. We enrolled women in mid-pregnancy who were intending to
CO:COLLECTION_SUMMARY            	breastfeed, randomized them to the diet intervention (n=13) or to a usual care
CO:COLLECTION_SUMMARY            	group (n=14) and followed them to 6 weeks postpartum. Data collection included
CO:COLLECTION_SUMMARY            	surveys of detailed maternal dietary information, as well as collection of
CO:COLLECTION_SUMMARY            	maternal blood, urine, and stool at three time points (25 and 36 weeks
CO:COLLECTION_SUMMARY            	gestation, and 6 weeks postpartum), and an infant stool sample at 6 weeks of age
CO:COLLECTION_SUMMARY            	along with information about infant feeding practices. The diet intervention was
CO:COLLECTION_SUMMARY            	initiated at 32 weeks gestation and continued until birth of the baby; thus the
CO:COLLECTION_SUMMARY            	25 week gestation biospecimens are pre-intervention and the 36 week gestation
CO:COLLECTION_SUMMARY            	biospecimens are after 4 weeks of receiving the diet intervention. We chose to
CO:COLLECTION_SUMMARY            	collect the second set of biospecimens at 36 weeks gestation to avoid missing
CO:COLLECTION_SUMMARY            	post-intervention samples in instances where women delivered preterm.
CO:SAMPLE_TYPE                   	Urine
#TREATMENT
TR:TREATMENT_SUMMARY             	We enrolled women in mid-pregnancy who were intending to breastfeed, randomized
TR:TREATMENT_SUMMARY             	them to the diet intervention (n=13) or to a usual care group (n=14) and
TR:TREATMENT_SUMMARY             	followed them to 6 weeks postpartum. We partnered with the hospital catering
TR:TREATMENT_SUMMARY             	service and the diet intervention consisted of weekly food delivery of 3 large
TR:TREATMENT_SUMMARY             	prepared salads (without dressing), 2 quarts of soup including either legumes
TR:TREATMENT_SUMMARY             	(e.g. minestrone with white beans) or whole grains (e.g. beef barley), and 5
TR:TREATMENT_SUMMARY             	pieces of fresh fruit (e.g. apples, oranges). In addition, in the first week,
TR:TREATMENT_SUMMARY             	participants received a collection of non-perishable high fiber foods (whole
TR:TREATMENT_SUMMARY             	wheat breakfast cereal, oatmeal, dried fruit, and canned beans) as well as
TR:TREATMENT_SUMMARY             	upscale olive oil and vinegar from a local store along with recipes for salad
TR:TREATMENT_SUMMARY             	dressing, side dishes, and some general information about the health benefits of
TR:TREATMENT_SUMMARY             	the Mediterranean diet.
#SAMPLEPREP
SP:SAMPLEPREP_SUMMARY            	Urine samples were thawed on ice, vortexed, and specific gravity (SpG) was
SP:SAMPLEPREP_SUMMARY            	measured. Samples were diluted with LC-MS grade water to the lowest measured SpG
SP:SAMPLEPREP_SUMMARY            	with ultrapure water. Aliquots of 20 μL of the diluted urine were prepared for
SP:SAMPLEPREP_SUMMARY            	analysis with the LC-HRMS. A third 20 μL aliquot from each sample was combined
SP:SAMPLEPREP_SUMMARY            	for use as a pooled quality control sample (‘LQC’). When aliquoting was
SP:SAMPLEPREP_SUMMARY            	complete, the LQC sample was re-aliquoted into 20μL samples. All aliquots were
SP:SAMPLEPREP_SUMMARY            	returned to -80°C until analysis. Extraction was performed immediately prior to
SP:SAMPLEPREP_SUMMARY            	LC-HRMS analysis. All sample aliquots were thawed on ice, combined with 180uL of
SP:SAMPLEPREP_SUMMARY            	acetonitrile containing internal standards. Samples were then centrifuged and
SP:SAMPLEPREP_SUMMARY            	80μL of supernatant transferred to an LC vial for analysis. Following the same
SP:SAMPLEPREP_SUMMARY            	protocol matrix blank (replacing the urine with H2O) and multiple LQCs were
SP:SAMPLEPREP_SUMMARY            	extracted.
SP:PROCESSING_STORAGE_CONDITIONS 	On ice
#CHROMATOGRAPHY
CH:CHROMATOGRAPHY_SUMMARY        	Sample extracts were analyzed using an ultra-high performance liquid
CH:CHROMATOGRAPHY_SUMMARY        	chromatography (UHPLC) 1290 Infinity II system (including 0.3 µm inline filter,
CH:CHROMATOGRAPHY_SUMMARY        	Agilent Technologies, Santa Clara, USA) with 1260 Infinity II isocratic pump
CH:CHROMATOGRAPHY_SUMMARY        	(including 1:100 splitter) coupled to a 6550 iFunnel quadrupole-time time of
CH:CHROMATOGRAPHY_SUMMARY        	flight (Q-TOF) mass spectrometer with a dual AJS electrospray ionization source
CH:CHROMATOGRAPHY_SUMMARY        	(Agilent Technologies, Santa Clara, USA). Samples were maintained at 5C in the
CH:CHROMATOGRAPHY_SUMMARY        	autosampler module. For polar metabolites separation, 2 uL of sample was
CH:CHROMATOGRAPHY_SUMMARY        	injected onto a HILIC SeQuant® ZIC®-HILIC column (100 mm × 2.1 mm, 100 Å,
CH:CHROMATOGRAPHY_SUMMARY        	3.5 µm particle size, Merck, Darmstadt, Germany) with a guard fitting (14 mm ×
CH:CHROMATOGRAPHY_SUMMARY        	1 mm, 5.0 µm particle size, Merck, Darmstadt, Germany) maintained at 25C.
CH:CHROMATOGRAPHY_SUMMARY        	Separation occurred using Mobile phase A consisted of water with 0.1% formic
CH:CHROMATOGRAPHY_SUMMARY        	acid and Mobile phase B consisted of Acetonitrile with 0.1% formic acid at a
CH:CHROMATOGRAPHY_SUMMARY        	flow rate of 0.3 ml/min as described in Table 1. Data was acquired with a mass
CH:CHROMATOGRAPHY_SUMMARY        	range of 40-1200 m/z. Solvent gradients were as follows: 95% solvent B, hold for
CH:CHROMATOGRAPHY_SUMMARY        	1.5 min; linear decrease to 40% solvent B at 12 minutes; hold for 2 min, linear
CH:CHROMATOGRAPHY_SUMMARY        	decrease to 25% solvent B at 14.2 min, hold for 2.8 min; increase to 95% solvent
CH:CHROMATOGRAPHY_SUMMARY        	B at 18 min, hold for 7 min.
CH:CHROMATOGRAPHY_TYPE           	HILIC
CH:INSTRUMENT_NAME               	Agilent 1290 Infinity II
CH:COLUMN_NAME                   	SeQuant ZIC- pHILIC (100 x 2.1mm, 3.5um)
CH:COLUMN_NAME                   	Merck, Darmstadt, Germany)
CH:FLOW_RATE                     	0.3 mL/min
CH:COLUMN_TEMPERATURE            	25C
CH:SOLVENT_A                     	Water with 0.1% formic acid
CH:SOLVENT_B                     	Acetonitrile with 0.1% formic acid
CH:ANALYTICAL_TIME               	25 min
#ANALYSIS
AN:DATA_FORMAT                   	.D
AN:ANALYSIS_TYPE                 	MS
#MS
MS:INSTRUMENT_NAME               	Agilent 6550 QTOF
MS:INSTRUMENT_TYPE               	QTOF
MS:MS_TYPE                       	ESI
MS:ION_MODE                      	POSITIVE
MS:CAPILLARY_TEMPERATURE         	250C
MS:CAPILLARY_VOLTAGE             	3000
MS:MS_RESULTS_FILE               	ST001040_AN001702_Results.txt	UNITS:Peak Intensity
#MS_METABOLITE_DATA
MS_METABOLITE_DATA:UNITS         	Peak Intensity
MS_METABOLITE_DATA_START
Samples	LQC_1	LQC_2	LQC_3	LQC_4	LQC_5	matrix_1	matrix_2	matrix_3	TCPP1	TCPP2	TCPP3	TCPP4	TCPP5	TCPP6	TCPP8	TCPP10	TCPP11	TCPP12	TCPP13	TCPP15	TCPP16	TCPP17	TCPP18	TCPP19	TCPP20	TCPP21	TCPP22	TCPP23	TCPP24	TCPP25	TCPP26	TCPP27	TCPP28	TCPP29
Factors	Sample Type/Matrix:Pooled quality control sample	Sample Type/Matrix:Pooled quality control sample	Sample Type/Matrix:Pooled quality control sample	Sample Type/Matrix:Pooled quality control sample	Sample Type/Matrix:Pooled quality control sample	Sample Type/Matrix:Water matrix blank	Sample Type/Matrix:Water matrix blank	Sample Type/Matrix:Water matrix blank	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine	Sample Type/Matrix:urine
3-(2-Hydroxyphenyl)Propanoate	111086.5886	115024.3243	114057.3392	116781.2779	113437.3537				102478.7304	102962.3426	116898.3864	79041.35655	108593.8848	48071.92134	238964.4084	90073.24745	69182.97309	173631.8051	125183.174	166102.383	105472.7601	126003.0357	97000.42714	132803.8324	53824.7189	128131.253	141135.5924	167655.6307	142464.6144	243910.3106	96982.81489	167230.8715	125140.5781	112090.1495
3-(4-Hydroxyphenyl)Pyruvate / Caffeate	3424.976626	2825.940541	3912.308601	3543.714373	3217.413779				10152.86724	7325.462247	12241.65082	7136.233681	6374.54404	3528.270548	14461.29177	7605.214453	5282.75396	11597.93044	7059.668762	15449.58555	6624.874999	7745.738558	5094.179123	11553.57691	3937.241606	10004.76823	11145.0758	18200.6443	12070.81772	10699.85806	5123.060749	9295.839832	14265.62526	12887.90477
Mevalolactone	7675.103679	11208.17126	12087.14167	9000.400408	9406.518195				12344.65498	17762.47788	11237.97683		12463.1206		11285.66504	12677.94426	10325.43764	76461.76701	12075.87158				16020.386	10598.64578						8260.644436	8156.401479	12548.92125	23915.81588	20643.9049
Cortisone	45112.6822	49933.97731	50102.70001	48381.46232	44140.12237				51116.79438	44718.12179	73056.1695	67247.61967	46261.00593	22627.9829	53709.69979	43763.25301	79709.98017	73733.24569	121590.3294	41236.96271	49133.52269	38516.84139	98947.23069	54664.55658	56017.01939	37512.64711	47647.58419	53444.92244	66507.84777	94372.56167	42547.10881	50075.13813	80003.61334	118411.8465
Methylpicolinate	12809.28279	13709.57144	12022.04264	16477.04205	11901.48537				6146.009735	19320.37232	25899.74311	11092.22002	8382.205751			24055.31337	10248.22658		5018.473623	17709.85497	11099.59402	10295.14307		10062.16322	25218.24612			24270.99063	41166.3246	6057.376691	14326.75242	8831.133853	10894.71414	17713.21174
N-Acetylphenylalanine	79655.47876	85814.91962	84780.45107	75928.91262	81205.91862				60027.06499	135976.5793	178608.159	51221.2796	212653.7999	97385.22642	138342.6364	75837.11399	200631.8326	32326.44464	29733.99312	47032.32385	22760.32486	30299.07962	55505.20928	38657.82586	73261.50304	35642.24474	82391.58382	101063.6485		45539.87623	55353.55609	92912.09586	40914.2368	77832.86626
Caffeine	4826946.722	4669362.038	4627793.671	4455830.01	4318022.007				5985032.52	104837.5007	14716688.83	256174.6402	186613.2572	335116.5273	1689116.509	469750.2613	2419802.971	16033775.33	3289100.164	1027125.435	5212202.368	65857.80256	21560254.2	1618349.446	765919.8559	504315.512	1256295.111	10946741.71	11812638.29	123765.0488	255008.021	4980155.796	1349108.857	13006844.31
Lumichrome	23549.87072	20118.00938	25690.78679	32245.2537	33901.96252				15520.17817	36924.29429	24808.27679	16439.21044	19347.58596				46769.35774	29866.72712	8517.765571	15915.15539	9132.472076	21461.61917	49674.56786	5687.587404	9114.370446	10597.57962	12859.77468			64855.43429			30366.67166	57960.56876
Indole-3-Acetate	68330.22526	57289.97914	60063.44075	57319.24639	57330.45944				56280.98683	148846.1781	49282.20234	97442.918	77923.68367	4624.455559	79001.81164	36200.16448	127010.5758	46671.26888	55168.25554	26612.73518	119639.2091	91354.82269	45265.65414	65948.72002	30648.52618	9209.171538	48034.42323	57564.40486	73166.77314	41971.69975	84127.01943	30218.31626	71842.81266	137714.9125
2-Quinolinecarboxylate																																		
N-Acetylmethionine	33841.45085	27491.92654	35159.9491	28701.27742	31918.32374				52144.51996		49899.27113	18886.08294	14884.11993	34301.95164	47425.5991	13389.49012	27536.48368		12602.60278		38607.8178		65373.49373		21504.0486			27075.89054	39498.39486			48488.18795		80292.96763
Cortisol	100719.277	93270.41204	89692.17381	87115.61636	89467.8287				66961.25655	95104.75478	89033.62976	103080.6388	103196.6717	96370.53083	55903.86462	86294.01392	111254.9641	100576.9088	171081.7897	92700.78344	64107.93923	67610.90566	91471.99281	57155.86976	99839.4357	79163.00173	132914.3569	102098.8691	90776.09686	188327.4049	162430.3862	68672.52891	182080.8294	82369.16323
4-Aminobenzoate / Anthranilate	15132.58969	14235.77501	14997.70645	15972.7516	13746.79848				9411.165436	18981.74924	20406.73553	14302.58389	10797.0969	17962.13892	18450.96842	17486.93039	13336.22421	12222.21001	13019.74462	10563.20501	13001.25576	8123.643427	17110.19482	12648.69702	26289.27489	12184.88745	14761.10643	16335.26761	18958.65257	13092.54727	14634.11086	12231.17841	12652.93217	22836.61155
Phenol	342744.2977	313987.3602	336654.4861	329237.3919	314286.5276				372236.349	205505.1391	386586.9315	319685.2939	763914.7363	275167.8522	101774.0863	373229.7022	386402.011	236730.1181	164444.6502	132916.1108	516779.3514	105987.126	117790.1433	219249.3749	380469.7866	216144.2744	274272.1569	632637.3505	155038.4323	174499.3601	338941.7518	232278.3855	162354.9775	287140.3998
Hippurate	7095405.501	7169055.64	6692004.627	6782409.533	6723914.8				8290712.728	4730185	8721051.929	7579382.068	17271822.37	5618398.905	1861258.209	8201357.373	7499916.626	4935678.961	3225585.765	2278540.641	10529336.79	2074673.158	2095795.419	4796145.714	8591019.826	4845050.446	5851136.919	14756542.75	2986378.164	3233164.982	7384810.871	4560333.682	3273346.65	6668004.104
4-Hydroxybenzaldehyde	9995760.173	9417045.04	9441252.607	9325198.896	9029489.154				11080345.89	5992280.439	11530925.66	9860912.623	23037505.52	7507197.486	2441102.347	10991351.46	10795672.38	6668542.908	4451724.381	3046704.592	15152095.83	2842316.717	2879016.946	6353465.757	11294328.15	6320059.862	8064706.446	19089623.67	3875417.809	4384558.007	9660732.325	6153411.849	4543412.838	8574042.044
Glycochenodeoxycholate	87619.27726	87364.57749	85336.52982	82718.80856	78500.83676				41166.54902	99402.49829	93139.32163	37006.48066	148954.9949	101548.2918	28756.43156	331497.4481	38781.19658	62376.04594	99965.44784	47823.8628	65713.7209	33118.3552	21875.42311	64613.6869	183718.1116	10787.7902	228244.0569	118095.0174	46335.87669	103247.0773	103271.078	196744.5615	14658.09375	23408.56914
Acetaminophen	1467243.287	1401197.855	1421261.782	1326092.842	1308469.945												10726.10002	20973337.77															1507341.988	
Thiopurine S-Methylether				4518.816161	5497.567871				2945.055233	3165.485672	3856.723656	3391.546127		4746.984471		3341.518506	2226.788422		3592.774407	2608.194583	3374.738783		4059.216703		9469.815712	7882.868533	9056.681034				4839.366386		6855.582741	
Paraxanthine / Theobromine /Theophylline	16460309.98	15085707.8	15898521.42	14949707.72	14627509.83				15538366.31	3422001.905	28946052.45	6605147.581	1088551.321	4257548.873	5525277.527	22800668.67	22124099.9	19340928.72	11785355.52	7306513.338	16972246.64	1117168.636	37951952.71	19820106.85	6097207.76	7399302.078	6778294.848	31497148.81	35484650.26	2862929.175	13736725.65	19561954.39	9620960.416	21312811.25
N-Acetylproline	222352.2268	225581.4529	219434.6815	217866.4298	216077.4922				233764.0065	503491.6838	409820.3247	485423.8588	889556.0485	321370.0695	284906.1601	451752.4431	363403.8946	138391.0331	116009.7597	121152.2534	246571.7796	147029.7357	209717.0992	132207.6374	312798.7628	316748.9521	190191.7835	509602.133	236168.3607	139651.9276	530371.3417	189006.4876	231600.3802	265146.7271
Indole-3-Acetamide	8374.267349	6445.250652		8609.433882	8263.577057					7323.12195	10779.17264	6253.772736	7537.707187	10893.99681	14208.71527	34268.94799	14735.58679	6485.744109	4055.072733	5435.135948	4063.038809	6792.155344	14189.94905	18395.52668	5077.418361	8091.762474	9200.418795	8424.964316	7760.153228	4235.85714	17091.21179	4467.723794	4127.382267	11397.3887
Maleimide		1141.489928	1266.406493	1167.87952													1876.40223				1348.597662					2965.673091								1782.281389
N-Acetylcysteine	16997.96444	20264.15161	22816.95324	21527.12581	22531.98282				19480.77644	16444.32503	32584.96781	24372.31278	21153.47581	37439.49794	24900.19878	22439.40239	15047.23162		13291.79077	13182.42813	16897.60569	23009.7826	38294.48654	19072.27494	26410.32248		23278.19907	19164.98287	38656.18743	26560.83272	28636.09217	26117.20546	21414.1985	41579.43715
N-Acetyltryptophan	77208.2797	80234.86728	84393.80079	70250.14578	67471.1782				52631.63149	61752.51818	105674.0104	86471.20949	101883.9512	70780.46411	61151.77752	86581.1452	228139.839	56403.54038	53602.76625	35120.02157	48154.90317	37765.37423	54102.8817	72682.37779	141468.2794	25853.96322	84526.40192	50907.07323	154811.5059	53150.11584	204745.8266	58650.63721	64985.49934	59483.8579
3-Hydroxyanthranilic acid	657645.3083	677632.0887	620167.666	649486.8985	605328.218				1186030.328	745238.17	579733.7922	469392.7324	607637.1524	191675.5726	284325.2478	559318.7854	1193273.713	421221.2997	1030755.766	362469.2773	387468.4486	300833.914	431616.1453	635263.0371	830656.9793	680952.6869	390062.0212	373381.4913	1541256.482	998596.7021	658632.0975	957427.9534	758926.1086	180681.3941
4-Acetamidobutanoate	1032950.886	953729.5579	942834.0593	929755.1638	913987.9114				399427.5198	1107546.227	1309298.439	1299426.176	862124.4676	1381930.634	1473558.894	1060263.184	1061232.753	572360.6799	687590.9604	710144.1686	744934.9055	1070063.083	930720.5459	573052.1875	1081084.64	939161.7862	865019.7769	1224739.385	984797.7746	781599.7481	1238736.697	799837.4096	764289.5745	629967.3061
Dihydrouracil	69357.294	72395.2691	71127.49681	63682.50254	65545.26771				52302.56955	75403.20113	62526.42963	50448.3036	52756.35137	65096.14289	32265.69105	64415.42637	101924.1917	49515.53534	102179.5617	65738.76182	81817.01118	72710.39375	56682.88365	51516.87796	88476.76323	69938.82899	74588.88084	46406.46055	61516.77095	110458.4251	152897.1748	54983.74119	78033.25321	49412.5204
Thymine	58927.82868	47705.78072	54090.11279	53798.89162	50605.95161				41077.6891	65656.96241	44397.2317	35521.97331	61286.90116	43499.49317	35279.49341	59480.46558	70816.61606	43569.80142	78371.48256	59195.82001	43407.26599	37617.20804	45950.56576	42049.19024	71011.05922	71994.7307	66953.88306	33899.67484	64848.81797	44378.63545	66788.67092	36314.59774	68459.11539	61014.56477
Nicotinic acid	24833.35098	27375.33289	26616.44323	24951.55585	22539.78135					22335.58873		9544.368808		5442.063347	5421.821841			145854.9329	9660.432178			45870.26803	45688.01811	5534.909132	12314.00555	16424.16318				15258.11938	6885.399268	10161.48841	118127.6827	56826.30575
Lauroylcarnitine	20806.26174	19395.71107	19035.30808	17260.71803	17820.80522				10905.79055	12848.93548	8625.581618	17538.07834	10799.85953	12127.84775	7855.872161	16894.58785	28523.5867	17728.91704	27441.14137	18259.8102	15535.07103	20461.3455	21847.69212	12086.85743	51100.01472	35263.29317	46267.47378	6496.486651	9197.052894	30056.7935	28628.17244	14246.15878	17638.85085	15489.35236
Pantothenate	2579208.049	2512258.965	2429595.068	2376170.62	2237902.075				1485603.882	1142008.558	2974633.209	2109457.442	1379527.108	715651.6689	2229525.439	2835566.496	3325224.37	2989988.311	1752245.975	1240741.273	1188814.454	718650.1848	6988961.892	1500627.517	1711641.107	1700587.59	2946313.391	828096.3287	680022.0302	8310350.735	1142853.442	1197388.635	5081919.861	2706774.101
2-Hydroxypyridine	25627.21616		15130.12474	22908.75787					23283.34035		60141.46104	19858.46168		26908.59034	52424.91903						32184.7061	35318.30844	51725.53285						41006.6361					
N-Acetylglycine	34158.48516	35034.76604	34837.90804	34415.87205	32621.99236				65439.04415	19991.43613	112078.0013		37871.5986			30055.8306	130754.9374	60450.08433	41807.78959	20110.50471	25252.01989	13446.53013	22220.91308	24754.37148	65968.56292	25204.32377	71645.82419	13900.32035	42619.38304	18636.02745	45403.97405	49873.75532	18266.87206	10209.69794
Phenylacetylglutamine	37624703.14	37117286.42	35037231.58	36204832.44	34220786.19				23455075.51	48577469.18	48281798.93	28505926.14	39460182.63	58395125.72	64680125.59	27842925.77	32942977.08	18804521.65	25661507.54	19436518.99	30850203.29	19172138.1	18537564.33	39393230.35	41903720.09	17804463.55	56735082.38	51009389.07	13337959.72	26224068.56	40070497.57	31353370.29	27079196.35	23340496.17
Uracil	232524.8069	228236.1523	236536.4735	215636.0418	223282.3599				102795.7384	309322.8615	204964.2299	195469.9796	190477.8267	106222.9196	60185.38587	260476.522	220818.3623	104030.1233	422136.0308	377485.7412	256881.7211	372671.5573	206234.6131	218218.9755	405392.0053	262222.7664	295336.4663	30077.38266	277068.6535	148069.283	255450.1176	175531.9497	300475.0631	262225.6439
Pyroglutamate	6125999.224	6006021.311	5841908.057	5900229.794	5544911.72				4586115.12	6852218.362	7840649.209	5118466.332	5668169.97	7654719.956	8353356.425	6260612.64	6967085.755	3902886.463	4599147.215	4142790.37	5461389.645	4432206.027	4018187.315	5141971.645	6250644.526	4966049.342	8305778.91	6797530.463	3832824.135	4788852.87	7069382.827	5243860.268	4454658.446	4306080.309
Glycocholate	87179.20786	81971.79091	83344.15793	80060.14401	85227.21297				24048.48061	90866.81946	80847.18615	14264.38757	58300.27196	115992.6404	68164.09282	361276.2384	17815.07225	44614.99841	51597.88176	101907.431	134496.1916	105831.6989	38823.89813	93938.55453	77986.6578	112999.6065	135324.7629	30621.37217	47463.4781	219923.1403	90771.13527	101653.2366	50722.61315	18294.02158
6-Hydroxynicotinate	87805.23156	95395.03432	92416.40835	91223.06012	74962.3433				57173.43857	64010.81721	51866.69785	184068.9022	80363.96841	48591.43987	69517.58057	65430.86115	27161.22017	30945.46547	69095.50051	130284.0822	127691.9976	294367.5491	99406.95481	57593.99586	111741.2204	147278.5709	117790.3627	47038.1219	80613.68838	26395.48238	166599.3676	59236.23129	119405.3725	63331.59333
Kynurenic acid	2370285.809	2323819.707	2201937.685	2158442.007	1986967.914				1555900.066	2115332.584	2073376.224	2056122.241	2863113.386	3215872.54	2716595.788	1453928.465	1990831.332	2335046.809	1751723.562	1881326.702	2132890.171	1222910.671	2966052.522	2351320.111	3385235.195	2250996.616	2572156.991	2301837.813	1769393.553	3575539.339	1266091.745	1606654.276	2866859.415	1604159.936
Nicotinamide	166533.6418	148457.0324	169670.6862	162021.6208	135202.7439				188830.2423	75892.61526	47183.9214	95128.55792	83436.66851	46396.30448	35280.62542	49963.91531	195112.7999	171921.1802	114448.0577	104067.7264	120488.6418	58355.54098	1350927.292	240252.0043	125358.5114	124648.4428	69632.13349	43686.77821	92936.44384	268137.2072	142814.4443	82387.81399	64405.8712	151941.7655
Deoxyuridine	473941.9086	429355.1469	433251.4978	409907.9803	382114.4704				927655.2234	262966.7765	1362718.575	422705.6622	282098.6053	130613.4466	1156690.27	57262.50319	129670.9048	144591.0497	129229.8417	347860.5327	457993.2838	54620.51175	1590485.583	106273.0339	229644.5737	125274.0539	272415.6388	1001115.964	654784.5254	94432.54666	128407.2388	202535.2362	113962.7276	735979.6754
5-Hydroxyindole-3-Acetic Acid	319023.5013	310126.0926	297937.1485	288584.4692	282768.7991				88512.90177	178300.5536	213791.982	236147.7307	214176.0065	420160.3685	333211.8103	170286.7707	185843.5698	152919.859	1437353.213	572744.0156	116814.7462	174138.6845	171016.2282	159376.7518	259273.1546	172673.4345	244396.045	258903.1167	381028.6363	203205.5268	186281.8375	1062453.196	162003.7922	288001.5316
N-Acetylglutamate	281149.3077	270466.6574	259900.7321	256357.7684	244317.3495				269675.853	253171.062	324646.5376	227705.1192	388066.6826	499564.405	306169.8123	390981.2942	258521.7781	226084.8445	261761.395	262256.2814	198378.4169	230501.4875	279786.8462	177532.1385	375111.8769	290715.6976	399830.5069	365772.5408	157656.1197	284245.7665	388015.5613	285906.5752	256744.6289	110869.3781
N-Acetylserine	320772.7507	310356.3792	296024.7674	287054.6303	257686.4085				334920.3786	255856.4663	391140.3527	224263.0881	400580.5849	471188.4176	285487.2851	451546.2109	353066.8179	216375.3575	313137.4583	269270.1798	216617.7141	239825.8883	277235.0126	170499.6859	412994.6696	309644.8792	416475.0613	371744.363	205123.0722	311454.7504	438828.2885	323153.5677	277787.5252	139017.9498
N6-(Delta2-Isopentenyl)-Adenine	10371927.98	10247585.8	9852322.349	9432223.738	9125214.032				8507544.019	6058758.007	10902221.82	24439235.06	6098723.412	3591155.433	14043734.12	4822625.857	32054367.72	7702493.495	1820901.207	1404252.579	4942383.515	4722596.514	4789759.922	8759570.805	14482599.04	5209641.396	19588272.83	2579795.389	24779509.85	9273615.819	10364097.41	12575687.09	4883451.224	1753698.148
O-Acetylcarnitine	11518336.68	11425432.06	10905775.24	10547542.9	10127229.46				9606998.123	6804222.066	12336715.47	26877471.35	6846212.328	3838447.939	15611271.26	5346943.971	35994193.52	8614934.639	1968966.129	1535393.153	5487494.586	5321780.971	5392673.521	9967622.479	16334055.25	5801485.348	22207709.65	2855211.535	27442154.93	10499725.6	11576714.87	14257626.22	5284749.913	1980973.017
N-Acetylaspartate	249201.6387	259673.6291	237691.2697	239767.4757	235410.8973				194390.4219	198868.4127	411439.9373	169049.7083	318808.0499	523803.8052	222770.2665	373283.7089	224639.5057	146156.0431	185954.4465	186565.9945	183465.0004	214999.1501	209495.4513	147452.7322	351650.1203	393991.819	404999.7208	324128.9886	160101.0767	245556.6552	460544.8395	366630.5919	237399.9008	89555.96375
S-Carboxymethylcysteine	35617.58685	35694.71075	36175.37427	29141.51884	36887.305				17109.74197	33489.84563	35019.9909	26545.85069	20674.01541	51079.33833	24361.46439	21153.40366	9061.583078	16808.39917	18934.3133	18649.8326	54944.77585	19657.20208	16233.70783	14625.11328	48051.32725	19898.55355	34110.27643	54755.80561	16428.44752	33382.45402	34273.64148	59099.12031	339409.8764	17084.19419
4-Pyridoxic acid	353771.8649	350926.8914	327515.2055	311734.6661	315661.0739				629491.3127	208558.3066	263688.134	208725.3215	669079.1419	193222.5128	465512.728	144748.4568	272289.5384	652547.8675	366185.6672	606742.5003	287425.1716	105469.9302	772461.5711	667969.5289	436380.1935	339157.1791	345736.5894	341295.9526	205811.7289	608890.5433	56123.29048	71943.64415	515298.4285	214880.7223
Xanthurenate	368327.8761	380763.3659	368091.1182	342691.843	345433.2444				655481.4752	204481.4669	310560.5986	195038.8631	700201.3827	230310.0259	473321.7543	152999.7462	300054.0287	631553.5646	407323.0158	604157.5085	297134.527	105777.1702	763527.6935	681706.1996	454166.9499	364355.3691	374117.4967	385019.7245	205429.7364	601918.8287	47339.62067	101217.668	541331.0185	182567.6474
Ureidopropionate	286781.1907	276506.2174	278263.979	274068.4356	265548.9457				170917.3715	252000.0697	328879.7336	192282.6021	241488.9831	396552.6317	236992.0898	305415.3087	348211.3294	109014.3238	304136.5009	238095.2884	238499.9311	276009.607	236393.2797	190612.3076	396904.1336	234737.7289	355393.0529	329732.8662	231181.9456	312541.1483	423610.1902	253834.8025	226740.6811	221350.5653
Aniline-2-Sulfonate																		63504.6324	6281.531099															
Orotate	14495.67057	14873.25396	14755.13006	16044.74853	16581.61741				14683.74022	16448.37848	9599.396521	16784.38335	21210.97896	7184.988119	10202.71945	10051.83389	11855.83824	20338.49391	18741.57445	24902.78593	18302.11302	17666.06008	14319.25339	22678.80583	11752.74304	15569.29837	16130.4684	12601.74611	16696.37021	12838.92221	8511.041945	13864.92008	19790.78255	15451.516
Riboflavin	590730.6889	583318.7944	513493.0908	490190.1671	432972.229				222452.7573	1397284.626	688186.0454	530344.7061	400633.6516	30834.23136	73799.78372	91465.93036	1072643.014	952447.4524	179349.2284	402031.7892	194993.9134	354608.3436	1589659.676	243910.4677	257244.5047	69933.83949	297265.8913	107907.0999	84987.18321	1771354.83	71621.57552	101986.936	1113032.676	1840520.471
N-Acetylasparagine	173995.0383	194455.8008	179541.1775	168120.1107	169375.675				90350.33616	225065.0688	240370.1789	83842.64294	148762.9797	144601.4931	30701.88121	348394.4619	238482.9357	129274.0194	296948.1702	173684.8172	91390.82683	75260.64943	215432.6106	87710.53075	452094.0815	100152.088	106813.971	246620.2907	161734.9921	257184.9148	257710.3797	192778.0342	217944.3175	83015.9174
Xanthine	726677.043	681207.2515	705564.4997	694981.0601	645374.4538				276069.8965	685085.5626	498869.6407	550932.4592	340853.5231	463225.4749	314373.7122	377659.6732	844679.1796	392990.7539	1159845.943	659788.4486	593322.927	872617.9203	626008.7788	1108422.638	1093743.882	771952.9046	494528.0529	449201.7958	434607.3658	1178104.73	1734108.932	551361.1549	876187.2067	664765.8885
Sepiapterin														26850.64643			18742.51481			8613.788074			8245.82158			12345.06377	11145.54963	9322.12196	6167.479515	8494.485899	19025.24818			7174.554625
Succinate	37097.34101	36372.77218	39176.68276	38010.52186	35318.12274				18515.0288	38118.17378	33570.67528	54039.44005	22246.60789	35158.13293	42704.01911	30757.27262	47129.37844	27596.96556	48214.24669	30185.70514	25966.57647	41807.86621	42851.52936	33139.97549	68126.30579	34683.91892	36182.61738	32452.66962	40847.89804	36055.01603	59808.20289	39559.27509	29630.87955	35385.28381
Hypoxanthine	4002023.721	4142911.627	3890593.806	3841355.331	3668440.734				1859009.968	4113081.755	4318417.681	2345383.114	1889567.043	2270272.602	1649169.456	2302154.854	6849948.281	2744058.465	6535593.111	2496824.872	2985176.751	5180824.318	5778801.551	4602598.908	10379413.99	2996239.978	4237182.563	1974680.253	2065081.107	3948060.813	6934367.458	2851030.208	3147011.588	4525087.857
1-Methyluric Acid	1466006.299	1532847.359	1421738.426	1391409.734	1344295.839				1853030.695	430444.2771	3746807.116	453637.39	229135.324	1108979.082	1782831.233	1191176.271	1343357.291	997285.7596	1111770.302	619735.098	1479393.789	485920.7274	1580059.624	2261710.904	875325.7442	1212443.051	1517342.874	2523575.987	1437981.823	381289.5254	661079.9898	3972503.466	438137.8479	2059529.106
3,4-Dihydroxybenzoate	9930.759376	9575.376359	10847.73041	11098.09721							7552.942121	9128.005152		5184.477209	3614.626156	10098.77928	33619.5091		18909.50866	10651.35276		7754.515846	16824.22316		6694.974725	39054.82495		24601.49421	3691.222435	34175.13102	6265.751173	10485.34815	11321.23841	
Cotinine N-oxide	87218.79834	74992.36873	82416.76209	86370.69267	69178.18388						84773.83134			49161.94073		149852.7001	39186.12947				43722.81698	576317.3844				24873.08932	23641.37647	131860.137				71567.27772		
3-Amino-4-Hydroxybenzoate	219389.7378	212188.5739	198554.1787	192576.5624	199149.623				721575.0026	90728.43343	296930.5453	77127.07566	295110.9883	258368.8219	465508.0738	222225.6244	234691.254	71404.838	133412.5698	204894.5374	61559.31773	132176.4048	177965.0103	188382.9718	291576.9487	287251.0436	266535.9325	227408.8271	69318.53574	464205.4572	88654.25479	142337.627	255194.1887	88211.99961
Methylthioadenosine	112206.1047	123656.359	118007.201	132020.4873	130755.2837				50811.60236	798467.1661	107231.7222	484990.6646	83077.94502	92482.67903	214286.063	74093.65886	333050.032	205870.2886	480727.6707	214437.8092	593811.2063	330067.0715	98542.70675	831539.3532	216406.6342	88369.48703	78107.98415	196771.6757	562295.212	272864.4498	486978.3648	107712.5664	98853.01669	352790.415
Inosine	29965.866	35793.6355	28804.35527	36933.57429	32190.83031				15131.16604	43308.28562	26950.82283	12292.64086	23364.42257	7900.643016	5502.34345	32555.76732	59504.97804	14384.65888	63871.00984	14388.34584	12435.938	62446.58885	13391.02147	36308.96355	31790.27646	15616.84834	18063.31046	23865.50673	15734.05383	28056.07636	53422.96168	57473.36953	30840.74539	61022.8319
Xanthosine	124972.5188	122303.7113	115351.5693	118596.5899	108560.3177				62329.04822	117111.6866	143985.3878	90963.00453	100931.2841	150706.939	110347.0104	132717.404	118310.6815	73092.74322	125838.282	98830.11602	81945.85239	112587.9085	108369.1362	112977.3717	106389.9028	191776.9412	128952.9353	184542.1275	109025.1328	119302.6325	148850.9042	208292.355	98005.45816	93059.15561
Cotinine			2488.284916	9175.072911									23300.39477						6070.31719					4018.110604								22897.58387		
Fucose												21770.01895				19488.39686																121581.181		
Pterin	120913.3744	113069.2605	127732.7603	115603.279	110598.0481				60503.62752	78286.84841	85323.46509	131452.512	139929.1967	64327.99842	101262.2337	73406.67151	94666.16597	86314.24381	72279.76484	203936.3206	109062.2581	146530.7458	106530.8979	101390.3842	125979.2185	140952.5267	90126.29641	200508.5741	78495.01214	244802.7876	254068.2842	267432.5449	116903.1953	72568.60676
3-Nitro-L-Tyrosine	2274702.256	2189368.536	2176636.343	2206248.654	2086282.892				1265334.238	2448923.898	2226634.015	2004993.285	1689228.774	3293390.77	2093088.723	3031782.951	2187864.323	1613437.77	2329992.369	1903417.344	1754098.037	2319485.846	2023961.706	1807502.118	2842863.554	2731122.276	2461789.939	2361681.544	1948886.207	2121390.499	3168826.499	2538814.382	1933515.219	1835823.997
5'-Deoxyadenosine	1431738.371	1441099.48	1388917.672	1454876.761	1344897.255				861073.0745	1663237.397	1384280.806	1344136.834	1215162.883	2142575.349	1333071.788	1775393.229	1296138.924	1060675.536	1533457.867	1126322.363	993852.9882	1503949.872	1231686.672	1233018.365	1663441.574	1933800.494	1772689.58	1716691.141	1153367.157	1461216.249	1991128.691	1742198.736	1234116.998	1150974.725
Folate															8752.928561			5714.187692																
Deoxyguanosine		10139.45759		6814.958928					24237.84188						29095.66508			18795.5076					19354.72836			8301.724636		11679.01167	23928.27366					26648.6858
D/L N-Acetylgalactosamine / D/L N-Acetylglucosamine / D/L N-Acetylmannosamine	694528.371	673678.7042	688964.5239	661821.826	673092.626				495330.5971	857258.5794	647047.4611	464824.6312	524135.7865	922279.3093	516337.9443	982542.6821	623602.0314	624369.9846	782610.6257	594908.4413	661147.5751	701083.2927	429759.8698	542399.0362	1114571.663	779649.8932	783465.9081	541454.0959	576281.3317	719222.3438	1159624.072	689408.6424	716163.8885	492851.7362
Uric acid	16702333.33	16043589.66	16082764.19	15500031.01	14694547.64				20330198.46	13630861.13	20466598.93	19500486.11	18162911.07	20617336.89	19098057.11	23368452.61	20675317.03	18282598.39	16367557.91	18631254.87	13641087.51	18379192.21	20303888.22	14835458.81	17968804.82	23084600.86	16669174.95	21747063.14	9534919.08	16034477.06	18666661.95	20083687.21	17382045.51	10578601.8
Allantoin	68867.71817	63240.37122	62133.17581	56260.40455	51978.82533				74947.84951	51486.63013	87337.19377	80943.98571	75232.87665	82575.65545	78270.5456	83950.45526	74777.01328	68603.63267	64886.46506	77470.53318	48671.01999	64117.83856	75341.36413	53267.99204	71020.79812	85802.5512	64514.97158	84278.03309	40325.96858	68522.10254	71712.50988	76765.14785	67702.64133	36347.12037
Glutarylcarnitine	1262346.528	1139930.391	1199831.015	1213161.041	1099895.941				976364.7027	864978.1777	1210339.537	1064949.837	1243127.093	2570832.535	1161531.676	1473076.067	894205.6661	891027.9045	1147179.542	911505.524	1172305.551	643022.1726	1237860.951	846103.2975	1287141.388	1685755.422	1924003.021	1006526.177	710723.4825	1139204.184	1453373.236	1383419.054	1207050.655	1050356.668
L-Phenylalanine	655079.9536	647452.0293	616178.8999	617385.0511	592874.6189				908900.2869	747513.429	1751370.336	443858.8292	549939.1431	630782.7429	423555.7461	835626.5666	1014822.408	544154.3767	1058954.746	868775.9315	584500.5767	586466.147	535685.5109	495848.1912	591018.623	992705.032	493702.44	1702858.466	693246.8934	637533.1031	886631.6211	585995.7591	610682.2666	463233.1209
Deoxyadenosine																																		
L-Leucine	326643.3429	328063.3532	338066.4445	337541.3758	353593.9929				1098793.115	557947.5455	730842.2467	136587.4274	689600.3857	145358.2822	185900.428	667355.4973	1537542.037	168134.9979	302430.215	201132.32	209374.5428	418045.4325	612338.4685	124753.8565	508326.553	939831.0656	259816.325	957871.3403	277099.4307	256691.7261	301689.009	218872.8276	151019.4931	274945.6544
Kynurenine	315153.2044	295895.0263	309424.4835	311352.0306	289120.2224				371587.366	423246.9926	377064.3327	93464.50819	505607.2831	164454.2721	173476.2496	311777.0401	491620.834	113897.8743	336295.419	113393.6804	241252.5465	168942.727	427314.6996	119153.5857	112812.86	488491.444	272074.9603	271005.5134	531371.2923	157316.8653	462211.2826	236112.3698	124481.0171	149338.375
Malate																																		
Dopamine	66773.14729	69958.03935	78163.35839	78462.02348	67167.1419				80545.47961	83207.85665	71898.00748	14889.99521	125721.5346	39059.09076	53542.68764	74789.96393	86289.29907	39923.5714	62313.3161	57089.93658	7873.719511	20591.45147	93541.93072	11595.66679	16655.04372	123850.0871	70975.38218	69606.64038	150955.5604	24941.49572	96761.02021	89308.13326	9493.17419	28101.27485
L-Isoleucine																																		
Biopterin	114254.9713	111868.981	111202.553	114939.199	120401.4818				107569.0579	106067.3062	141131.2459	108098.1788	162479.2407	88967.0135	118214.5981	227423.2531	141861.84	71472.44571	85429.56587	125477.4395	92333.47177	152473.8161	150611.6204	58472.73075	162182.7822	120860.2673	173591.0759	174120.5026	82217.29434	101063.3958	214101.0217	150156.5629	60928.28966	86589.3396
Guanosine	30884.66528	33079.76683	30454.17798	31698.87336	29462.58245				21864.50843	28739.4367	26558.50833	19534.66066	30713.01931	17086.44559	11733.88565	46183.0004	44858.3338	18529.21128	57003.24254	14852.54611	25232.04493	39928.30183	21424.96935	34048.44544	30583.08442	32036.87784	23246.14541	22812.61629	23102.03234	31494.13578	40496.1616	59834.883	27714.89802	22213.841
Tryptamine	582806.6663	588604.312	632468.6731	565283.954	527253.7374				543166.557	620361.8219	334939.0094	454776.8123	614881.0375	562174.5893	356744.4373	404458.8845	452381.6387	474985.2653	1382157.392	746214.3541	425991.0982	620512.1073	451478.4943	194173.6845	499850.3585	817494.0079	585286.8736	792926.9623	973067.4436	650313.4134	811861.509	719045.3924	308073.8725	417967.5183
Gluconate		5528.330801		812.0275089					4866.97735			1419.737861	5923.332164	5517.232652	2000.500751			2435.290058	6847.811892	3617.278989	4643.849014					11370.8589	1297.821382		6455.69988	2244.970587	3551.878689			
Adenosine	887466.8154	906475.3468	850803.3204	830007.2794	770004.7743				626947.4637	513557.9311	462329.4218	915516.6828	1080621.829	1084147.551	555186.7535	1276590.31	1151242.132	764328.4087	1300460.792	899187.801	1011991.691	412249.3176	736634.3093	841654.8077	1312890.671	1367484.498	1259709.776	677542.0269	450253.7277	1145496.974	1349033.925	1406472.009	790146.881	98132.56399
trans-3-hydroxycotinine	277193.2588	270219.7119	276083.5908	260848.2992	238431.385											621931.15						5809705.967												
Tryptophan	177250.5447	162583.3576	170601.0157	158905.9275	165568.757				178418.2252	181575.4747	19787.51919	153312.258	250617.8104	176350.6268	105530.035	142335.6905	187665.2161	139625.679	229501.7905	159880.4078	174384.9989		110977.312	57498.11575	158582.8119	285134.3434	166710.2239		190210.8194	115767.2253	233529.2973	85618.96374	55579.9355	204796.1943
Dihydrobiopterin	410061.689	463005.9713	412252.9669	406544.4118	381767.7992				290864.2919	197214.3603	194231.2289	290504.1542	468019.862	578051.0875	395462.0377	702246.4331	478410.9274	290000.4644	299583.8112	433113.7553	302477.0035	352450.6912	248748.6487	212692.2783	459709.3905	650099.8951	627921.5861	545852.5004	190270.5346	286763.0513	1023622.272	489840.7527	238306.5405	142726.6746
2-Deoxy-D-Glucose	415266.1834	449125.8941	421154.2328	407663.5582	406323.2211				200090.4954	157829.177	261152.3165	210934.8445	405817.4526	1194629.971	1641507.611	393224.7536	308203.881	279934.7015	241378.5831	267226.7046	439443.1159	226830.9612	208467.0457	123304.1668	191577.6951	264672.315	181789.2424	116491.9669	134875.1296	154796.6103	394299.6478	481536.7516	196939.0164	150009.656
Galactitol	919730.7704	939783.8136	896038.5306	894699.9681	857658.4669				489726.6122	380559.2686	432153.1278	358871.969	821040.1004	2423996.831	2649676.442	740922.8448	753400.7118	539032.0434	646714.4884	537406.7857	835077.6627	340936.1436	413943.9758	279232.8948	434088.831	551291.7825	337393.4797	433015.9244	303868.4268	316355.0548	838798.9151	1271488.573	402218.1766	336275.7165
Phenylethanolamine	57381.34821	49072.79613	57280.76432	48665.0222	46074.45346				28375.26868	30061.59903	63710.23773	34738.01119	40542.29103	64477.43469	30157.90979		32006.35839	19714.39882	39874.1521	28881.20796	17591.12741	25820.36671	28603.46558		51737.9204	42902.4697	22361.03374		14303.46668	29137.88866	52307.93164	60550.13243		52149.14804
2-Phosphoglycerate									45217.47246								19419.10585																	
Glucose	72218.19261	70131.76004	70051.98546	69045.41721	64008.28033				789900.5806	17001.57807	93887.44904	18112.49862	24615.21313	29397.43763	39929.02414	29083.86945	406782.7903	43916.41865	46729.51732	20718.55374	45657.72496	21914.60656	83212.04404	34333.23826	38201.5251	23925.06004	39403.35425	115597.9113	56444.90126	25066.38726	28980.80252	74205.26778	31712.23594	10947.44762
L-Methionine	358225.6881	365049.7151	326525.0248	300370.2471	278293.4724				873656.1645	332239.6402	245865.9713	152922.9612	312401.4183	402448.5523	224707.9447	260479.603	653005.0204	267617.6388	398341.2399	279072.7496	168396.4492	202255.9799	205692.6907	195229.9361	394775.0299	388910.5572	259527.0728	348165.9164	149337.0364	229785.2083	411882.73	302671.8892	204527.9182	63947.57613
Phenylglycine												9475.101257																						
3-Methoxytyramine	73296.38598	79119.86507	70987.9885	67434.0638	59634.83683							377546.8394			251946.7564					31955.57644					85495.24879				322838.7717		65280.75564			
Deoxycarnitine	539546.3886	525905.552	537154.5125	534085.6659	505232.9101				481227.683	385990.8351	401274.4785	2404199.849	486473.988	279473.0581	1215452.829	447218.1618	445265.7234	361131.0639	235222.5642	404354.2484	461197.6556	404140.0501	300173.9994	209116.5433	547103.4991	321993.8345	362788.7258	299625.9013	1317322.824	306328.1412	590738.0938	405610.1606	199407.0764	728257.4133
Galacturonate / Glucuronate	51852.21907	44920.32714	47909.23589	53275.99399	42406.95988				26954.2201	60640.24985	58229.29044	24617.49883	41985.37932	75548.83427	38358.67943	78183.0176	86564.24288	46059.74535	51486.34797	50302.61744	24744.11699	67969.72053	46409.003	39436.11045	54348.92333	101030.204	58566.01362	58465.06675	14306.02143	69657.90996	44911.73966	46698.80475	48454.25947	26078.89604
3-Hydroxybenzaldehyde	26403.72342	23789.87665	25359.70189	23709.98214	24751.50977				44753.41726	42562.07258	28830.41268		26277.42046	40400.36938	15328.95059	45919.26457	60395.72628	25005.2327	40097.51067	21165.23802	16890.68825	34024.77079	32806.32148	38575.07573	24551.14505	42191.20515	41630.24515	37457.37491	10004.42642	36710.71099	32778.82383	31497.59513	36568.19181	17241.28882
Sorbate																																		
Inosine Monophosphate	5090.744347	5102.965832	4488.93988	4492.653396	4092.583877				297913.1517								134438.32																	
Trigonelline	13993933.31	14360405.5	13227535.38	13082741.28	12383291.45				53455865.87	6329262.019	43629708.1	6728780.621	8390280.611	5550875.89	20261693.23	2222788.389	27627108.55	2335747.147	11474607.09	8327007.9	32114465.79	4657638.364	56067553.85	8813539.23	5573507.219	8346557.19	6036999.782	30400003.35	24009425.75	3822210.289	5891984.941	15967101.95	5973177.319	48699540.15
Ectoine	316152.1663	296652.5118	303709.9772	282551.4272	274908.9313				272452.002	669947.5089	560024.9441	159110.6284	194210.8472	548093.8063	183416.7641	770899.8219	287350.6724	249448.9342	898120.8163	191227.6731	704839.1219	114977.1222	286001.0174	936168.4225	531141.3343	255722.714	317887.2403	1574596.284	224492.714	788269.6153	100051.1151	206469.7676	261300.1106	185479.8896
7-Methylguanine	2919375.638	3021801.637	2813075.189	2807385.036	2663150.994				1711006.708	5875157.195	2787219.843	1275132.003	2455141.516	2488087.538	1864023.136	3449523.142	4909779.338	3479593.454	5787417.282	2492786.85	2408472.327	6921252.548	2425992.688	4289739.984	4573240.944	7019985.084	2617228.221	3893822.478	1447369.401	6196611.709	4101277.289	5719123.063	4731307.498	1957761.16
3-Methoxytyrosine																																		
Pipecolate	670387.2286	684636.7947	644351.9592	631779.5257	600711.3868				1066712.109	245664.9204	289244.5274	1414204.131	179074.7806	152880.2479	942005.5944	106816.9413	316657.2371	238390.6944	123225.619	566775.2973	164298.2896	91903.83833	862229.96	123548.1108	270019.3844	116644.0164	128333.278	126829.0097	4069769.498	85847.58131	2491089.51	127123.4189	135567.9249	170659.9134
Betaine / L-Valine/ Norvaline	9047960.776	9203144.428	8502643.551	8501530.614	7938119.529				33271072.16	16426015.72	12498530.48	4394773.965	9398456.69	7426568.289	3410334.171	7012914.494	19351888.52	10403148.03	13988636.05	13241916.75	8820733.586	5857486.943	8783465.435	6551624.889	6602254.629	8315973.995	8229583.1	4307189.292	11196871.23	12850781.46	14237978.58	8914412.035	8930646.572	3844863.983
Hydroxykynurenine	49193.21249	50479.78236	47741.62428	43834.13892	43437.10725				69907.59812	48767.03811	34017.37112	17549.78342	36103.94503	74008.5063	27339.85199	43426.98649	38865.00981	47598.29295	130340.9262	34862.62398	22551.52555	33354.94198	35863.49653	39635.0483	29608.74597	77934.86984	48000.27514	31506.12329	64447.01889	48594.56473	59790.92797	51482.23203	52922.0349	29439.2636
Guanine	274139.6177	271534.9924	260785.6637	235149.2647	240753.0432				142958.1065	250818.6875	272014.7165	150863.3315	126989.8956	115618.8767	107944.6973	101502.0854	436929.8389	206258.538	488279.2412	191982.2779	303338.2247	497256.4363	391984.952	439207.8355	553996.0794	331282.3737	160884.0764	260583.2242	147747.8184	290786.1099	204999.4116	394814.126	271264.5254	504236.6625
Adenine	57742.68864	56327.75149	53748.90298	56626.08586	49081.743				25836.47861	114424.7399	50252.89883	53396.7394	36933.62557	28755.02401	41769.89691	29855.04777	56667.85297	106463.0568	60072.42925	38005.57278	66101.07343	131564.0215	49471.99012	86670.17652	73113.9497	62023.89705	18670.04214	139800.5894	37419.66652	62782.05855	60956.09304	68102.44388	79034.49382	164407.009
Aminocaproate	947192.8512	998284.0736	937422.4846	914877.934	848189.3594				1134627.506	1232286.909	452730.3667	476217.0292	1444702.708	759584.2378	518710.1695	511243.4745	858367.1567	1088507.427	1919025.276	1501693.422	784963.9003	636735.504	665125.9116	661442.6638	795320.1078	1587744.735	713458.2034	1260005.034	1116791.528	1302678.404	1464808.574	660712.341	845311.4476	554105.2207
L-Tyrosine	2219576.641	2203149.072	2091265.798	2061221.579	1980650.551				2659950.487	2554992.908	1022934.528	1106344.27	3234601.09	1594090.316	1148782.187	1132961.255	2026615.225	2570273.764	4193143.551	3490717.699	1797796.417	1500998.2	1561238.247	1476902.565	1780974.593	3700510.174	1667503.679	2713214.381	2608837.93	2978618.117	3516564.164	1588233.283	1983196.934	1357218.463
L-Tryptophanamide	4712.003887	4071.899933	4591.721477							6331.574108	2117.6652	2864.90651		4983.551083	7065.759418	3213.583551	5617.226716	6968.861847	7572.855256	5915.081041	8545.763671	7336.562886	6717.944469	7895.278728	4830.231922	4679.345951	7445.763603	7689.115561	3365.594051	6848.083872	1415.284949	4489.404759	7014.477936	
N-Methylglutamate	143304.5533	136021.9174	128582.2031	111247.4768	122535.4355							1055952.21	42500.8201	93393.58182	462058.396	98212.77973				141379.5159					290825.5641		46964.98938	20844.04905	133322.428		347967.2027			
L-Proline	403008.3234	381243.2924	389844.5416	359207.8468	323254.8114				926399.3159	272595.463	652564.7447	432925.162	212371.6064	278632.3747	546634.8873	174027.7197	510687.6607	254256.1426	258683.4282	271999.1986	532134.9761	168159.7947		143780.1557	344917.4719	200640.1035	164123.6517	669692.9956	527612.0592	144384.6972	394858.1262	223530.308	158221.0176	820098.2516
Cyclic AMP	273697.829	272819.4492	258422.0741	251983.039	229116.1337				97186.82331	221316.9512	292385.5839	195639.3791	198634.787	387486.3008	336192.7118	374716.9495	210761.2604	204606.2749	265416.4238	230211.6649	211273.7731	233018.3279	266744.7267	233620.6631	236206.1917	302115.2602	443931.9799	306793.9586	218984.2955	208640.7177	375179.7704	320075.0145	183638.4018	199640.9901
Sucrose / Trehalose / Lactose	557808.9401	576762.6946	569990.728	568069.9405	570315.6342				170324.4738	296498.0369	790578.124	255855.7725	209272.8454	591613.7781	141913.2134	447179.7963	475939.4319	357732.0932	276189.4714	430300.8704	224445.6102	667709.5749	277886.6545	156387.863	238818.4152	169821.4119	407412.3449	538787.6539	471506.5782	277879.2839	228376.0852	726842.6147	253992.1454	208159.3196
Dimethylglycine	419174.8568	469115.0982	425114.4305	395418.7838	345130.4864				1061328.216	430128.2999	593122.6139	262612.9233	476899.7309	307917.0077	232995.9392	174943.5278	401367.7978	371251.85	404745.1105	386001.0313	189772.9388	230136.2836	204750.6922	261612.0125	274664.0179	582550.119	280375.2863	509066.817	724461.2922	317195.6935	930705.7338	411990.9272	571687.5753	221304.8807
Choline	12643655.38	12548495.7	11820889.91	11371132.8	10825645.78				47301188.15	11616600.54	8560963.591	4949213.209	13425885.65	12817213.64	2759481.612	7627825.94	11395864.04	8676006.553	15365774.25	13416638.48	5628719.027	5454147.076	9916660.532	3678583.748	14522018.3	12802312.64	10641173.43	8227631.273	14848502.46	15737553.66	20478538.38	7687864.757	12582230.32	3937365.092
Taurine	554239.4206	516103.3357	512325.297	510268.1012	495021.3764				1647495.849	256046.7778	250944.4906	1428044.859	308590.4684	429127.1033	223680.2482	533808.851	373984.4282	309779.2686	747593.8846	223894.2771	1227803.076	869275.3927	206019.0587	203161.9843	264310.5857	239130.7119	420712.164	182653.7794	130796.2881	222250.4907	1059027.6	322182.9927	545571.3161	448068.3682
4-Imidazoleacetate	308239.078	303338.8836	295822.8748	277303.9824	271474.4694				108347.4354	223145.5151	266405.2165	405361.2499	248697.0764	269263.6049	273903.9757	225740.0469	269832.4662	688725.2613	291487.2472	983072.6729	625892.031	155187.6319	235091.031	246848.0419	239584.9977	398020.3296	207057.1908	362073.8509	221884.4412	433462.6173	286653.8332	260989.9702	111144.4468	203086.5407
L-Cysteine									5869.519361				8487.381612	17812.89851	12718.48823	10854.46585										13824.24657	6737.077872	4876.675484			7556.21542	7035.518796		
trans-4-hrdroxy-L-proline																																		
Sarcosine	187997.5322	162794.0146	185339.1608	167342.4101	157771.6403				319450.1373	91023.46312	224752.7698	79851.91697	35650.4936	24678.44177	27119.43045	307714.6258	193032.7064	448047.7299	305995.5789	225192.1699	196078.1688	190726.703	9092.425482	63961.77208	199602.1363	69450.53543	47964.98681	52075.28648	29250.14962	733529.2208	45205.5779	28170.93267	95006.49023	58161.82428
Aminoadipate	184776.9924	172612.9592	188567.287	175056.261	180237.6917				363103.4275	308757.5528	113094.24	161622.777	500321.0046	120000.7746	145734.039	153487.6927	245296.5664	307615.6585	204922.2842	317224.0564	250510.3739	140832.7867	278497.2237	107889.8925	209337.1578	282680.4415	205106.8651	223610.5865	115242.9291	267044.2741	140461.2111	149065.774	144684.3571	118000.3941
Aminoisobutanoate / 2-Aminoisobutyrate / Gamma-aminobutyrate	256259.02	272095.9442	226213.7951	228510.864	239459.0571				210048.9297	142122.5605	164111.2735	108725.8235	755254.1208	218888.4424	204468.0186	154359.2276	522751.3667	200653.4382	87784.88862	84423.53868	459471.9001	137786.0383	149715.7947	128707.8798	500016.8259	349749.0419	243219.7393	425227.1774	159035.8765	197270.3261	325368.2473	240296.0333	122784.8497	139160.8714
Creatine	118289867.7	114980491.8	117006786	113590242.4	113424355.7				67464435.4	109531039.7	119778247.9	129230905.8	104098414.6	170771114	106908830.1	130454749.2	107100884.2	98595441.2	110144558.8	96225599.19	141901823.4	112770999.7	105291131.8	127940988	113233206.9	133641482.3	126961692.1	119260954.4	109124059.7	107548223	119009093.7	129490873.1	101482376.5	110061818.6
Serotonin																																		
Creatinine	123979831.3	120792836.6	121937854	118284769.9	117673708.6				83757413.27	126186740.8	119501161.9	116496576.4	114970154.8	166652498.2	112390879.4	134216767.2	110939607.9	104843984.4	117495515.7	104243565.1	110646082.8	117201087.2	119354033	116088374.2	134283487.3	142306140.3	137852094.3	128037839.5	105955810.7	117065712.5	128061594.4	126881842.5	108662552.5	108751114.1
Raffinose	19521.50955	12094.50639	32693.27763	29484.47667	18504.19896					59617.75244	19774.90849	37243.36848	18935.12046	16446.81614	25007.06356	11748.44968	23251.22716	29192.99438	50884.78038	17410.01959	11287.61219	19617.68747	27948.84381	18099.61985		33764.37705	7472.298043		36238.72763			59761.51038	53944.11688	
N-Methyl-D-aspartic acid	226325.7132	177834.0206	170911.4116	170936.5464	181535.189				118749.7482	268971.0104	126610.1816	212528.7472	149894.7496	117910.0814	164511.8714	194427.6883	153799.7961	177493.2395	192740.3512	98968.56528	344494.6453	195304.258	151496.7421	94562.79299	222641.6879	249756.2302	108257.2483	111443.7307	145113.9696	122759.4991	211490.3017	146308.9261	180205.3904	271673.1692
L-Glutamic Acid	175036.5547	146362.8635	124031.2791	129611.599	142126.4818				115206.3596	264747.5955	123430.692	204990.1442	145711.0334	114959.3481	159709.3442	190264.3792	150060.0586	173901.3053	186745.5701	97015.39329	316041.738	192518.846	149204.1302	91882.13402	219135.2047	244828.5608	105782.7727	107331.7359	141149.0233	118229.4746	207975.723	144871.4957	177646.4951	266388.2502
5-Hydroxytryptophan	4748.092363		2565.248492	4666.713632	3041.23773				1110.748779		3183.164353	6991.519388	4836.375878		7699.107136	5010.021368		6778.861292		6223.870238		3517.532071	3163.187249	1460.124034	6097.308986	4728.640024	3411.326444	4621.879531		5436.233247	1838.045405	3766.527675		
Alanine / D-Alanine	22523.70207	19582.11484	19922.5903	20419.24232	20983.93709				34024.03164	10565.11217	25335.55125	9040.77896	28508.50967	16455.73245	9213.684184	17623.62004	50730.59637	12306.32396	51638.35197	30557.49504	9013.371452	10038.0125	11230.91439	9187.735338	18427.71478	18602.63302	5581.965583	14196.42862	46120.84932	17115.62982	39631.26462	24169.94224	14093.06325	5249.014711
Carnitine	7858193.079	7391657.315	7546435.099	7024814.786	6565652.579				2576784.794	8217008.677	3628676.063	32965941.95	3567490.339	3734244.285	12474088.2	3505364.046	12467127.18	7118292.596	1783323.653	1462432.028	3802321.885	4805169.49	4952858.493	8469982.355	6153795.883	4473025.946	6118385.716	1469070.612	16951309.56	8653005.251	7769827.879	9909029.265	3531931.671	1972775.953
cis-4-hydroxy-D-proline	51027.4946	51752.03063	36242.7708	48636.78172	33953.65625				117299.8552	67707.93405	20770.39756	34360.0482	55041.23186		35683.64563		155538.5517	3533.216243	20713.59386	51865.18949	37272.62875	1855.116552	33323.10383	20191.90025		26674.35165	23139.85896	27560.85675	100639.1257		149741.6696	115536.5599	83646.64493	9405.877718
Octopamine																																		
1-Aminocyclopropanecarboxylate	661364.7517	640244.7373	618638.8104	561377.8498	550340.5635				1490208.551	615089.6294	429656.576	279772.1048	1845568.167	368699.2844	121424.2402	287276.5108	759896.0101	776490.7954	1675810.866	880789.8634	323185.2988	131128.1894	259211.7244	321316.7095	701835.6235	467505.7786	559272.8677	441519.1646	1381817.643	629235.0809	737157.637	428549.6124	450961.9369	165798.0534
L-Threonine / Homoserine / Allothreonine	3263931.412	3180636.003	3120232.064	2958503.183	2880960.656				8076770.895	3238750.28	2422176.973	1530575.952	9796613.95	2028676.1	591038.5838	1507577.544	3959707.295	3959755.796	8493885.101	4518628.615	1681847.979	734889.0962	1315666.591	1748531.117	3628087.909	2567556.647	2870577.128	2229249.052	7574314.899	3226132.722	3943865.323	2294908.653	2332975.539	889684.5183
1-Methyladenosine	3175303.366	3219887.993	3032812.733	2944348.408	2864598.315				1748691.533	3857987.456	2840530.804	2742517.066	2602394.792	5095154.216	2874113.557	4235703.885	2431001.39	2586089.571	4063948.945	2602180.29	2898132.113	3017146.04	1532888.938	2648818.234	3782227.228	3698845.969	3385114.361	4199516.159	2742938.551	2224993.246	4842215.028	4402993.341	2558403.048	2734019.115
5-aminolevulinic acid	45080.3195	40163.81718	45497.33837	38798.37913	44713.75271					35562.47606	15366.93344	47653.22224	18742.95851	38118.26396	31311.50751	27357.74611	37498.08368	5942.028115	52708.62472	21623.48928	27781.9054	43318.49263		39474.777	75994.37827	46195.85156	56867.41342	26203.48777	14565.60705		101102.9892			19471.9964
5-Methylcytosine	189234.0074	236297.094	158600.1596	161443.8211	223081.7496				79666.01939	218754.946	171551.9204	151570.2779	233692.2851	312105.8152	108480.4172	265246.0027	246870.0357	157338.2674	261586.9867	170752.4266	170092.9932	168101.3522	94071.73945	138099.4954	214970.28	205565.2429	196427.0502	281697.6699	101125.3782	189327.388	265650.0883	193560.9499	139218.0673	145085.2433
N-Alpha-Acetyllysine	368651.1986	363367.7647	353003.5438	317976.9004	309390.8185				136823.6909	529892.6428	420350.3029	202906.2639	204809.8753	295135.8384	107294.4708	615436.9551	431352.9707	309503.843	570925.1771	282064.338	250123.957	225361.0775	641320.2532	168260.3671	540549.9737	259366.0443	252884.3856	482912.8118	139580.6799	577657.2928	202308.0706	184699.0211	369580.1928	259192.6632
Pro-Gly	293497.3417	276989.8483	257105.282	258700.9922	250649.5629				182905.2509	193098.6927	102924.1483	162449.9156	95503.3819	123662.9077	131448.8278	177703.924	250820.7231	191385.9413	387677.5793	131195.9314	378265.7477	167245.1475	215671.0821	277791.4358	336869.1509	185573.1979	258199.7175	153837.2005	147805.3719	220035.5842	477114.3123	352547.872	321461.5899	98983.30883
Glutamine	4532140.232	4413578.2	4293649.161	4080015.368	3968221.957				3828032.137	4490302.394	3372992.536	1986436.935	6607072.932	4684179.688	1555217.818	3957884.281	5624984.52	4660056.823	9518608.365	5900032.568	3209855.493	1798934.247	2827750.924	2622137.496	4007050.651	5482291.235	4996202.287	3647909.774	6480255.517	4662239.907	7687422.593	4406388.397	3356013.153	1758715.299
Adrenaline(Epinephrine)	10030.53902	15329.9795	12641.68522	12340.32467	13933.14284				5385.546014	11980.22062	10297.3712	15858.02949	11503.67879	15918.627	12219.54734	11363.79159	12007.34312	11570.07015	9894.434774	10908.62978	12638.73452	11086.87296	14870.79301	8038.205282	9176.026052	15900.22502	12089.4178	12860.78274	8136.719321	14363.85784	11006.56371	10396.96094	13017.33481	7575.250847
1-Methylnicotinamide	94505.18492	97428.63671	111470.2914	89101.70269	90968.29868				30524.61257	86623.98814	108930.1351	98412.76346	98686.00001	72799.31953	53151.50519	118960.1345	111994.1832	93782.02082	148023.9638	118912.6349	91529.02005	87800.66727	53107.92834	82688.01597	129043.9326	92138.23438	81198.69164	61032.79425	89292.91472	116266.3713	110660.4082	35905.55534	91498.37972	49738.24612
Glycine	197255.247	194752.0401	194912.4401	179705.6724	174091.0347				134743.2387	168021.2983	205622.5974	198888.9265	186827.9701	183064.224	118392.2037	267740.3212	214053.7601	190476.3389	241039.308	246850.2059	198162.5336	184418.5379	108395.0538	187833.8853	259077.4507	172602.431	227414.0358	164621.0833	184513.0388	216373.6672	208529.8895	109402.4589	195713.3309	93725.00134
Guanidinoacetate	18866682.95	19101704.6	18024437.22	16574064.74	16101643.49				11206364.78	16678655.76	18120331.17	19846015.17	15824572.14	17472860.65	11839001.2	26604018.69	20916849.46	17525689.61	20994824.6	23665084.04	20920265.05	17850324.24	9895841.453	17712750.84	24841313.54	15263206.2	23771099.25	14182360.18	14273558.08	22252969.4	17897106.56	7193906.747	17726330.29	8704994.514
N-Acetylputrescine	883096.5149	861121.245	853091.519	780692.0783	750482.7749				352656.5329	889447.8331	987695.7328	911255.4059	756836.968	1247167.86	770027.6865	1093243.903	874197.9088	614286.8488	733329.013	652567.1439	601159.9019	1242601.173	589703.2899	540146.5872	992935.0398	895196.0822	703114.2714	1251037.14	899633.3944	696836.5387	1150003.086	702970.1559	710178.1928	429684.4904
Cytidine 2',3'-Cyclic Phosphate																														5674.476301		6812.364802	5908.211251	10391.20878
Deoxycytidine	26994.92414	27644.71457	26671.94824	19513.69241	24179.3446				20446.62162	24136.42633	16574.16633	24596.37539	9033.625109	44037.13605	19218.69939	16535.81722	19446.6283	21558.18222	25031.59995	15908.42264	19602.23535	21998.65061	23169.93328	23643.71823	23011.08621	21849.02549	27260.11794	22589.45988	20425.17734	45247.87958	27611.50311	37407.03336	20290.43347	25721.62063
Guanidinosuccinate	370081.4179	381194.8465	358116.8008	335389.3287	324116.8536				515097.5024	326560.323	671571.3008	490884.1579	326826.7403	548297.6465	421699.43	412135.5457	193520.5842	278433.8454	375503.2266	296187.4253	333474.1924	396376.6748	770991.1031	207039.6961	360446.8367	280729.2238	359016.3505	525811.4957	241124.573	270936.2428	185846.0941	234789.6048	230398.0478	258149.69
Citrulline	335883.5366	481628.4139	324809.9713	214495.9705	322472.9173				303228.7742	608213.8369	169572.2539	343037.8822	483040.3439	342512.925	173715.5208	561872.2493	362043.5918	410051.0972	426475.9868	698278.125	149716.7297	219474.2375	269456.6411	799046.1091	395061.2118	833523.5874	652810.8469	350673.571	200133.3759	415813.106	363753.9628	615262.1963	526907.794	109413.2052
L-Aspartic Acid	112440.5531	109009.0152	98605.89982	93155.79062	92470.66696				134131.1741	122581.8293	62004.52274	53803.29442	251938.4875	77832.50959	28228.64907	57981.28117	104039.9837	142215.2066	274939.1674	183525.4726	64773.03783	34070.91586	53319.75486	43557.44565	132893.8182	99817.82004	61751.38889	80756.42569	248991.9152	78188.57914	183259.7491	76935.85644	67769.2726	20661.34745
Asparagine	1407892.581	1398529.963	1317350.223	1284092.077	1266289.525				1760722.101	1621798.192	758104.6151	704185.0285	3110964.981	1107373.661	320981.998	712795.122	1295182.775	1929979.921	3245099.911	2278986.338	833824.3986	435733.6985	689596.6658	640891.6502	1692148.195	1314435.461	782206.6323	1010023.097	3382386.723	1058600.269	2309745.67	1040913.64	955381.1111	282587.0812
L-Serine	931040.4001	932950.103	880845.5099	870246.8719	831577.4425				1279251.71	856731.7827	780171.6724	560054.4388	2029792.635	1076696.776	323860.3137	722852.9765	1065884.446	1167062.009	2208226.718	1199352.038	452385.11	399592.4809	530226.86	564878.2805	1201672.471	925300.0345	879228.9488	780912.3103	1775348.287	707636.6792	1692256.759	812440.4798	786596.9945	392651.1726
Cytosine	366310.94	376570.3518	337294.7453	307600.6467	303763.0303				393128.07	174076.555	687427.228	441247.6873	465869.2642	301153.855	214569.9346	291234.8073	272237.3303	193019.3911	353950.3435	262491.1516	181116.9204	133957.4335	303114.9523	113081.7894	272421.2228	713966.6057	1197803.856	334405.0151	573801.9402	219102.8421	620531.1166	794767.6078	324949.3332	189237.86
Beta-Alanine																																		
Diethanolamine	80305.43949	86149.27969	74922.54954	74234.01236	67701.3485				42708.62004	122206.5303	61996.0556	63289.53073	52866.55843	50953.62939	24236.07308	37431.65355	48577.50293			36773.67586		95660.67115		64124.52878				31255.31952		58285.10777				51918.97589
nicotine-1-N-oxide																11910.82023	1807.62922					242073.3136		6733.357704		1195.529021				1881.299742				
Cytidine	49759.76582	48766.388	50874.87074	42983.16881	41426.7134				34488.46381	53392.5873	29312.75786	39556.22113	50100.30821	41463.15707	26051.25525	95228.22549	46525.22671	38011.1851	29625.72241	86287.72962	45719.35963	30880.92326	32712.80564	38056.53044	65826.83457	43774.62175	50162.22863	52880.06335	41809.17117	51657.18328	51528.50011	41339.85077	42270.92479	28120.55093
Nicotine	11862.21282		11680.91754																			77803.10868												
6-Hydroxydopamine																																		
Noradrenaline											4887.878865																							
S-Adenosylhomocysteine	7578.052527	6406.522937	6129.206112	5963.067369	4545.80523				3771.243898	5534.587287	4457.784209	6099.672391	6159.129539	10280.65176	9334.150859	7557.580181	6847.349146	5003.036479	4351.707489	4572.668882	4546.953727	4030.100223	4410.964294		8819.425641	8097.325492	8241.427873	8130.22995	4419.429936	6178.417197	8734.952992	7378.00925	3785.955465	3503.648805
L-Cystine	58622.45372	50293.60902	53988.76644	52434.21603	47020.02913				42311.68108	198370.021	43120.53897	87143.3249	49053.36309	59281.59083	32350.32477	46525.62908	70620.49224	253003.646	75345.13048	39524.1328	150457.115	54235.21509	70630.82177	68703.14007	40704.84221	36787.47552	18161.42507	43378.83229	128600.2777	30421.21814	31199.59628	26233.78078	41780.57904	23694.57708
Cystathionine	7051.838873	5141.612283	5589.124028		5230.075389				4650.972189	10750.89952		11807.73324	6787.457673	6987.67335	5209.246876			9489.073978	5660.098684	4539.241785	5257.009294				14148.85675	9641.808263	6973.989184	5766.402855	11627.22844	4024.702314	6836.772202		5830.614886	
D/L Glucosamine/ D/L Galactosamine/ D-Mannosamine	58139.98058	91026.4371	78372.41535	89784.06401	72426.99094				29634.25285	146361.0007	55937.25088	87761.52855	68040.8509	101768.6515	60983.12249	249399.5477	135981.1207	91155.77641	55917.54611	23692.18369	64222.14004	83965.01697	60284.41964	44961.67226	34625.01446	55490.89191	37007.36676	39279.59693	48109.46261	51223.70098	42373.16648	61922.3705	81048.15212	242062.1381
D/L Glucosamine / D/L Galactosamine	33177.87862	38737.56338	37681.87742	34985.08556	20268.50959				15970.71311	63155.09766	28148.68705	73086.37891	19812.23063	31420.48452	12610.13331	23324.79351	115657.8893	37050.00945	64483.7844	24413.44822	57020.18459	49728.95812	25291.40147	50032.47352	29384.45105	22083.56926	13137.46479	32483.59344	47107.59682	12746.1077	17483.04363	14959.24935	29713.28307	44113.2585
Asymmetrical dimethylarginine	2568948.815	2238222.184	2331130.32	2315218.006	2155852.142				1401639.032	2386998.537	1812527.339	1862448.474	2402954.719	4112824.21	2198913.237	2465604.18	2400693.659	2578818.826	2680745.705	1735236.205	2287136.493	2596801.772	2160237.082	2122660.901	2273044.278	2535353.475	2438638.294	2577712.717	2690938.542	2288418.336	2980591.488	2831177.097	2121507.987	2067443.062
L-Histidine	34975981.22	32843473.96	32491797.16	31579810.63	30887902.17				14345516.8	44427836.88	13560113.6	28475837.16	30488000.99	25524551.37	9359537.011	9448376.149	37679147.03	47870101.52	57332387.28	43352408.98	35292212.17	20608060.12	18516591.07	26733675.23	26860937.69	20370949.09	9463210.909	33165531.01	49772669.49	33758660.75	37409753.18	20943070.86	24028988.63	17010958.29
1-Methyl-L-Histidine	22808676.86	20798107.66	20457661.25	19645771.08	18761544.03				4704116.082	37145481.72	21023435.64	21738781.7	4728424.814	27925925.01	6841194.507	9663796.843	14382941.24	14288235.61	13921034.84	5567864.211	46355339.79	6747234.186	6198396.685	28229008.39	25814043.36	8746679.759	7203104.41	68535932.51	7903103.756	64370989.87	8207315.756	5734179.121	10887861.14	17096829.78
L-Arginine	35405.6497	32381.31638	34051.78039	32722.39065	32663.11412				26206.49582	53768.62814	13979.48142	42831.20872	35522.28664	62296.06998	44403.27141	23835.28683	22362.29755	70094.88247	34312.01618	23134.17998	62054.82878	25427.71582	32685.03849	56632.55098	21060.8199	100265.8619	19959.48444	18626.86336	38494.30833	28085.79188	29542.54112	23940.5895	42942.729	59577.66247
L-Lysine	21248.14504	19989.39868	16363.09137	14215.68083	15014.04669				31262.53222	52225.47889	4303.555607	19706.73342	34736.76426	19603.691	13770.41873	15795.02671	35037.61025	111981.2897	18431.03314	7667.844956	85389.68024	11162.36783	26067.74011	29267.37974	6360.400365	15511.46587	9381.040804	8624.25087	40392.06046	18897.67362	7607.005272	7300.636502	13554.70248	25461.79955
5-Hydroxylysine										1585.543865														8724.179078										
N,N,N-Trimethyllysine	323300.4909	330601.5053	291609.206	285897.4228	279124.4036				149301.6731	408741.3681	156860.5187	375237.6516	260270.5238	479661.2069	273164.2819	213571.9246	217484.9961	328534.6635	334540.3223	230975.2003	396807.0884	333864.6291	253915.7485	605839.7677	335799.997	331723.5216	259331.2075	248900.2957	303972.4595	380432.0826	374764.9702	425405.2472	406620.9839	269259.1358
Anserine	36133.47523	39651.33503	36469.46273	33180.72224	33190.07015				10901.73503	5597.267684	57351.45622	28256.8352		15468.15916	11109.61834			4446.639143	6891.414598		42340.18995			12720.40281			5875.873415	341531.8894		186311.7719		1155.31834	47632.53278	
Carnosine	10991.42082	8650.240367	10711.05433	10123.50256	7450.129802					10590.4336		21277.34581							18942.76563															
S-Adenosylmethionine	6939.306541	6638.803484	5720.852009	5690.616409	6067.678363				2611.563827	18851.97654	3298.220004	12567.85823	4706.668444	6663.195278	5792.574968	3451.548342	6447.992384	8417.260108	9974.640308	5873.543956	9389.051459	8438.970564	4656.314514	13219.70823	6162.571286	5053.920542	3086.498803	4300.809802	9374.296278	6376.095859	4870.307994	6656.918619	7199.408016	7340.671283
Cadaverine																																		33243.43942
Histamine	19020.06049	19966.71958	15788.621	13901.96497	17396.6058				9219.729152	38641.82119	10263.71786	10743.25095	12931.41305	9972.748391	10866.86378	10326.26006	10750.43552	10083.39017	22821.55624	14476.10949	9711.929339	12853.87693	18407.19281	9770.85646	12991.5172	12798.35256	9565.754878	27708.56456	9205.752208	40821.13414	12008.8287	11270.57104	10297.70999	69785.45329
3-methylhistamine	25889.87761	25846.51406	24987.13058	26362.26037	20401.34816				9573.916463	40843.48681	17791.48843	29385.7759	30275.73671	32673.23937	24754.84223	25018.78996	27686.32686	26120.10664	23811.41865	33066.59281	29630.53323	32339.08313	19302.12926	21246.96111	23584.23005	25737.11924	26382.81683	39706.05184	21422.24368	27568.13787	22491.04578	24631.67132	20081.03081	22455.19058
MS_METABOLITE_DATA_END
#METABOLITES
METABOLITES_START
metabolite_name	RT (min)	quantified m/z	PubChem ID	KEGG ID	Mass	RT (sec)	Adduct	Formula
3-(2-Hydroxyphenyl)Propanoate	0.76	167.0704			166.0626	45.6	M+H	C9H10O3
3-(4-Hydroxyphenyl)Pyruvate / Caffeate	0.77	163.0393			180.0421	46.2	(M+H)+[-H2O]	C9H8O4
Mevalolactone	0.86	113.0602			130.063	51.6	(M+H)+[-H2O]	C6H10O3
Cortisone	0.93	361.2001			360.1923	55.8	M+H	C21H28O5
Methylpicolinate	0.96	120.0452			137.048	57.6	(M+H)+[-H2O]	C7H7NO2
N-Acetylphenylalanine	1.01	208.1005			207.0914	60.6	M+H	C11H13NO3
Caffeine	1.05	195.0881			194.0803	63	M+H	C8H10N4O2
Lumichrome	1.07	243.0875			242.0797	64.2	M+H	C12H10N4O2
Indole-3-Acetate	1.11	176.072			175.0642	66.6	M+H	C10H9NO2
2-Quinolinecarboxylate	1.17	174.0563			173.0485	70.2	M+H	C10H7NO2
N-Acetylmethionine	1.18	192.0724			191.0646	70.8	M+H	C7H13NO3S
Cortisol	1.19	363.2158			362.208	71.4	M+H	C21H30O5
4-Aminobenzoate / Anthranilate	1.19	120.0455			137.0483	71.4	(M+H)+[-H2O]	C7H7NO2
Phenol	1.22	77.0389			94.0417	73.2	(M+H)+[-H2O]	C6H6O
Hippurate	1.22	180.066			179.0582	73.2	M+H	C9H9NO3
4-Hydroxybenzaldehyde	1.23	105.0339			122.0367	73.8	(M+H)+[-H2O]	C7H6O2
Glycochenodeoxycholate	1.23	432.3092			449.312	73.8	(M+H)+[-H2O]	C26H43NO5
Acetaminophen	1.32	152.071			151.0632	79.2	M+H	C8H9NO2
Thiopurine S-Methylether	1.34	167.034			166.0262	80.4	M+H	C6H6N4S
Paraxanthine / Theobromine /Theophylline	1.38	181.0722			180.0644	82.8	M+H	C7H8N4O2
N-Acetylproline	1.41	180.0649			157.0751	84.6	M+Na	C7H11NO3
Indole-3-Acetamide	1.43	197.0686			174.0788	85.8	M+Na	C10H10N2O
Maleimide	1.44	120.0085			97.0187	86.4	M+Na	C4H3NO2
N-Acetylcysteine	1.45	164.0377			163.0299	87	M+H	C5H9NO3S
N-Acetyltryptophan	1.46	247.1073			246.0995	87.6	M+H	C13H14N2O3
3-Hydroxyanthranilic acid	1.54	136.0398			153.0426	92.4	(M+H)+[-H2O]	C7H7NO3
4-Acetamidobutanoate	1.61	146.0813			145.0735	96.6	M+H	C6H11NO3
Dihydrouracil	1.64	115.0508			114.043	98.4	M+H	C4H6N2O2
Thymine	1.67	127.0499			126.0421	100.2	M+H	C5H6N2O2
Nicotinic acid	1.71	124.0404			123.0326	102.6	M+H	C6H5NO2
Lauroylcarnitine	1.79	343.2723			343.2723	107.4	M+	C19H37NO4
Pantothenate	1.99	220.1182			219.1104	119.4	M+H	C9H17NO5
2-Hydroxypyridine	2.05	96.0447			95.0369	123	M+H	C5H5NO
N-Acetylglycine	2.13	118.051			117.0432	127.8	M+H	C4H7NO3
Phenylacetylglutamine	2.27	265.1186			264.1108	136.2	M+H	C13H16N2O4
Uracil	2.36	113.0346			112.0268	141.6	M+H	C4H4N2O2
Pyroglutamate	2.39	130.0504			129.0426	143.4	M+H	C5H7NO3
Glycocholate	2.69	466.316			465.3082	161.4	M+H	C26H43NO6
6-Hydroxynicotinate	2.8	162.0206			139.0308	168	M+Na	C6H5NO3
Kynurenic acid	2.91	190.0503			189.0425	174.6	M+H	C10H7NO3
Nicotinamide	3.12	123.0555			122.0477	187.2	M+H	C6H6N2O
Deoxyuridine	3.21	211.0717			228.0745	192.6	(M+H)+[-H2O]	C9H12N2O5
5-Hydroxyindole-3-Acetic Acid	3.45	192.0656			191.0578	207	M+H	C10H9NO3
N-Acetylglutamate	3.8	190.0711			189.0633	228	M+H	C7H11NO5
N-Acetylserine	3.8	130.0504			147.0532	228	(M+H)+[-H2O]	C5H9NO4
N6-(Delta2-Isopentenyl)-Adenine	3.92	204.1233			203.1155	235.2	M+H	C10H13N5
O-Acetylcarnitine	3.92	204.1232			204.1232	235.2	M+	C9H18NO4
N-Acetylaspartate	4.12	176.0553			175.0475	247.2	M+H	C6H9NO5
S-Carboxymethylcysteine	4.13	162.0219			179.0247	247.8	(M+H)+[-H2O]	C5H9NO4S
4-Pyridoxic acid	4.18	206.0449			183.0551	250.8	M+Na	C8H9NO4
Xanthurenate	4.18	206.045			205.0372	250.8	M+H	C10H7NO4
Ureidopropionate	4.25	133.0622			132.0544	255	M+H	C4H8N2O3
Aniline-2-Sulfonate	4.27	156.0119			173.0147	256.2	(M+H)+[-H2O]	C6H7NO3S
Orotate	4.44	139.0168			156.0196	266.4	(M+H)+[-H2O]	C5H4N2O4
Riboflavin	4.58	377.1456			376.1378	274.8	M+H	C17H20N4O6
N-Acetylasparagine	4.6	175.0719			174.0641	276	M+H	C6H10N2O4
Xanthine	4.67	153.0409			152.0331	280.2	M+H	C5H4N4O2
Sepiapterin	4.86	238.094			237.0862	291.6	M+H	C9H11N5O3
Succinate	4.87	119.0357			118.0279	292.2	M+H	C4H6O4
Hypoxanthine	4.87	137.0463			136.0385	292.2	M+H	C5H4N4O
1-Methyluric Acid	4.88	183.0519			182.0441	292.8	M+H	C6H6N4O3
3,4-Dihydroxybenzoate	4.93	137.0234			154.0262	295.8	(M+H)+[-H2O]	C7H6O4
Cotinine N-oxide	5.16	193.0982			192.0904	309.6	M+H	C10H12N2O2
3-Amino-4-Hydroxybenzoate	5.25	136.0398			153.0426	315	(M+H)+[-H2O]	C7H7NO3
Methylthioadenosine	5.26	298.0985			297.0907	315.6	M+H	C11H15N5O3S
Inosine	5.52	269.0886			268.0808	331.2	M+H	C10H12N4O5
Xanthosine	5.61	285.0834			284.0756	336.6	M+H	C10H12N4O6
Cotinine	5.7	177.1046			176.0968	342	M+H	C10H12N2O
Fucose	5.74	165.0768			164.069	344.4	M+H	C6H12O5
Pterin	5.75	164.0567			163.0489	345	M+H	C6H5N5O
3-Nitro-L-Tyrosine	5.85	209.0562			226.059	351	(M+H)+[-H2O]	C9H10N2O5
5'-Deoxyadenosine	5.87	274.0925			251.1027	352.2	M+Na	C10H13N5O3
Folate	5.91	464.1244			441.1346	354.6	M+Na	C19H19N7O6
Deoxyguanosine	6.01	290.0883			267.0985	360.6	M+Na	C10H13N5O4
D/L N-Acetylgalactosamine / D/L N-Acetylglucosamine / D/L N-Acetylmannosamine	6.03	204.0872			221.09	361.8	(M+H)+[-H2O]	C8H15NO6
Uric acid	6.15	169.0361			168.0283	369	M+H	C5H4N4O3
Allantoin	6.15	141.0411			158.0439	369	(M+H)+[-H2O]	C4H6N4O3
Glutarylcarnitine	6.24	276.1442			275.1361	374.4	M+H	C12H21NO6
L-Phenylalanine	6.25	166.0869			165.0791	375	M+H	C9H11NO2
Deoxyadenosine	6.26	252.1098			251.102	375.6	M+H	C10H13N5O3
L-Leucine	6.34	132.1022			131.0944	380.4	M+H	C6H13NO2
Kynurenine	6.38	209.0922			208.0844	382.8	M+H	C10H12N2O3
Malate	6.38	135.0304			134.0226	382.8	M+H	C4H6O5
Dopamine	6.38	136.0769			153.0797	382.8	(M+H)+[-H2O]	C8H11NO2
L-Isoleucine	6.45	132.1024			131.0946	387	M+H	C6H13NO2
Biopterin	6.46	238.0959			237.0881	387.6	M+H	C9H11N5O3
Guanosine	6.56	284.0995			283.0917	393.6	M+H	C10H13N5O5
Tryptamine	6.57	144.079			160.0977	394.2	(M+H)+[-NH3]	C10H12N2
Gluconate	6.69	219.0489			196.0591	401.4	M+Na	C6H12O7
Adenosine	6.73	268.1044			267.0966	403.8	M+H	C10H13N5O4
trans-3-hydroxycotinine	6.78	193.0976			192.0898	406.8	M+H	C10H12N2O2
Tryptophan	6.85	205.0966			204.0888	411	M+H	C11H12N2O2
Dihydrobiopterin	6.86	240.1092			239.1014	411.6	M+H	C9H13N5O3
2-Deoxy-D-Glucose	6.89	165.0758			164.068	413.4	M+H	C6H12O5
Galactitol	6.89	183.0866			182.0788	413.4	M+H	C6H14O6
Phenylethanolamine	6.89	142.0677			137.0885	413.4	(M+Na)-[H2O]	C8H11NO
2-Phosphoglycerate	6.91	187.0054			185.9976	414.6	M+H	C3H7O7P
Glucose	6.92	203.0533			180.0635	415.2	M+Na	C6H12O6
L-Methionine	6.96	150.0578			149.05	417.6	M+H	C5H11NO2S
Phenylglycine	6.97	152.0713			151.0635	418.2	M+H	C8H9NO2
3-Methoxytyramine	7.04	150.0922			167.095	422.4	(M+H)+[-H2O]	C9H13NO2
Deoxycarnitine	7.04	145.1126			145.1126	422.4	M+	C7H15NO2
Galacturonate / Glucuronate	7.14	217.033			194.0432	428.4	M+Na	C6H10O7
3-Hydroxybenzaldehyde	7.14	123.0446			122.0368	428.4	M+H	C7H6O2
Sorbate	7.16	95.0502			112.053	429.6	(M+H)+[-H2O]	C6H8O2
Inosine Monophosphate	7.2	349.057			348.0492	432	M+H	C10H13N4O8P
Trigonelline	7.21	138.0555			137.0477	432.6	M+H	C7H7NO2
Ectoine	7.22	143.082			142.0742	433.2	M+H	C6H10N2O2
7-Methylguanine	7.24	166.073			165.0652	434.4	M+H	C6H7N5O
3-Methoxytyrosine	7.26	212.0935			211.0857	435.6	M+H	C10H13NO4
Pipecolate	7.29	130.0867			129.0789	437.4	M+H	C6H11NO2
Betaine / L-Valine/ Norvaline	7.36	118.0866			117.0788	441.6	M+H	C5H11NO2
Hydroxykynurenine	7.38	225.087			224.0792	442.8	M+H	C10H12N2O4
Guanine	7.46	152.0571			151.0493	447.6	M+H	C5H5N5O
Adenine	7.47	136.0617			135.0539	448.2	M+H	C5H5N5
Aminocaproate	7.56	136.0759			131.0967	453.6	(M+Na)-[H2O]	C6H13NO2
L-Tyrosine	7.56	182.0816			181.0738	453.6	M+H	C9H11NO3
L-Tryptophanamide	7.57	186.1061			203.1089	454.2	(M+H)+[-H2O]	C11H13N3O
N-Methylglutamate	7.58	162.0768			161.069	454.8	M+H	C6H11NO4
L-Proline	7.58	116.0718			115.064	454.8	M+H	C5H9NO2
Cyclic AMP	7.62	330.0598			329.052	457.2	M+H	C10H12N5O6P
Sucrose / Trehalose / Lactose	7.64	365.1054			342.1156	458.4	M+Na	C12H22O11
Dimethylglycine	7.66	104.0709			103.0631	459.6	M+H	C4H9NO2
Choline	7.68	104.1077			104.1077	460.8	M+	C5H14NO
Taurine	7.77	126.022			125.0142	466.2	M+H	C2H7NO3S
4-Imidazoleacetate	7.87	127.0504			126.0426	472.2	M+H	C5H6N2O2
L-Cysteine	7.93	122.0272			121.0194	475.8	M+H	C3H7NO2S
trans-4-hrdroxy-L-proline	8	114.0547			131.0575	480	(M+H)+[-H2O]	C5H9NO3
Sarcosine	8.09	90.0551			89.0473	485.4	M+H	C3H7NO2
Aminoadipate	8.12	162.0767			161.0689	487.2	M+H	C6H11NO4
Aminoisobutanoate / 2-Aminoisobutyrate / Gamma-aminobutyrate	8.14	104.0709			103.0631	488.4	M+H	C4H9NO2
Creatine	8.17	132.0771			131.0693	490.2	M+H	C4H9N3O2
Serotonin	8.2	177.105			176.0972	492	M+H	C10H12N2O
Creatinine	8.22	114.0665			113.0587	493.2	M+H	C4H7N3O
Raffinose	8.38	527.1497			504.1599	502.8	M+Na	C18H32O16
N-Methyl-D-aspartic acid	8.43	148.0632			147.0554	505.8	M+H	C5H9NO4
L-Glutamic Acid	8.43	148.0632			147.0554	505.8	M+H	C5H9NO4
5-Hydroxytryptophan	8.43	221.0939			220.0861	505.8	M+H	C11H12N2O3
Alanine / D-Alanine	8.44	90.0551			89.0473	506.4	M+H	C3H7NO2
Carnitine	8.48	162.1125			161.1047	508.8	M+	C7H16NO3
cis-4-hydroxy-D-proline	8.5	132.0664			131.0586	510	M+H	C5H9NO3
Octopamine	8.52	154.0875			153.0797	511.2	M+H	C8H11NO2
1-Aminocyclopropanecarboxylate	8.56	102.055			101.0472	513.6	M+H	C4H7NO2
L-Threonine / Homoserine / Allothreonine	8.57	120.0657			119.0579	514.2	M+H	C4H9NO3
1-Methyladenosine	8.66	282.1204			281.1126	519.6	M+H	C11H15N5O4
5-aminolevulinic acid	8.7	132.0661			131.0583	522	M+H	C5H9NO3
5-Methylcytosine	8.71	126.0669			125.0591	522.6	M+H	C5H7N3O
N-Alpha-Acetyllysine	8.75	189.1231			188.1153	525	M+H	C8H16N2O3
Pro-Gly	8.77	173.0921			172.0843	526.2	M+H	C7H12N2O3
Glutamine	8.86	147.0768			146.069	531.6	M+H	C5H10N2O3
Adrenaline(Epinephrine)	8.87	188.068			183.0888	532.2	(M+Na)-[H2O]	C9H13NO3
1-Methylnicotinamide	8.88	120.0656			137.0684	532.8	(M+H)+[-H2O]	C7H9N2O
Glycine	8.88	76.0394			75.0316	532.8	M+H	C2H5NO2
Guanidinoacetate	8.88	118.0617			117.0539	532.8	M+H	C3H7N3O2
N-Acetylputrescine	8.89	131.118			130.1102	533.4	M+H	C6H14N2O
Cytidine 2',3'-Cyclic Phosphate	8.9	306.0493			305.0415	534	M+H	C9H12N3O7P
Deoxycytidine	8.91	228.0982			227.0904	534.6	M+H	C9H13N3O4
Guanidinosuccinate	8.94	176.0672			175.0594	536.4	M+H	C5H9N3O4
Citrulline	8.96	176.1034			175.0956	537.6	M+H	C6H13N3O3
L-Aspartic Acid	9.04	116.0345			133.0373	542.4	(M+H)+[-H2O]	C4H7NO4
Asparagine	9.04	133.0612			132.0534	542.4	M+H	C4H8N2O3
L-Serine	9.05	106.0503			105.0425	543	M+H	C3H7NO3
Cytosine	9.06	112.0508			111.043	543.6	M+H	C4H5N3O
Beta-Alanine	9.07	90.0563			89.0485	544.2	M+H	C3H7NO2
Diethanolamine	9.38	106.0863			105.0785	562.8	M+H	C4H11NO2
nicotine-1-N-oxide	9.4	179.1175			178.1097	564	M+H	C10H14N2O
Cytidine	9.42	244.0936			243.0858	565.2	M+H	C9H13N3O5
Nicotine	9.52	163.1234			162.1156	571.2	M+H	C10H14N2
6-Hydroxydopamine	9.91	170.0811			169.0733	594.6	M+H	C8H11NO3
Noradrenaline	9.92	170.0817			169.0739	595.2	M+H	C8H11NO3
S-Adenosylhomocysteine	10.66	385.1286			384.1208	639.6	M+H	C14H20N6O5S
L-Cystine	10.73	241.0303			240.0225	643.8	M+H	C6H12N2O4S2
Cystathionine	10.98	223.0722			222.0644	658.8	M+H	C7H14N2O4S
D/L Glucosamine/ D/L Galactosamine/ D-Mannosamine	11	162.0764			179.0793	660	(M+H)+[-H2O]	C6H13NO5
D/L Glucosamine / D/L Galactosamine	11.24	162.0764			179.0794	674.4	(M+H)+[-H2O]	C6H13NO5
Asymmetrical dimethylarginine	11.97	203.1504			202.1426	718.2	M+H	C8H18N4O2
L-Histidine	12.26	156.0773			155.0695	735.6	M+H	C6H9N3O2
1-Methyl-L-Histidine	12.45	170.0929			169.0851	747	M+H	C7H11N3O2
L-Arginine	12.9	175.1187			174.1109	774	M+H	C6H14N4O2
L-Lysine	13	147.1133			146.1055	780	M+H	C6H14N2O2
5-Hydroxylysine	13.25	163.1077			162.0999	795	M+H	C6H14N2O3
N,N,N-Trimethyllysine	13.34	189.1601			188.1523	800.4	M+H	C9H20N2O2
Anserine	13.55	241.1293			240.1215	813	M+H	C10H16N4O3
Carnosine	13.63	227.1149			226.1071	817.8	M+H	C9H14N4O3
S-Adenosylmethionine	14.86	399.1442			398.1364	891.6	M+H	C15H22N6O5S
Cadaverine	15.72	103.123			102.1152	943.2	M+H	C5H14N2
Histamine	15.88	112.0881			111.0803	952.8	M+H	C5H9N3
3-methylhistamine	15.97	126.1028			125.095	958.2	M+H	C6H11N3
METABOLITES_END
#END