#METABOLOMICS WORKBENCH Armando_Alcazar_20240220_140724 DATATRACK_ID:4664 STUDY_ID:ST003101 ANALYSIS_ID:AN005072 PROJECT_ID:PR001924
VERSION                          	1
CREATED_ON                       	02-06-2025
#PROJECT
PR:PROJECT_TITLE                 	Parallel pheromonal, metabolite, and lipid analyses reveal patterns associated
PR:PROJECT_TITLE                 	with early life transitions and ovary activation in honey bee (Apis mellifera)
PR:PROJECT_TITLE                 	queens
PR:PROJECT_SUMMARY               	We used a novel pheromone detection method to quantify retinue pheromone (QRP)
PR:PROJECT_SUMMARY               	concurrently with shotgun metabolomics and lipidomics analysis to determine what
PR:PROJECT_SUMMARY               	changes in pheromones and small molecules may underpin differences in age,
PR:PROJECT_SUMMARY               	laying status, and acceptance by workers in honey bee queens.
PR:INSTITUTE                     	University of British Columbia
PR:DEPARTMENT                    	Life Sciences Institute
PR:LAST_NAME                     	Alcazar Magana
PR:FIRST_NAME                    	Armando
PR:ADDRESS                       	2350 Health Sciences Mall, Vancouver, BC, V6T1Z3, Canada
PR:EMAIL                         	armando.alcazarmagana@ubc.ca
PR:PHONE                         	5416097172
PR:DOI                           	http://dx.doi.org/10.21228/M81B11
#STUDY
ST:STUDY_TITLE                   	Parallel pheromonal, metabolite, and lipid analyses reveal patterns associated
ST:STUDY_TITLE                   	with early life transitions and ovary activation in honey bee (Apis mellifera)
ST:STUDY_TITLE                   	queens
ST:STUDY_SUMMARY                 	We used a novel pheromone detection method to quantify retinue pheromone (QRP)
ST:STUDY_SUMMARY                 	concurrently with shotgun metabolomics and lipidomics analysis to determine what
ST:STUDY_SUMMARY                 	changes in pheromones and small molecules may underpin differences in age,
ST:STUDY_SUMMARY                 	laying status, and acceptance by workers in honey bee queens.
ST:INSTITUTE                     	University of British Columbia
ST:DEPARTMENT                    	Life Sciences Institute
ST:LAST_NAME                     	Alcazar Magana
ST:FIRST_NAME                    	Armando
ST:ADDRESS                       	2350 Health Sciences Mall, Vancouver, BC, V6T1Z3, Canada
ST:EMAIL                         	armando.alcazarmagana@ubc.ca
ST:PHONE                         	5416097172
ST:SUBMIT_DATE                   	2024-02-20
#SUBJECT
SU:SUBJECT_TYPE                  	Insect
SU:SUBJECT_SPECIES               	Apis mellifera
SU:GENDER                        	Female
SU:SPECIES_GROUP                 	Insects
#SUBJECT_SAMPLE_FACTORS:         	SUBJECT(optional)[tab]SAMPLE[tab]FACTORS(NAME:VALUE pairs separated by |)[tab]Additional sample data
SUBJECT_SAMPLE_FACTORS           	-	Q21	Sample source:Bee head | Treatment:Banked	RAW_FILE_NAME=Q21_11-1-2023_R-C6_14915; RAW_FILE_NAME=Q21_11-1-2023_R-C6_14980; RAW_FILE_NAME=Q21_11-3-2023_R-C6_15044; RAW_FILE_NAME=Q21_11-3-2023_R-C6_15103
SUBJECT_SAMPLE_FACTORS           	-	Q22	Sample source:Bee head | Treatment:Banked	RAW_FILE_NAME=Q22_11-1-2023_R-C7_14921; RAW_FILE_NAME=Q22_11-2-2023_R-C7_14986; RAW_FILE_NAME=Q22_11-3-2023_R-C7_15050; RAW_FILE_NAME=Q22_11-3-2023_R-C7_15109
SUBJECT_SAMPLE_FACTORS           	-	Q23	Sample source:Bee head | Treatment:Banked	RAW_FILE_NAME=Q23_11-1-2023_R-C8_14914; RAW_FILE_NAME=Q23_11-1-2023_R-C8_14979; RAW_FILE_NAME=Q23_11-3-2023_R-C8_15043; RAW_FILE_NAME=Q23_11-3-2023_R-C8_15102
SUBJECT_SAMPLE_FACTORS           	-	Q24	Sample source:Bee head | Treatment:Banked	RAW_FILE_NAME=Q24_11-1-2023_R-C9_14941; RAW_FILE_NAME=Q24_11-2-2023_R-C9_15006; RAW_FILE_NAME=Q24_11-3-2023_R-C9_15070; RAW_FILE_NAME=Q24_11-4-2023_R-C9_15129
SUBJECT_SAMPLE_FACTORS           	-	Q25	Sample source:Bee head | Treatment:Banked	RAW_FILE_NAME=Q25_11-1-2023_R-D1_14908; RAW_FILE_NAME=Q25_11-1-2023_R-D1_14973; RAW_FILE_NAME=Q25_11-2-2023_R-D1_15037; RAW_FILE_NAME=Q25_11-3-2023_R-D1_15096
SUBJECT_SAMPLE_FACTORS           	-	Q26	Sample source:Bee head | Treatment:Banked	RAW_FILE_NAME=Q26_11-1-2023_R-D2_14940; RAW_FILE_NAME=Q26_11-2-2023_R-D2_15005; RAW_FILE_NAME=Q26_11-3-2023_R-D2_15069; RAW_FILE_NAME=Q26_11-4-2023_R-D2_15128
SUBJECT_SAMPLE_FACTORS           	-	Q27	Sample source:Bee head | Treatment:Banked	RAW_FILE_NAME=Q27_11-1-2023_R-D3_14929; RAW_FILE_NAME=Q27_11-2-2023_R-D3_14994; RAW_FILE_NAME=Q27_11-3-2023_R-D3_15058; RAW_FILE_NAME=Q27_11-4-2023_R-D3_15117
SUBJECT_SAMPLE_FACTORS           	-	Q28	Sample source:Bee head | Treatment:Banked	RAW_FILE_NAME=Q28_10-31-2023_R-D4_14897; RAW_FILE_NAME=Q28_11-1-2023_R-D4_14962; RAW_FILE_NAME=Q28_11-2-2023_R-D4_15026; RAW_FILE_NAME=Q28_11-3-2023_R-D4_15085
SUBJECT_SAMPLE_FACTORS           	-	Q29	Sample source:Bee head | Treatment:Banked	RAW_FILE_NAME=Q29_10-31-2023_R-D5_14898; RAW_FILE_NAME=Q29_11-1-2023_R-D5_14963; RAW_FILE_NAME=Q29_11-2-2023_R-D5_15027; RAW_FILE_NAME=Q29_11-3-2023_R-D5_15086
SUBJECT_SAMPLE_FACTORS           	-	Q30	Sample source:Bee head | Treatment:Banked	RAW_FILE_NAME=Q30_10-31-2023_R-D6_14899; RAW_FILE_NAME=Q30_11-1-2023_R-D6_14964; RAW_FILE_NAME=Q30_11-2-2023_R-D6_15028; RAW_FILE_NAME=Q30_11-3-2023_R-D6_15087
SUBJECT_SAMPLE_FACTORS           	-	Q11	Sample source:Bee head | Treatment:Early mated	RAW_FILE_NAME=Q11_11-1-2023_R-B4_14920; RAW_FILE_NAME=Q11_11-2-2023_R-B4_14985; RAW_FILE_NAME=Q11_11-3-2023_R-B4_15049; RAW_FILE_NAME=Q11_11-3-2023_R-B4_15108
SUBJECT_SAMPLE_FACTORS           	-	Q12	Sample source:Bee head | Treatment:Early mated	RAW_FILE_NAME=Q12_11-1-2023_R-B5_14910; RAW_FILE_NAME=Q12_11-1-2023_R-B5_14975; RAW_FILE_NAME=Q12_11-2-2023_R-B5_15039; RAW_FILE_NAME=Q12_11-3-2023_R-B5_15098
SUBJECT_SAMPLE_FACTORS           	-	Q13	Sample source:Bee head | Treatment:Early mated	RAW_FILE_NAME=Q13_11-1-2023_R-B6_14938; RAW_FILE_NAME=Q13_11-2-2023_R-B6_15003; RAW_FILE_NAME=Q13_11-3-2023_R-B6_15067; RAW_FILE_NAME=Q13_11-4-2023_R-B6_15126
SUBJECT_SAMPLE_FACTORS           	-	Q14	Sample source:Bee head | Treatment:Early mated	RAW_FILE_NAME=Q14_11-1-2023_R-B7_14934; RAW_FILE_NAME=Q14_11-2-2023_R-B7_14999; RAW_FILE_NAME=Q14_11-3-2023_R-B7_15063; RAW_FILE_NAME=Q14_11-4-2023_R-B7_15122
SUBJECT_SAMPLE_FACTORS           	-	Q15	Sample source:Bee head | Treatment:Early mated	RAW_FILE_NAME=Q15_11-1-2023_R-B8_14911; RAW_FILE_NAME=Q15_11-1-2023_R-B8_14976; RAW_FILE_NAME=Q15_11-2-2023_R-B8_15040; RAW_FILE_NAME=Q15_11-3-2023_R-B8_15099
SUBJECT_SAMPLE_FACTORS           	-	Q16	Sample source:Bee head | Treatment:Early mated	RAW_FILE_NAME=Q16_11-1-2023_R-B9_14909; RAW_FILE_NAME=Q16_11-1-2023_R-B9_14974; RAW_FILE_NAME=Q16_11-2-2023_R-B9_15038; RAW_FILE_NAME=Q16_11-3-2023_R-B9_15097
SUBJECT_SAMPLE_FACTORS           	-	Q17	Sample source:Bee head | Treatment:Early mated	RAW_FILE_NAME=Q17_10-31-2023_R-C1_14903; RAW_FILE_NAME=Q17_11-1-2023_R-C1_14968; RAW_FILE_NAME=Q17_11-2-2023_R-C1_15032; RAW_FILE_NAME=Q17_11-3-2023_R-C1_15091
SUBJECT_SAMPLE_FACTORS           	-	Q18	Sample source:Bee head | Treatment:Early mated	RAW_FILE_NAME=Q18_11-1-2023_R-C2_14917; RAW_FILE_NAME=Q18_11-2-2023_R-C2_14982; RAW_FILE_NAME=Q18_11-3-2023_R-C2_15046; RAW_FILE_NAME=Q18_11-3-2023_R-C2_15105
SUBJECT_SAMPLE_FACTORS           	-	Q19	Sample source:Bee head | Treatment:Early mated	RAW_FILE_NAME=Q19_11-1-2023_R-C3_14916; RAW_FILE_NAME=Q19_11-2-2023_R-C3_14981; RAW_FILE_NAME=Q19_11-3-2023_R-C3_15045; RAW_FILE_NAME=Q19_11-3-2023_R-C3_15104
SUBJECT_SAMPLE_FACTORS           	-	Q20	Sample source:Bee head | Treatment:Early mated	RAW_FILE_NAME=Q20_10-31-2023_R-C4_14904; RAW_FILE_NAME=Q20_11-1-2023_R-C4_14969; RAW_FILE_NAME=Q20_11-2-2023_R-C4_15033; RAW_FILE_NAME=Q20_11-3-2023_R-C4_15092
SUBJECT_SAMPLE_FACTORS           	-	Q31	Sample source:Bee head | Treatment:Late mated	RAW_FILE_NAME=Q31_11-1-2023_R-D8_14925; RAW_FILE_NAME=Q31_11-2-2023_R-D8_14990; RAW_FILE_NAME=Q31_11-3-2023_R-D8_15054; RAW_FILE_NAME=Q31_11-3-2023_R-D8_15113
SUBJECT_SAMPLE_FACTORS           	-	Q32	Sample source:Bee head | Treatment:Late mated	RAW_FILE_NAME=Q32_11-1-2023_R-D9_14935; RAW_FILE_NAME=Q32_11-2-2023_R-D9_15000; RAW_FILE_NAME=Q32_11-3-2023_R-D9_15064; RAW_FILE_NAME=Q32_11-4-2023_R-D9_15123
SUBJECT_SAMPLE_FACTORS           	-	Q33	Sample source:Bee head | Treatment:Late mated	RAW_FILE_NAME=Q33_11-1-2023_R-E1_14912; RAW_FILE_NAME=Q33_11-1-2023_R-E1_14977; RAW_FILE_NAME=Q33_11-3-2023_R-E1_15041; RAW_FILE_NAME=Q33_11-3-2023_R-E1_15100
SUBJECT_SAMPLE_FACTORS           	-	Q34	Sample source:Bee head | Treatment:Late mated	RAW_FILE_NAME=Q34_11-1-2023_R-E2_14937; RAW_FILE_NAME=Q34_11-2-2023_R-E2_15002; RAW_FILE_NAME=Q34_11-3-2023_R-E2_15066; RAW_FILE_NAME=Q34_11-4-2023_R-E2_15125
SUBJECT_SAMPLE_FACTORS           	-	Q35	Sample source:Bee head | Treatment:Late mated	RAW_FILE_NAME=Q35_11-1-2023_R-E3_14928; RAW_FILE_NAME=Q35_11-2-2023_R-E3_14993; RAW_FILE_NAME=Q35_11-3-2023_R-E3_15057; RAW_FILE_NAME=Q35_11-4-2023_R-E3_15116
SUBJECT_SAMPLE_FACTORS           	-	Q36	Sample source:Bee head | Treatment:Late mated	RAW_FILE_NAME=Q36_11-1-2023_R-E4_14927; RAW_FILE_NAME=Q36_11-2-2023_R-E4_14992; RAW_FILE_NAME=Q36_11-3-2023_R-E4_15056; RAW_FILE_NAME=Q36_11-3-2023_R-E4_15115
SUBJECT_SAMPLE_FACTORS           	-	Q37	Sample source:Bee head | Treatment:Late mated	RAW_FILE_NAME=Q37_10-31-2023_R-E5_14900; RAW_FILE_NAME=Q37_11-1-2023_R-E5_14965; RAW_FILE_NAME=Q37_11-2-2023_R-E5_15029; RAW_FILE_NAME=Q37_11-3-2023_R-E5_15088
SUBJECT_SAMPLE_FACTORS           	-	Q38	Sample source:Bee head | Treatment:Late mated	RAW_FILE_NAME=Q38_11-1-2023_R-E6_14922; RAW_FILE_NAME=Q38_11-2-2023_R-E6_14987; RAW_FILE_NAME=Q38_11-3-2023_R-E6_15051; RAW_FILE_NAME=Q38_11-3-2023_R-E6_15110
SUBJECT_SAMPLE_FACTORS           	-	Q39	Sample source:Bee head | Treatment:Late mated	RAW_FILE_NAME=Q39_10-31-2023_R-E7_14901; RAW_FILE_NAME=Q39_11-1-2023_R-E7_14966; RAW_FILE_NAME=Q39_11-2-2023_R-E7_15030; RAW_FILE_NAME=Q39_11-3-2023_R-E7_15089
SUBJECT_SAMPLE_FACTORS           	-	Q40	Sample source:Bee head | Treatment:Late mated	RAW_FILE_NAME=Q40_11-1-2023_R-E8_14924; RAW_FILE_NAME=Q40_11-2-2023_R-E8_14989; RAW_FILE_NAME=Q40_11-3-2023_R-E8_15053; RAW_FILE_NAME=Q40_11-3-2023_R-E8_15112
SUBJECT_SAMPLE_FACTORS           	-	V1	Sample source:Bee head | Treatment:Virgin	RAW_FILE_NAME=V1_11-1-2023_R-A2_14936; RAW_FILE_NAME=V1_11-2-2023_R-A2_15001; RAW_FILE_NAME=V1_11-3-2023_R-A2_15065; RAW_FILE_NAME=V1_11-4-2023_R-A2_15124
SUBJECT_SAMPLE_FACTORS           	-	V10	Sample source:Bee head | Treatment:Virgin	RAW_FILE_NAME=V10_11-1-2023_R-B2_14932; RAW_FILE_NAME=V10_11-2-2023_R-B2_14997; RAW_FILE_NAME=V10_11-3-2023_R-B2_15061; RAW_FILE_NAME=V10_11-4-2023_R-B2_15120
SUBJECT_SAMPLE_FACTORS           	-	V2	Sample source:Bee head | Treatment:Virgin	RAW_FILE_NAME=V2_10-31-2023_R-A3_14896; RAW_FILE_NAME=V2_11-1-2023_R-A3_14961; RAW_FILE_NAME=V2_11-2-2023_R-A3_15025; RAW_FILE_NAME=V2_11-3-2023_R-A3_15084
SUBJECT_SAMPLE_FACTORS           	-	V3	Sample source:Bee head | Treatment:Virgin	RAW_FILE_NAME=V3_11-1-2023_R-A4_14913; RAW_FILE_NAME=V3_11-1-2023_R-A4_14978; RAW_FILE_NAME=V3_11-3-2023_R-A4_15042; RAW_FILE_NAME=V3_11-3-2023_R-A4_15101
SUBJECT_SAMPLE_FACTORS           	-	V4	Sample source:Bee head | Treatment:Virgin	RAW_FILE_NAME=V4_10-31-2023_R-A5_14905; RAW_FILE_NAME=V4_11-1-2023_R-A5_14970; RAW_FILE_NAME=V4_11-2-2023_R-A5_15034; RAW_FILE_NAME=V4_11-3-2023_R-A5_15093
SUBJECT_SAMPLE_FACTORS           	-	V5	Sample source:Bee head | Treatment:Virgin	RAW_FILE_NAME=V5_10-31-2023_R-A6_14902; RAW_FILE_NAME=V5_11-1-2023_R-A6_14967; RAW_FILE_NAME=V5_11-2-2023_R-A6_15031; RAW_FILE_NAME=V5_11-3-2023_R-A6_15090
SUBJECT_SAMPLE_FACTORS           	-	V6	Sample source:Bee head | Treatment:Virgin	RAW_FILE_NAME=V6_11-1-2023_R-A7_14933; RAW_FILE_NAME=V6_11-2-2023_R-A7_14998; RAW_FILE_NAME=V6_11-3-2023_R-A7_15062; RAW_FILE_NAME=V6_11-4-2023_R-A7_15121
SUBJECT_SAMPLE_FACTORS           	-	V7	Sample source:Bee head | Treatment:Virgin	RAW_FILE_NAME=V7_11-1-2023_R-A8_14939; RAW_FILE_NAME=V7_11-2-2023_R-A8_15004; RAW_FILE_NAME=V7_11-3-2023_R-A8_15068; RAW_FILE_NAME=V7_11-4-2023_R-A8_15127
SUBJECT_SAMPLE_FACTORS           	-	V8	Sample source:Bee head | Treatment:Virgin	RAW_FILE_NAME=V8_11-1-2023_R-A9_14926; RAW_FILE_NAME=V8_11-2-2023_R-A9_14991; RAW_FILE_NAME=V8_11-3-2023_R-A9_15055; RAW_FILE_NAME=V8_11-3-2023_R-A9_15114
SUBJECT_SAMPLE_FACTORS           	-	V9	Sample source:Bee head | Treatment:Virgin	RAW_FILE_NAME=V9_11-1-2023_R-B1_14923; RAW_FILE_NAME=V9_11-2-2023_R-B1_14988; RAW_FILE_NAME=V9_11-3-2023_R-B1_15052; RAW_FILE_NAME=V9_11-3-2023_R-B1_15111
#COLLECTION
CO:COLLECTION_SUMMARY            	Queens were produced by Scandia Honey in May 2023 in Scandia, AB, Canada,
CO:COLLECTION_SUMMARY            	according to standard queen rearing methods.
CO:SAMPLE_TYPE                   	queen bee head
CO:STORAGE_CONDITIONS            	-80℃
#TREATMENT
TR:TREATMENT_SUMMARY             	very young (≤ 1 day old) larvae were grafted from a single mother colony into
TR:TREATMENT_SUMMARY             	queen cell cups (JZBZ) and reared into queen cells in strong cell builder
TR:TREATMENT_SUMMARY             	colonies. Ten days after grafting (June 1), queen cells were placed in mating
TR:TREATMENT_SUMMARY             	nucleus colonies (nucs).
#SAMPLEPREP
SP:SAMPLEPREP_SUMMARY            	two-phase extraction was conducted according to methods previously described at
SP:SAMPLEPREP_SUMMARY            	J. Lipid Res. 49, 1137–1146 (2008)
SP:PROCESSING_STORAGE_CONDITIONS 	4℃
SP:EXTRACT_STORAGE               	-80℃
#CHROMATOGRAPHY
CH:CHROMATOGRAPHY_SUMMARY        	Separation of compounds was achieved using a multigradient method on an Inertsil
CH:CHROMATOGRAPHY_SUMMARY        	Ph-3 UHPLC column (2 µm, 150 x 2.1 mm) (GL Sciences) equipped with a Ph-3 guard
CH:CHROMATOGRAPHY_SUMMARY        	column (2 µm, 2.1 x 10 mm
CH:INSTRUMENT_NAME               	Thermo Vanquish
CH:COLUMN_NAME                   	Inertsil Ph-3 UHPLC column (2 µm, 150 x 2.1 mm)
CH:COLUMN_TEMPERATURE            	55
CH:FLOW_GRADIENT                 	0 min (5% B), 0–1 min (5% B), 1–8 min (35% B), 8–10.5 min (99% B),
CH:FLOW_GRADIENT                 	10.5–14 min (99% B), 14–14.5 min (5% B), and 14.5–18 min (5% B)
CH:FLOW_RATE                     	0.3 ml/min
CH:SOLVENT_A                     	100% water; 0.1% formic acid
CH:SOLVENT_B                     	100% methanol; 0.1% formic acid
CH:CHROMATOGRAPHY_TYPE           	Reversed phase
#ANALYSIS
AN:ANALYSIS_TYPE                 	MS
#MS
MS:INSTRUMENT_NAME               	Bruker Impact II
MS:INSTRUMENT_TYPE               	QTOF
MS:MS_TYPE                       	ESI
MS:MS_COMMENTS                   	For positive ion mode, the mass spectrometer settings were as follows: capillary
MS:MS_COMMENTS                   	voltage of 4500 V, nebulizer gas pressure of 2.0 bar, dry gas flow rate of 9 L
MS:MS_COMMENTS                   	min-1, dry gas temperature of 220°C, mass scan range of 60-1300 m/z, and a
MS:MS_COMMENTS                   	total cycle time of 0.6 s. To obtain comprehensive structural information,
MS:MS_COMMENTS                   	collision energy of 20 V was ramped through each MS/MS scan from 100 to 250%.
MS:ION_MODE                      	POSITIVE
MS:MS_RESULTS_FILE               	ST003101_AN005072_Results.txt	UNITS:Rel Abundance	Has m/z:Yes	Has RT:Yes	RT units:Minutes
#MS_METABOLITE_DATA
MS_METABOLITE_DATA:UNITS         	Rel Abundance
MS_METABOLITE_DATA_START
Samples	Q21	Q22	Q23	Q24	Q25	Q26	Q27	Q28	Q29	Q30	Q11	Q12	Q13	Q14	Q15	Q16	Q17	Q18	Q19	Q20	Q31	Q32	Q33	Q34	Q35	Q36	Q37	Q38	Q39	Q40	V1	V10	V2	V3	V4	V5	V6	V7	V8	V9
Factors	Sample source:Bee head | Treatment:Banked	Sample source:Bee head | Treatment:Banked	Sample source:Bee head | Treatment:Banked	Sample source:Bee head | Treatment:Banked	Sample source:Bee head | Treatment:Banked	Sample source:Bee head | Treatment:Banked	Sample source:Bee head | Treatment:Banked	Sample source:Bee head | Treatment:Banked	Sample source:Bee head | Treatment:Banked	Sample source:Bee head | Treatment:Banked	Sample source:Bee head | Treatment:Early mated	Sample source:Bee head | Treatment:Early mated	Sample source:Bee head | Treatment:Early mated	Sample source:Bee head | Treatment:Early mated	Sample source:Bee head | Treatment:Early mated	Sample source:Bee head | Treatment:Early mated	Sample source:Bee head | Treatment:Early mated	Sample source:Bee head | Treatment:Early mated	Sample source:Bee head | Treatment:Early mated	Sample source:Bee head | Treatment:Early mated	Sample source:Bee head | Treatment:Late mated	Sample source:Bee head | Treatment:Late mated	Sample source:Bee head | Treatment:Late mated	Sample source:Bee head | Treatment:Late mated	Sample source:Bee head | Treatment:Late mated	Sample source:Bee head | Treatment:Late mated	Sample source:Bee head | Treatment:Late mated	Sample source:Bee head | Treatment:Late mated	Sample source:Bee head | Treatment:Late mated	Sample source:Bee head | Treatment:Late mated	Sample source:Bee head | Treatment:Virgin	Sample source:Bee head | Treatment:Virgin	Sample source:Bee head | Treatment:Virgin	Sample source:Bee head | Treatment:Virgin	Sample source:Bee head | Treatment:Virgin	Sample source:Bee head | Treatment:Virgin	Sample source:Bee head | Treatment:Virgin	Sample source:Bee head | Treatment:Virgin	Sample source:Bee head | Treatment:Virgin	Sample source:Bee head | Treatment:Virgin	
10-hydroxy-2-decenoic Acid	19906.2496	27429.9091	45288.0247	36822.9406	19852.3182	15687.0490	17102.6397	44571.8535	38730.8281	20346.4155	68532.3048	65909.6067	52726.0968	47167.0982	65102.7879	80925.1218	75666.5255	43866.2029	18666.5189	66717.2366	43263.6756	48199.6611	17950.5713	58205.9615	36799.0981	51236.5316	43158.7170	40658.9788	48247.0276	27950.3476	83748.9052	65599.2198	92967.1329	111348.3571	44888.3238	79502.2440	98268.9508	51675.8288	111031.8317	50023.4715
20-COOH-leukotriene E4	2693.8154	3011.3898	4340.8332	2943.5126	3235.4488	1908.0053	1731.2559	1715.0537	3068.8023	1655.5405	1031.3641	1295.6628	1211.2121	1322.0965	1046.8564	1391.3708	1505.3665	910.5548	757.0643	967.1739	1423.6894	1992.9424	1424.3994	1579.3326	2063.3988	2149.8294	1859.3942	3760.0677	2205.4822	1959.8508	278.6516	251.1029	229.7992	265.3614	124.9935	219.2845	514.1065	109.1214	325.5272	163.0288
2_6-nonadien-1-ol	3376.8830	3399.2561	4997.9230	4470.0246	3685.3879	2409.5723	3114.7707	4902.0643	5730.1305	3525.4391	4694.0835	5398.7268	4022.8350	3939.7961	4837.5668	5145.2973	5536.8645	3953.5023	2483.9662	5006.2916	3942.4113	4186.6711	3074.0508	4672.8565	4072.9582	4409.6913	4853.9418	4166.2180	5680.1485	3457.1551	4460.5721	4099.0233	6755.5466	5649.6069	2960.6809	5632.0530	4228.5609	3247.4003	5677.6668	3627.0608
2-amino-1-phenylethanol	18037.5495	28957.6151	28688.0917	23474.4984	25543.0269	27326.4696	30532.0431	29197.5927	33276.3123	24104.0321	39574.6360	23079.7893	33426.8109	25155.0409	27282.7113	28131.6689	23363.1712	31686.7355	26525.3604	34211.7198	31711.8494	24322.4436	34102.6446	43100.4930	38604.7246	36832.1887	32387.1446	30002.5818	25326.1869	28560.2202	170885.6050	187655.0620	87205.5743	95090.0528	222793.5089	100802.3226	97637.1326	198227.1907	119118.4459	185625.5326
3_4-dihydroxydecanoylcarnitine	235.8726	111.4915	314.8446	215.5779	280.3669	97.9897	57.8740	122.0002	197.7439	91.6666	367.4299	465.6781	254.0808	398.9136	581.8296	450.1609	684.1092	417.8170	201.0969	481.6571	118.4379	227.0104	116.7159	103.5918	135.9685	314.6983	89.6522	198.8661	179.9541	140.3058	28.9529	28.1562	44.4920	66.7489	20.8198	52.2337	71.8901	10.4528	37.2773	19.1421
3-hydroxy-DL-kynurenine	5547.3858	5376.3675	5720.9624	6391.1161	4900.3897	6604.3250	5914.7210	6288.6716	5102.7898	5038.4575	15783.3850	16326.7065	15993.7614	15160.5828	11989.9317	15947.0470	12465.9353	14954.5888	13710.6891	10325.0670	4766.7325	6676.7887	6599.0141	7992.5322	8839.0878	5605.5009	6214.3304	9120.9990	5363.9179	6395.5246	54786.4478	49411.4450	41861.2659	54306.7253	46526.5166	57096.0934	48379.6838	46227.9804	51608.2298	58628.2246
4-hydroxy-3-methoxyphenylethanol	6502.3198	5327.5984	5680.7493	5483.6361	5677.6035	6469.8110	3288.5007	11473.5987	2674.5066	4395.5759	7861.1205	4420.6278	12700.4580	2182.0427	1484.9946	3458.2913	5290.7279	5438.5805	5729.8745	2645.7457	6646.5248	9106.6521	5246.4504	15090.6188	10615.3758	12476.1144	15130.2963	8942.2590	5297.3938	11374.3182	765.7657	733.8235	603.4180	622.4105	825.3392	692.6372	664.4377	967.5300	797.7223	846.9558
5^-deoxy-5^-(methylthio)adenosine	5340.1837	3219.4001	14642.6114	7537.9290	4112.5622	4218.3314	2688.3638	5745.6735	5344.0108	2364.5439	3993.8114	4399.9808	3708.4753	4002.9052	3412.1015	6950.2596	3783.3839	4286.4856	2396.3554	2605.5894	5374.2662	9106.6885	5600.7509	5246.4004	6455.4748	7137.1830	5178.4005	7345.7407	4230.7566	4634.4912	2791.3560	2116.1536	1405.7230	2282.9219	2832.5721	2017.7414	2354.7798	2478.4171	2095.7462	2552.5410
9(R)-hydroxydec-2(E)-enoic acid	360152.5931	302542.9721	395347.0102	525236.9193	390277.6703	332779.9831	438932.8531	302372.7126	533230.8534	388717.8022	188377.2842	236127.9747	265173.9326	268931.3540	224764.0348	259050.2177	226348.0427	232906.8360	180235.1080	172708.6400	320804.1013	384659.7077	323583.2395	378613.3532	408614.6181	370689.3020	388011.5993	513852.1185	424900.8289	380962.7604	153322.2672	210217.7521	101269.4043	178451.8980	41254.2143	112537.0787	252257.9466	46478.4137	187634.8239	93397.9650
acetylhistamine	2072.8561	5752.9316	2732.4406	2089.2193	1299.9185	3543.1393	2842.3742	1671.0188	1971.5832	3398.1622	319.7375	206.9656	490.9241	407.2346	744.6425	348.3096	569.0913	254.6135	819.7077	510.8492	1154.4441	1491.7088	1687.6360	2374.6344	1548.5781	2008.2108	4601.1398	1185.3437	2594.1026	2697.2593	72.9232	54.4361	98.8746	70.8827	98.2855	106.1585	106.0990	71.8354	62.7775	98.2790
acetyl-L-carnitine	789.8760	1438.6308	553.2818	754.0587	704.6927	1254.4598	761.2710	719.7252	707.5275	876.9971	459.8994	354.8745	450.7135	377.3063	456.2752	385.0596	434.2525	393.3013	360.0520	379.1362	517.2212	586.0961	370.1564	369.4597	466.5635	362.1693	293.3879	274.6133	255.8339	347.3539	851.0129	436.2635	443.1235	377.9501	762.4749	449.1722	420.7504	634.8409	395.9846	595.8829
acetylputrescine	230.7512	452.2482	213.2514	261.4183	142.3289	324.7216	218.9648	174.3440	178.3728	229.4216	101.3444	104.2533	108.1010	117.7973	109.0513	95.6323	125.4384	115.5233	176.2579	125.3279	112.9151	162.2572	121.5632	140.1617	107.3477	134.2072	214.2696	82.2451	99.7570	115.5726	145.9069	106.1850	113.1924	142.0174	172.3543	103.5877	101.9506	183.4035	103.2828	225.6233
adenosine	18933.9884	22327.5695	16962.7571	14539.6436	17608.6567	19566.7627	16676.5425	14966.4331	14623.6514	16891.5712	13064.5071	11815.4271	12644.2921	12761.5358	11494.2412	11023.0716	10296.3388	11252.9224	14285.7416	11934.5438	16715.4712	18189.9417	16870.4217	17259.7968	14248.6462	16904.0756	11285.7381	14782.5637	14220.8896	12807.3334	19100.2176	17879.9109	15010.5423	19285.2010	13061.6181	19867.2806	19220.5687	13759.9319	17723.1657	15872.4010
alpinetin methyl ether	253.8063	309.5169	332.4258	289.4866	274.2164	303.9443	197.8823	231.0303	233.1215	161.5080	108.0532	312.0514	247.5713	206.6708	154.6828	330.6087	470.8338	186.4057	319.2570	130.8422	224.8456	324.0947	169.9578	645.4556	375.7881	189.9584	391.4699	434.7157	439.5220	240.8247	58.5481	76.9375	53.1662	58.0363	65.3895	51.4575	54.4685	78.5472	60.2133	55.8525
beta-nicotinamide adenine dinucleotide	5247.7271	3360.2349	3677.4726	3481.4749	4680.3112	3509.1274	4843.1713	4835.0509	5164.5734	5258.5386	4228.6788	4735.5383	4404.9343	4118.6760	4601.0896	5027.7547	5087.9621	4844.8847	4598.8970	4932.3798	3261.6633	2975.3907	3529.8922	3584.2469	3290.3277	3736.3085	3698.6048	4088.3866	4230.0038	4645.0176	3223.3165	4150.4917	2676.9929	3668.3850	3803.2426	3944.8002	4406.7461	4030.3986	4191.3255	3560.2437
caffeine 13C3	18996.7784	23915.0517	23348.1867	23890.0343	23580.3847	19223.0648	23966.1088	23858.9882	26578.6972	27284.4300	24614.0251	23162.7359	24834.9228	22746.7523	23386.9908	23245.5570	23043.6857	23864.5252	23999.2649	23570.0333	23975.3281	22697.0125	23559.2208	22324.6345	22634.8487	23407.6406	24981.7817	23286.5612	25540.2397	23322.2134	24841.4762	24851.6615	29796.0076	25423.1672	26186.3711	26330.2034	24241.5067	25473.3154	25077.2303	26050.4343
carbamoylpyrrolidine-2-carboxylic acid	142.5260	160.9733	165.6560	164.3038	339.1946	146.3998	162.0711	135.4485	164.2170	163.9841	529.9898	271.0241	477.7099	171.0039	327.2264	361.0580	475.0845	376.2803	234.6656	249.6063	458.0401	808.3772	715.7507	777.1520	296.1069	447.4755	613.0834	581.9972	656.4454	658.0043	20932.8366	13841.3370	11323.2162	14574.7675	9173.5775	18069.1230	10442.5438	6016.5842	13915.1900	11132.8409
carnitine	3650.1863	4260.4076	3295.2019	3324.3190	3107.0823	3389.6295	5149.1818	3366.6017	3906.5112	3198.0547	3844.9254	5184.5243	3829.1710	5096.0021	6583.7316	4751.9289	5504.8542	4954.2732	3739.2218	5110.5238	1325.8598	1462.2062	772.3339	852.3963	758.3299	760.8737	524.4532	1313.9534	509.1011	561.2948	4797.1686	5437.8516	4343.3573	4460.1157	5592.4885	5217.8032	5225.2052	5347.2376	4792.4932	4404.9746
cinnamaldehyde	507.0804	683.9791	1109.2497	881.9123	413.2834	600.4271	334.4315	1245.5370	814.5050	329.1886	1999.9585	2066.1947	1752.3811	2377.1929	785.9720	2810.8961	3278.5164	1979.1998	1725.9041	1486.4998	725.4864	862.2316	587.2118	1618.0818	1134.1353	1380.3788	1416.2968	1218.7915	1898.1934	834.5289	119.2182	646.0966	340.1302	998.2516	38.5861	409.2275	1340.8535	59.3690	918.0973	86.9482
cuminyl alcohol	36522.8869	36235.1520	48494.0595	47063.6374	38304.2975	29363.7965	37444.9234	46313.4835	55763.5647	36739.6361	44885.5113	47723.0700	42323.8175	40946.4804	45037.7100	49172.5780	50685.7218	39583.0211	27421.4938	45183.4456	41333.6772	43770.8665	33992.6626	47963.1866	43724.0533	47792.6802	46841.1058	44810.2864	52340.2651	37608.5360	46723.5442	39715.4812	54074.4024	52343.4419	35026.2314	48815.3115	43445.6819	34892.9090	51506.3995	39162.7021
delta-octanolactone	25700.7155	22610.6307	25088.9791	15578.4924	19149.0602	10494.3513	13208.2443	21805.4144	26429.7318	17945.2342	16554.1097	12233.3510	14459.0962	11547.8613	18382.2628	15446.3962	19812.6390	15350.6426	8229.9977	18343.6111	19340.2563	22897.3715	25858.9735	20720.4549	26339.0732	23729.1319	25930.4566	30083.0569	44161.9624	20991.7519	4400.3671	5883.4706	9818.3031	7929.2686	1783.5832	9323.6177	9490.1414	1573.9976	9465.2731	2595.3270
dopamine	2953.1181	3801.5062	3572.5560	3324.5767	3124.8935	2669.4380	3793.0242	2870.6744	3885.4823	3544.8322	4153.2682	2324.5191	1710.2985	1819.0633	1667.8464	2921.6767	2302.3911	2670.0127	2617.8978	2342.7889	2797.8730	2594.4667	3004.6677	4683.3421	4656.0982	6162.1531	3548.4559	3314.5579	2708.6837	2715.5549	30405.4571	28279.2804	15975.3902	15302.4699	65240.6710	25551.5836	14934.7977	40158.6209	20264.0616	40861.3688
dopamine quinone	128.6514	106.2314	213.9365	454.3747	107.8332	233.3514	248.9073	118.8425	113.7680	95.2292	382.9867	239.1678	551.9265	721.1996	234.4180	368.4697	212.5428	277.3316	490.9353	352.8880	150.6402	145.3915	93.5436	144.0885	254.0472	76.0695	214.9362	230.1970	316.3081	194.2466	666.7323	703.5953	598.8829	578.3323	638.6945	617.9373	682.1389	740.7504	723.3693	651.4237
D-phenylalanine-d5	26174.3677	26501.3315	27305.8566	30581.1106	31326.8334	28612.9453	31230.3045	27026.3198	28965.7946	29683.1010	26914.3683	28510.2099	31216.2916	28152.4645	29606.9110	27070.2882	29356.1174	31796.0049	28647.1199	28228.4513	27114.6804	32368.4322	31833.8974	28749.0835	29585.1791	27084.6066	28745.0053	30792.8309	28865.5969	30517.7332	25573.9564	26718.2952	24668.1767	27552.8157	22403.4322	21587.5427	23170.3995	24611.4400	23690.0709	25389.8949
E-3-(4-hydroxy-3-methoxyphenyl)-prop-2-en-1-ol	67.8150	86.4116	90.2654	95.4689	72.3339	103.1184	69.1645	138.0419	66.3170	72.9493	272.6941	113.3610	314.0462	94.5714	95.2365	166.3408	156.4986	166.8854	223.3080	83.9407	94.3708	131.7714	63.4475	139.6251	163.1461	104.3531	139.0024	116.2345	90.5635	108.4494	42.0304	55.3672	46.7489	46.2038	48.2110	75.8995	72.9474	60.7752	60.4438	53.8991
E-9-oxodec-2-enoic acid	356167.8429	326437.9892	395401.1352	361448.4960	336573.1716	337556.1143	325213.6617	428573.1477	250706.8564	274066.8413	384521.8538	366709.9455	347786.6026	396723.9056	346703.7900	383796.8809	463926.5758	375785.7208	305917.8268	369008.5934	247607.0130	345802.9813	301424.7743	352363.6824	328976.6608	356348.1522	332064.2739	360647.4630	371673.0877	269774.8952	42188.5128	97445.0814	63244.0799	49725.4326	10689.9475	77870.4867	150096.0766	11894.1249	122218.8799	21194.7797
estragole	197659.9675	183677.3255	207925.1323	204702.7454	188069.1928	197239.6039	183415.1952	221970.3783	154631.7295	158913.6313	214103.1308	204672.2602	203731.4302	223476.0556	198084.3719	205280.6670	245402.8471	209455.9357	191113.3263	205221.8590	149656.1790	193431.5036	173759.9560	192752.1496	187365.3343	195370.5746	183473.9530	198438.6979	197223.7279	162804.4233	55496.0250	86949.4554	56155.2688	56966.4480	17963.1365	70307.8320	102218.5318	26807.7134	98555.6464	36132.0015
ethylcarboxamidoadenosine	9188.2862	10535.6565	8743.3846	10213.5205	6194.8664	11286.7598	12695.8651	8836.4366	9168.0407	6439.6152	10765.5317	4739.1322	6696.1962	6662.4150	864.1272	5764.7661	5267.2498	6318.2727	5097.8570	8193.7933	15702.1554	18732.4010	16478.8986	12172.6389	10971.1414	11907.5414	7657.8396	9857.5008	11789.8492	10481.2236	5822.1170	4621.3567	2219.4960	4516.2843	3801.7157	4377.4832	5096.6134	3570.3753	3919.1006	3414.9572
ferulic acid-d3	27874.7379	30397.5958	28860.3752	31502.0041	29419.4807	31607.0820	27718.7010	28055.2148	31205.9525	27276.1297	27862.6431	28448.4488	31742.6780	30588.2062	27086.6286	27620.8530	27273.5664	28438.6384	28505.1409	30410.4261	29432.7808	33632.3505	25389.5550	27164.7222	28414.1837	29775.7141	30920.6619	28726.7991	31264.1793	30521.2653	30924.3679	30504.4714	32940.7363	28107.6116	32666.5125	31016.8262	30204.1683	35387.6465	30099.1657	34501.1987
fructoselysine	301.0113	311.7163	346.0036	290.6197	268.0168	424.7009	374.3870	252.5439	244.6970	209.1077	297.7017	205.9057	240.3370	162.2363	193.1218	196.1733	211.8176	267.1186	245.6707	302.4389	409.2286	419.1305	478.5961	430.7407	322.0203	365.2808	251.6430	358.7517	421.0971	320.5353	300.0463	311.3421	170.2322	271.2672	312.2329	221.6959	212.0814	323.7262	252.7985	259.5824
galactosamine	17407.2514	3387.8132	15921.0922	3580.2955	10894.6790	9777.9130	4055.4064	6864.7292	15749.1215	7090.5252	9873.1010	9625.0262	8916.3681	9550.7651	12993.5306	8521.4144	10175.0056	10169.7979	8531.1898	8827.1071	15722.7279	2645.9239	11851.1904	7708.1202	9859.4417	1702.0139	5432.0166	11392.7297	4761.3808	11491.3345	3192.6823	1288.0095	4628.7727	3677.0176	3820.4110	2203.2477	6012.4418	2083.8315	3255.6934	1983.5233
gamma-aminobutyric acid	2679.9859	2187.9791	2202.1094	1625.1977	1498.2324	1857.9353	2114.6139	2681.6592	2213.2267	2915.4952	1793.3923	2053.3735	1732.5721	2105.1354	1848.1527	2081.1292	1984.9993	2162.0774	1900.2303	2445.3222	2375.0891	1546.1459	2417.4535	2055.5267	1830.0087	1486.1414	2416.5470	1618.7180	1858.0442	2310.1737	1756.6577	1370.6359	1678.8063	1763.8464	2541.8315	1771.3200	2074.1265	1838.0298	1894.3781	1742.9870
gamma-glutamylglutamine	3337.5424	2958.0370	2962.9325	3011.3512	3287.0883	2961.8688	4274.6652	2979.7742	3197.9583	3764.4957	2773.1401	1722.1034	2565.8176	1868.2119	2571.2152	2336.0416	1953.7922	2630.2241	1882.6049	2944.0473	3753.6206	2781.8923	3803.3884	2677.3433	3047.5017	3550.0145	3330.3329	3220.9733	3483.9242	3109.6539	1626.4904	1537.4801	964.3042	1267.3939	2628.3807	1485.6299	1454.1171	3150.8824	1134.2169	1951.7424
gamma-glutamylphenylalanine	1047.6458	1250.6025	1396.4410	1488.1977	1258.2235	1349.5159	1652.2018	1199.2829	1422.2984	1236.3751	2263.0248	1254.4478	1497.6542	1281.7661	1412.6643	1819.3327	1167.6258	1788.9099	1460.9263	2089.5770	2206.4425	1230.7363	1588.5188	2091.9955	1768.9923	2704.7787	1993.9878	1336.3828	1507.9729	1693.5389	9151.0893	7104.1926	3142.0390	4480.2073	11030.5934	4949.4850	5524.7427	13167.3702	5840.6102	7132.6353
gamma-glutamyltyrosine	773.8745	779.9231	747.0553	672.7516	843.4209	759.6689	863.7220	751.9536	741.4269	722.3457	1324.7204	768.7806	815.1844	696.6060	750.3767	1002.6213	771.1858	1173.3972	851.4112	1109.5191	1018.4698	903.9598	1177.1188	1185.8772	1036.8275	1355.0081	1407.1988	995.0348	858.4299	950.6428	4060.8161	4561.4594	1886.5241	3251.6974	7633.0118	2977.7736	2935.9816	8797.3644	2374.5928	4041.6875
glutamic acid	118251.3056	127815.7299	122042.3251	110900.6057	121832.2949	114652.4430	130611.1220	129950.8049	145591.0729	126321.4756	125530.2850	118622.6688	132233.1562	110680.2922	132588.3353	120265.2793	111415.5722	125646.9278	108398.8391	131038.0148	127952.1871	123287.3778	145102.7646	133923.6048	128397.4821	152604.5364	121140.5665	130312.8307	122637.2833	91725.7357	98212.1049	105359.7848	95685.8619	93935.5900	106834.5086	104856.0736	103814.8823	103644.7465	94073.5709	112415.2375
glutamine	92119.5466	105285.1241	99908.2683	86645.5771	104861.4838	88923.6034	101995.8345	111668.1849	125384.2201	105462.1659	101504.1190	96279.9956	107811.6364	81266.6576	110467.5135	101697.4279	90101.8413	98980.4749	85435.9443	108972.9117	101727.3885	102193.3965	122293.3545	108848.5475	107889.8768	130918.7019	108060.5007	108234.2704	103659.1075	68035.8674	73758.2109	85668.5045	87139.6506	74561.8540	84019.4044	87214.6619	79646.1996	73973.8637	71104.4901	88733.2317
glutathione (oxidized)	1747.8298	1176.8459	974.1710	1159.3395	1433.6646	940.6940	2002.4258	2225.8304	1482.9273	1861.0955	2422.3863	2435.4984	1835.4482	2293.8998	1903.2502	2184.6666	2360.6789	4693.0840	2188.0564	2209.1666	1023.0326	1056.2023	1196.6457	2226.4938	1689.2795	809.8203	780.7336	1555.2170	1228.6753	1127.1771	1880.0765	2554.7047	995.7174	1091.3077	2957.7253	2206.9609	1456.2428	2564.5177	1604.2561	2416.3985
glycerophosphocholine	118671.8967	141590.9318	119478.2493	107049.8938	112402.7643	137837.0626	113956.5350	106731.7095	100801.5690	102464.1646	145738.4256	117138.0583	148461.6708	122128.6148	94466.8918	152196.9504	118269.4332	137692.8780	131166.9643	123733.7402	130295.5356	118844.8234	118112.5826	189009.1288	170553.0540	157326.3926	137772.4848	138704.6842	105885.1509	149441.9185	207190.0528	210166.5821	138940.8500	186083.6117	191086.0685	146366.8955	190814.6923	206941.1526	181866.8839	199648.2203
guanine	24311.7651	22564.9058	21423.4379	19438.5032	20142.5708	23571.0164	16805.2754	20244.6876	18018.5289	18864.6334	13221.8645	9659.8917	13444.0112	12530.5886	11544.9449	15307.5156	16513.4398	13905.5226	8980.4981	8232.4066	14908.5432	17878.4790	13997.1309	14405.6396	18010.8926	15895.7771	17878.0959	20974.7090	17749.3429	13585.6740	2238.4168	2617.7444	2095.2399	2830.7659	2762.1576	2383.0531	3252.0850	1556.8546	2350.2180	2217.9148
hydroxycaprylic acid	139883.1563	140939.3289	219643.2193	123870.5145	96984.2109	108464.6011	99215.5787	134289.9271	109653.2450	116193.4669	78555.1576	94324.6208	144594.6579	79418.9279	145740.9224	121161.9926	139326.0144	109253.6109	53711.6700	109054.2774	135011.4937	185452.6311	144001.7855	164481.5838	141458.3447	189599.7070	171465.2909	193045.6999	218344.7736	143201.5561	35720.6479	59544.7741	52846.1152	52005.8797	12730.2944	53280.8560	76846.1632	10146.4527	73565.0573	22323.8673
hydroxyprolyl-valine	1231.1713	1390.2658	1008.9326	1014.0690	1083.3706	1054.5118	997.3653	1306.2881	1286.0145	1477.9162	1080.1996	1011.7267	960.7532	1151.0533	996.2462	1003.8542	995.9289	1149.6964	943.2058	1016.9511	1271.8906	1102.6714	1292.4186	1080.7511	1002.5002	816.5025	942.4271	918.7656	1288.4279	880.5454	296.9200	265.3705	309.8082	364.0986	553.6072	436.1083	581.2133	313.9024	351.7412	323.7820
hypoxanthine	27527.9793	22701.6356	38061.8694	15821.3361	18211.4762	18457.9046	12838.4376	15847.3290	18967.0653	15169.5050	27041.0698	14884.0132	30368.3116	25364.2665	24918.3126	26758.2681	30777.7854	23829.2515	14114.3819	14699.4662	14703.5859	15081.0503	20220.3743	11070.6189	12568.1382	12558.6281	13934.5911	15550.6994	12587.6631	11492.6175	5184.8845	6619.0434	6516.8552	5956.1549	7804.9788	5428.5774	6846.9166	3611.3698	5244.0837	6142.1876
indole	42.3713	40.7650	49.7824	45.6868	39.5132	40.0985	47.0507	34.3062	44.0858	34.6225	53.0193	36.5874	53.9822	34.9135	27.3525	32.9640	32.8446	49.7189	39.4803	34.9131	46.9710	54.1662	54.2352	67.6133	69.7543	74.9051	39.9423	51.1580	42.9622	42.4389	1097.2504	637.5854	537.0027	611.6360	1218.6463	500.3815	423.6623	917.6138	604.3093	1281.1840
isophorone	9487.5753	7997.5456	12229.0090	8438.0373	9297.6975	10796.4936	7441.1457	14001.9179	7000.3037	7104.3093	11616.5088	12347.4087	9492.5457	11752.3436	12606.5349	13150.0233	20004.5225	10937.3547	10062.2202	13384.3953	9526.7578	7994.9671	9456.6339	7817.5807	10952.0051	10281.0658	11468.7062	9320.1902	10195.1884	7924.9287	1200.7792	1893.8301	1759.5643	1919.8830	900.3204	1956.1252	2929.5220	1018.2930	2632.3419	1073.9887
isoscoparin 2^^-(6-(E)-ferulylglucoside)	7626.4299	4959.5287	6898.7572	4796.3232	7800.6990	4086.7555	6936.0763	6377.8792	6911.6400	6182.2489	8537.5714	8608.5652	7717.0527	8690.3698	8203.9213	9754.8298	9486.5208	11040.8429	7819.4437	7972.7458	4253.6520	4819.6940	5457.1736	6033.0906	5338.4787	2151.5046	5516.7294	6409.6095	6262.6762	6145.8183	4728.1626	6523.3734	5849.4676	5629.4698	5626.2369	6643.2706	7426.0035	4938.5631	7363.8888	3884.2099
kynurenine	700.1607	547.6983	1187.8713	980.8271	669.1224	782.7472	1042.3896	937.5218	762.5124	635.3216	1760.4419	1104.2157	1463.4657	888.7115	757.6905	1383.9064	998.0619	1089.2559	1013.2718	961.8073	953.7794	936.5749	1181.9551	1886.7061	1741.6839	2829.1019	1870.6163	1403.7733	788.1221	1512.5714	9429.4157	12499.6050	10126.2234	12757.2545	6744.7126	8555.7690	7164.8775	3921.9572	8610.7179	12610.5018
L-2-amino-5-hydroxypentanoic acid	336.3103	264.7935	355.2360	154.8409	272.2069	224.5578	162.8326	350.7392	363.1884	273.3019	519.5032	178.8836	497.2314	128.7133	290.3635	186.1406	333.9768	409.7629	318.2022	273.5974	183.9315	115.7538	162.1902	139.4471	153.3328	106.0146	168.4479	145.1957	123.2411	132.7834	1037.6724	539.2510	1495.6928	605.3031	1605.1335	865.2491	2358.2590	1273.8224	615.2132	1017.5032
L-arginine monohydrochloride	19093.5195	17093.4448	16859.7477	18133.7245	17864.0490	17498.7188	18483.1679	18496.5352	17136.8964	16141.1458	18971.1738	18252.8064	18039.8020	17694.1345	18145.9401	16781.1422	19397.8474	19424.7292	17452.8440	20958.5634	15888.1450	16826.3946	16692.5564	22328.9257	18695.4620	20131.7737	15476.2490	20144.9215	18459.5044	17631.9283	20947.0950	17776.9252	14809.4072	18354.1884	23233.3408	14980.1829	18899.3865	24511.9492	18932.9691	21267.8968
lysine	4949.3686	7462.2114	6025.0317	5238.7741	6060.3646	6314.1391	6583.4966	5491.9533	6095.2801	5238.4699	5800.0345	3898.0953	4244.5384	2365.2436	7680.8972	4812.5043	4696.7220	5952.6582	5219.7582	8793.4441	6014.5407	5115.8707	8582.6733	8078.2897	6060.5540	9062.3762	5411.4486	6332.4573	6932.3855	4273.0536	5309.2591	4853.7229	3026.1481	2193.5305	7897.2867	2234.0682	2566.7588	7475.2170	2723.0873	5565.6061
maltose	72490.6405	44827.7211	64282.3259	40905.2576	40209.9265	47116.0937	49878.2382	42827.4511	45656.2630	46305.4698	54618.2740	52658.4327	51464.3171	104870.9697	54791.4922	48743.7121	52106.2338	54080.7401	44163.8170	72597.0810	92599.9753	55493.7257	43356.3443	47187.3242	53129.5851	23199.2376	64293.8605	51121.4264	44274.1504	85128.0518	33253.7416	29033.6802	34648.9770	40653.2244	39564.3304	30832.9570	60989.6721	35176.2606	43496.8553	21329.9321
mannitol	6159.7175	1787.8901	3743.6951	1400.3082	1837.1607	2873.1180	1845.2602	3644.3354	2865.4320	3775.9673	2755.9073	2748.9197	2437.9678	3014.0869	1918.3973	1925.6452	2105.4595	2412.5404	2909.1198	3214.3078	5677.0466	4096.8773	5397.8920	3518.4562	4474.2682	1648.3917	2736.9022	4188.1768	3742.6647	3569.1167	1993.1664	647.4776	1685.7457	2332.3317	1747.1641	1668.4422	2462.3563	1094.5080	1859.6390	891.9919
methionine	7876.9759	8746.1068	10090.2994	8149.4044	8283.1920	7517.6219	6957.5559	9175.8801	12005.3694	8109.0142	8161.2695	6689.4097	8460.5872	6086.1776	6391.6728	7109.3836	5611.6361	6950.3592	5532.7044	5327.9240	7021.7232	7319.0294	7315.3830	7556.3438	8324.4521	11840.3491	6571.0704	7695.9918	5835.6936	4406.8401	11547.9309	9041.1167	10819.3992	15133.7224	12281.3674	9740.4350	12137.9245	7902.2534	9282.4073	11489.0495
methionine-methyl-d3	27434.2667	31489.7656	27288.2506	30223.8979	26493.5221	26192.7883	24820.7199	26685.9022	28638.5679	29100.1174	25472.6467	24836.3636	25720.9214	25801.6330	25276.8818	26026.0348	25969.6198	26394.9530	24385.1946	26137.3330	26426.4675	24891.4544	26496.9753	27345.6466	25514.8466	26832.5033	27677.5023	24406.5294	26722.1681	25822.7267	23656.3914	24447.1159	25587.5675	24441.3027	24988.4786	26967.0323	26370.9251	25543.3868	25399.8507	21599.4787
methylguanosine	2755.7685	2320.7864	2871.7843	2471.8531	2247.2428	1914.6370	1421.4002	2198.7067	1779.9876	1644.5129	1492.2605	1503.0789	1601.2595	1324.5638	1518.1891	1978.4962	2094.2182	1545.4434	1113.4280	1153.1623	1568.3593	1728.4766	1651.2884	2044.5347	1968.3418	1845.1480	1986.9139	2749.3865	1976.1041	2049.8173	1849.8543	2035.6980	1859.3066	2183.3428	1837.5918	1964.3666	2170.1101	2159.9290	2599.9890	1939.8498
methylindole	74.2058	77.5019	99.2643	88.0749	82.8899	87.8263	98.9705	81.2520	91.2499	82.9779	113.7147	88.8695	87.9771	85.9371	69.8364	86.8093	62.4221	78.8840	90.1242	84.0536	94.9532	85.9634	117.9568	105.1511	117.8465	164.4298	91.2958	110.6085	95.7140	100.6007	2041.5489	1186.7926	1225.0014	1133.7440	2469.4327	1031.9914	778.8044	1666.1341	1123.4363	2494.5926
methyl-L-histidine	989.0259	1014.5883	848.6306	838.6972	769.9049	730.5315	1026.1787	934.5309	997.5420	1054.5035	844.7876	618.7285	589.0607	462.1561	451.7203	595.4231	611.2911	724.2253	522.6072	674.4182	694.7826	519.5039	634.6736	830.0219	660.7394	647.3256	705.8989	782.1103	551.2287	624.6945	7441.4859	4967.2692	5187.6889	6448.9569	7849.9282	5937.4722	3546.3469	6944.5601	3771.0639	7170.7327
methyl oleate	7239.0045	4051.3054	3493.8165	5042.1291	3038.0006	4430.4348	4321.5057	2306.4320	2456.6620	2673.3956	3547.7256	3196.4974	4237.2361	4236.4840	3090.5295	3094.7391	2775.9861	3152.9423	3522.3122	2813.1830	3989.6619	4120.1979	3156.7168	4077.9864	4111.6905	3620.1192	2465.5102	3840.6218	2794.4853	4185.4938	4064.7144	4579.3969	2349.0908	3381.1401	2716.3690	2707.6152	4143.0505	4462.5285	3807.2138	4342.7690
methylpiperidine-2-carboxylic acid	1863.7759	1393.5990	1134.8769	678.1218	1048.8514	1320.3560	1348.2495	1361.5786	1300.0910	1061.8465	3068.6575	3649.7726	8033.7386	3078.3799	2425.5102	6807.1169	8231.9883	7222.9808	4360.3671	2719.8798	2088.7244	842.4752	856.1473	3354.3077	1583.2475	1262.7551	1319.9497	3651.1793	1294.0704	1152.6224	448.7648	1047.2547	1128.1108	538.5465	263.1186	389.4136	902.1782	355.0392	435.1763	210.3487
methyltyrosinate	5539.2239	3990.0525	8419.1892	19064.7216	3900.6718	7800.8902	10018.9276	3989.8366	4063.9619	3330.9399	16890.8181	10114.9002	23931.2006	34911.1028	10831.7159	18589.5632	10465.0508	12374.3854	21763.0214	16948.7701	5665.3050	5720.4104	3837.5806	5737.9739	10794.1695	2595.9580	9074.5056	9652.2892	16792.9304	8026.2071	31827.0464	33091.5208	33132.7514	33020.2870	33227.1461	33910.1699	32047.6117	31947.4376	35504.9859	30350.5107
N2-methylguanosine	4538.2010	4394.6866	3788.4467	3277.1322	4185.3040	3911.5554	3373.5992	4674.1702	3203.6821	3477.1491	4090.3296	3601.4128	3316.2928	3621.2783	3451.6031	3393.5148	3666.5727	3165.9393	3601.6825	2836.0647	2959.5804	3666.2908	3021.5954	3736.4027	3992.8384	3522.6434	4304.8878	4988.0439	3325.2444	3354.9207	3265.8926	3408.8231	4518.7002	4526.2044	3354.3753	3762.8722	4339.6097	2507.0650	3778.2470	2244.7849
N6-methyl-lysine	66.2629	88.6560	63.4403	57.7606	62.9512	82.7611	81.3279	75.1395	56.4742	54.5159	55.5266	53.8818	76.3344	21.4035	28.1015	43.2645	48.8587	42.7868	65.7777	62.7942	61.2338	34.9583	49.7411	54.6675	46.7222	49.9220	58.0417	53.8000	45.0694	67.0546	432.3733	506.1715	240.6332	294.8627	500.9065	300.8794	239.6668	428.2418	338.3365	514.3711
N6_N6-dimethyllysine	520.9099	673.3293	571.2146	411.8985	496.4628	634.9114	655.4257	536.3064	243.1375	475.5169	352.9041	293.7682	338.7235	223.5862	162.8670	316.4842	288.1916	407.3954	258.1556	360.3639	408.7414	260.4289	491.3559	559.2307	434.4656	461.2312	655.3246	380.6265	353.8530	581.5782	2928.1591	2079.2105	1029.0788	1529.1008	3565.1956	1286.1120	1019.3988	3387.4545	1451.0799	2254.7712
N-acetyl-5-hydroxytryptamine	124.9881	171.3015	140.7995	171.8891	138.3693	180.8075	211.2983	107.7645	144.4717	112.6255	213.0162	212.6787	252.6839	255.2863	306.0038	272.9549	314.7787	457.7960	209.7356	276.8522	152.9547	165.0085	194.1542	141.2125	159.7382	140.2446	143.9327	161.0530	187.0590	196.3199	124.5060	151.3151	169.8702	129.3800	81.9806	175.1729	151.6656	179.9111	199.5162	163.9263
N-acetyl-D-mannosamine	554.5359	522.0810	573.5806	414.9301	480.8434	489.1695	405.4341	411.4566	457.8019	477.5361	495.3204	372.8889	347.5220	480.7515	433.5725	465.8448	375.3702	337.5450	420.3214	442.1302	518.4207	453.5759	551.5146	446.5226	590.4706	368.2297	452.5542	474.7118	363.2224	635.8895	587.5608	470.1526	433.8784	463.5762	563.8055	492.8566	530.7639	682.3722	535.5952	624.9354
N-acetyl-glutamic acid	4525.4235	3873.4345	5493.5047	4980.7129	4663.4473	5440.0321	5283.4406	4654.9857	4964.4264	4779.4434	7341.7652	6684.0015	8112.4593	7141.1744	5805.6001	7335.9143	5716.2455	5930.9571	4943.3676	5589.6878	5248.1650	6743.0074	6730.9210	8362.3608	7727.0610	8129.5975	7408.3310	7058.9463	6608.4828	6453.7878	5370.2628	4665.3868	2636.6913	3672.4160	4497.2049	4374.6749	5319.9617	6019.6318	5151.8899	5554.5360
N-fructosyl isoleucine	5477.0374	5710.2642	5795.8678	5399.1501	3265.8136	5003.5406	5607.5738	4758.2243	5805.2059	2792.5114	8271.9764	3168.6811	3476.1876	4490.5184	553.7394	3465.7874	3628.2304	3108.6902	2895.7801	3831.1764	7515.6734	9877.6152	7797.8720	6324.5971	5548.6690	5619.0209	3703.0034	4450.7187	5037.6947	5221.2332	5689.7672	3214.0115	1664.5496	4321.4834	2645.9820	3144.9308	4437.7778	2114.4362	3548.3643	1508.4333
N-fructosyl phenylalanine	924.9320	1183.3088	1060.2101	970.9023	659.9854	1286.1911	1252.5927	1075.1178	1017.7333	505.8607	1626.9563	653.7124	748.6843	970.7286	147.2464	709.3323	661.3433	850.7939	657.3591	1152.7982	2025.9877	1698.6117	1872.5703	1835.4370	1386.9103	1248.8006	1083.3672	924.5098	1154.8693	1312.6317	3880.1363	2827.4108	948.5062	2270.6039	2229.6268	2240.6496	2424.0229	1818.4094	3444.1559	1298.3659
N-fructosyl tyrosine	517.2744	543.1638	574.4830	627.0442	390.1427	547.3467	714.8514	541.5076	607.1916	337.8400	697.4575	315.4275	265.8685	344.8495	129.8644	407.1954	374.1360	349.2485	302.4716	395.3579	653.8738	850.9832	745.7223	699.6084	677.3848	666.8933	423.0372	565.3455	567.2785	581.3126	2906.4458	1860.1052	671.1446	1396.1593	1244.8009	1659.8597	1252.8283	1315.9202	1755.0209	1196.9986
nicotinamide	547.0712	879.0429	600.3080	451.5183	866.1372	674.4902	700.9733	748.3711	374.9630	401.4301	639.7004	534.5830	571.4322	625.7948	582.0082	593.1963	518.6476	542.3756	732.6443	734.1983	827.4729	248.6724	491.4273	487.9537	400.4150	574.9971	844.7167	355.8322	240.6556	346.8528	1006.0348	1365.9009	885.7767	1288.5412	552.3322	745.4742	1305.6327	482.1797	832.7265	811.9813
N-methyl-L-glutamic acid	3678.5285	416.4036	3365.6290	475.8351	2603.7275	2332.0528	457.4746	525.8640	3184.8436	681.7073	1858.0862	1699.1493	1890.2416	576.4536	2567.9103	1714.6603	1960.0774	2161.3630	1774.6049	662.6013	2896.8146	299.6178	2573.9804	1599.2633	2181.8136	355.4794	366.6267	2530.6898	335.3051	1738.1947	517.9249	410.8939	520.6224	414.9246	539.5458	411.6365	804.8237	448.2842	455.0504	582.1002
N_N-dimethylguanosine	6740.7457	7196.2523	7695.9674	5128.3622	5552.9641	4044.5107	3853.0339	6146.8278	4542.0739	3726.7146	3103.3785	2668.4907	3343.7438	2648.5087	3063.0734	4399.6447	3602.0460	2892.9253	2202.3808	2154.3411	3543.2456	4644.3816	4191.3205	4573.3873	5333.6707	4229.7792	4998.3488	7396.9537	4697.5944	6282.4316	3756.6817	4276.5682	3857.9297	4334.9035	3284.8282	3473.6189	4418.5849	3841.8031	4847.6848	3596.3754
N_N_N-trimethyllysine	1281.8406	1374.7636	1244.4446	1162.2283	1142.9827	1473.0125	1415.8344	1406.4467	1048.7806	1123.4629	1075.9963	825.8357	1082.8185	595.4927	607.2182	1181.1123	1139.5523	1218.6800	1088.8382	1230.8461	1174.6753	830.9407	1062.2147	1415.2051	1199.4510	1157.9341	1471.6246	1206.2211	1171.0588	1351.7549	7474.6554	7541.2509	3763.9588	5613.7087	7393.7283	5059.0466	4178.7541	7555.3141	5778.2466	8271.9964
N-omega-acetylhistamine	4714.3788	10653.5750	5605.2686	5058.6628	2931.4557	8561.2819	6609.4586	3825.5736	4746.5989	5994.6325	957.5209	678.5956	1411.7703	1451.6849	1979.3706	1028.2757	1678.6635	871.3184	2189.1971	1531.1302	2723.6043	3586.5410	3892.7147	5211.8886	3721.1592	4314.9909	8904.4948	3056.1488	5848.1959	6678.0486	449.0440	487.3975	395.2345	395.4554	702.8252	492.4756	490.9563	511.0007	518.0987	598.0764
norvaline	3295.3125	3519.6420	4016.5014	2483.0368	3711.1672	2288.3887	2905.3617	4272.0562	5699.1078	3635.2848	6716.1309	6244.9170	5725.3665	5264.2338	6501.5966	7897.4527	7033.7875	5118.5603	6075.6741	8340.5840	4570.9145	3869.7919	6605.1265	6525.3664	6727.9864	6078.8631	6120.4126	5857.3218	5523.1227	3890.4247	7520.8166	8317.9343	11251.3614	7882.4830	9429.4321	6388.2940	8895.6660	8347.2817	7692.0564	7891.0094
octanoylcarnitine	1069.4093	1509.4810	1201.3955	5247.6958	1250.1519	1570.4328	2508.3958	2491.4269	1308.8472	374.1964	1033.7538	2817.1681	848.9819	3192.4546	3147.4256	3386.5695	3516.9373	3372.8760	1794.7914	1873.9360	772.6869	1352.2297	422.8095	751.2060	608.6101	1089.7169	1439.0923	1583.2058	1425.8475	578.1164	177.7399	202.9789	203.0034	216.9514	67.9357	121.9165	383.1766	75.4193	224.9938	58.3115
octenoic acid	36369.0380	28152.8023	62888.4527	31470.2945	28978.1229	31391.6067	19224.3099	43301.8031	33086.6602	31732.7293	22558.7160	28032.1407	36056.6622	21892.3480	36921.9648	33359.0549	41858.9663	32189.5014	15128.7715	33518.5465	28238.5200	46746.0585	36539.8845	39558.4312	36352.3542	50584.7635	49848.1425	52026.1211	61350.9775	37255.6845	9565.8840	15807.4791	16474.6904	14267.0146	3883.9924	15470.6198	19415.9059	2821.8841	19640.1599	6215.6110
octopamine	2353.7801	3317.4474	2369.6951	3187.7112	2428.0177	2806.3058	2877.4712	2661.5852	3808.2893	2284.1859	3968.5418	1769.9954	1724.7096	1989.8840	1329.8414	2299.8398	1803.0245	2426.9218	1991.3087	2426.9843	2317.0034	2470.5890	3001.1538	4496.8120	4335.4420	5496.3222	2881.5233	2922.7143	2187.6902	2221.1005	33523.2915	33271.2296	13587.9340	14487.4544	62555.5505	22767.0745	17009.2110	54402.8620	25547.0795	36309.1496
phenacylamine	34.6775	26.6743	85.8489	61.0569	47.5320	53.7190	63.6925	60.0834	51.5960	43.3108	115.6929	72.4527	101.1711	61.7332	44.4025	100.3438	71.7301	78.7478	74.7162	50.8328	78.7230	56.9360	89.8644	146.6094	116.1744	242.5289	127.0822	104.5824	47.7819	117.4975	856.4720	1137.7547	943.4105	1191.3073	615.6615	759.4346	613.2363	282.1999	776.8571	1194.8590
phenylacetic acid	50.5091	61.8265	266.2894	82.3172	55.8394	71.7699	71.7286	61.7377	57.7292	42.4749	747.4118	647.8529	1027.6954	1099.7666	629.2452	1453.1167	1343.9866	668.2603	947.7135	1421.7676	47.1455	60.9301	50.6447	56.5716	62.3743	43.4239	66.0806	81.6591	46.8834	81.1254	170.6289	244.4438	311.9307	265.4161	123.1766	281.6799	380.1854	111.0270	333.2298	288.4644
phenylglycine	97.8950	98.6292	161.9467	297.9185	103.8756	171.8519	171.1689	115.0438	83.1397	65.3170	396.1679	218.8172	545.3261	838.7709	192.2821	419.7451	206.8638	366.6016	471.2303	338.8340	110.4768	115.9480	90.8613	108.2446	220.4232	69.6514	189.5067	150.3705	207.9615	125.4132	332.6160	349.2901	530.6174	447.6070	264.1228	393.9206	496.7907	249.7549	512.4154	317.9802
phosphorylcholine	118941.3402	108271.4150	102528.0731	125342.9169	101327.4010	124321.6097	135473.1777	106182.2627	115352.3987	114446.7344	104501.0991	92505.1254	94538.3545	98014.1114	104004.3886	96059.0635	98101.3359	86823.5069	105378.5994	110240.0683	111972.9916	132978.3243	120211.0111	127930.6723	118745.6171	146812.5070	113693.1863	136853.4161	110178.4430	131728.4425	83361.3845	104370.2708	65463.2059	79902.4850	64665.2226	68134.8641	82895.1019	75199.7580	88002.2742	78564.1782
planteose	8409.7574	7149.4754	9487.5672	6462.8907	7340.8293	6991.3744	8488.0456	6257.7879	7052.8291	7145.8960	9658.6848	9866.2162	9676.6459	19278.9438	10301.1127	10053.0631	9505.6680	10481.7612	8417.5542	12775.0892	13384.5225	10532.0071	6939.5508	8421.8197	10131.1303	3028.9695	12295.9710	9694.9614	6887.3452	13671.1744	5619.0772	5175.7425	5975.3010	6859.6530	7665.2249	5494.9417	10860.6805	6805.2418	7773.2806	3362.2998
p-menthen-1_2-diol	12916.0573	12256.6826	11616.0596	12990.4916	10860.7933	9443.2962	10297.2677	18563.8797	13090.6435	11297.9681	13466.5724	11006.5774	13748.1469	8670.2082	11898.3131	10488.3665	12781.5428	13479.4485	6542.0212	10748.7593	12723.4281	15508.8749	14708.8460	22248.0784	19138.2113	27521.8085	26094.3257	29412.5881	26250.8808	25921.5661	11276.4852	12367.6570	10673.7269	14497.2965	7277.5337	7652.8386	13975.1981	11884.8484	15363.9108	10282.7087
proline	155361.7474	156262.1897	134600.0551	113888.2381	139314.9111	117587.9787	122638.9244	161465.0155	173067.6833	167155.4474	123549.4779	128609.5953	112522.9689	130947.7737	132613.8308	132433.8906	134292.5508	137898.1550	121001.3017	134302.7093	152415.0713	132275.7795	157550.4772	138505.9505	127094.0110	109412.8635	136196.2253	123220.2392	148943.3537	117067.0719	48827.9250	44254.1778	64213.1197	60897.8461	78892.1109	74115.5356	82063.4439	57175.8095	60183.5208	50266.6124
proline_ 1-acetyl-4-hydroxy-_ cis-	51.9480	49.8604	52.3515	60.5575	78.4839	43.5190	68.2064	66.4017	68.9836	48.0010	49.8306	26.2921	34.0884	25.4119	14.0349	51.7378	33.0680	46.1969	26.8398	20.7555	82.6415	50.8293	55.9204	51.4489	47.7461	42.3876	71.2375	48.3483	63.3077	65.3489	489.1317	331.3782	236.1046	245.3696	57.5927	129.0431	328.0899	115.5363	264.6183	98.1554
PS(18:0/18:2)	274.9309	804.1392	719.6750	557.3562	943.7756	677.5174	957.9839	688.1677	1070.2609	856.7593	970.9388	797.4346	1214.1581	1025.0801	881.7209	1082.6278	1120.3653	1153.4341	836.5093	971.2419	582.5252	509.5064	578.9011	870.5298	432.6852	729.8662	497.5030	587.5503	539.9864	950.1534	2718.3969	2278.7409	801.8517	1446.3040	2096.5039	2795.0452	2555.1555	1577.2309	1901.0429	4652.3855
pyroglutamic acid	3846.8998	4612.8473	3187.0249	4333.7413	3922.3821	3647.6217	4295.4932	5454.2816	4595.7142	5212.4380	3221.8050	3493.4113	2909.0469	2912.3754	2980.8138	3452.8162	3620.7336	3285.9002	2687.7860	3351.9974	4364.4008	3737.1772	3657.9166	3976.5176	4394.1022	5222.9188	4691.3054	3409.7247	3812.0357	3190.6936	3760.2873	2960.5016	4167.1447	2771.1810	3650.5763	3377.8310	3926.6555	3778.6848	3825.4339	3997.8125
saccharopine	843.9999	801.3436	559.0600	533.5711	733.9170	1111.2839	734.9139	976.4073	665.9377	968.6063	956.6821	649.3770	755.7264	787.8888	793.0543	678.5605	479.6823	784.0564	705.1135	927.3970	421.7250	372.2919	884.6654	899.1556	658.2887	503.0923	754.1759	737.4188	442.1441	520.1014	507.8331	513.8916	302.8990	475.9727	561.4710	388.8347	583.6602	406.7958	596.8285	693.4919
S-adenosyl-methionine	783.9709	629.6284	723.7450	659.4483	580.0536	739.5419	710.3355	723.7121	716.9242	642.5573	734.3633	623.0151	604.4460	611.8286	705.6864	669.0551	682.6147	660.8517	694.0514	702.6887	757.6360	651.4715	697.4655	709.7044	819.9047	885.3837	664.0088	809.6900	633.4256	748.9540	1175.0149	954.4631	734.8981	978.6057	1108.0178	902.0130	917.5379	1119.1287	828.9466	1306.6772
serotonin	175.3300	193.2657	242.7773	209.8074	177.9144	208.3470	216.6763	237.6094	240.4369	190.8786	253.4589	218.5246	239.0007	227.4170	176.8866	217.1899	186.2307	228.2642	208.2312	211.2150	245.7580	277.5825	258.5230	330.6692	317.4408	374.9553	235.5091	250.2294	199.9783	229.5682	4365.1720	2711.3749	2539.9922	2460.4824	5081.7774	2133.9559	1719.4047	3693.7568	2373.6004	5140.3017
sorbose	79033.1499	37351.4367	61451.2018	35344.7282	23433.6389	43633.7477	39341.0881	43826.6414	43701.8556	43945.5079	41381.1615	41745.4105	31518.9228	86926.5972	44197.5857	25900.6052	34040.5819	34526.3021	31878.3809	61965.9418	86886.2491	34046.9713	39656.0310	32427.7401	38258.7544	20293.1289	43376.5629	34798.6403	36564.3582	77411.3161	28343.3261	16858.1438	28085.4810	33956.6755	29988.2814	21089.8000	50109.9044	22113.1773	33177.0808	14892.1379
spermidine	7.1177	40.0680	17.5908	7.6509	28.3378	14.2977	32.1621	33.4293	32.7170	22.1610	24.3690	26.9400	35.4406	23.9890	35.1068	59.8094	44.1032	44.7782	27.3598	49.0189	13.4826	5.7544	16.2399	18.3983	8.7221	13.2065	26.8076	13.9297	11.8900	20.9766	54.2503	58.4955	10.2032	31.0596	196.2573	37.9478	39.4654	139.4017	31.2846	296.4872
tert-leucine	162.9498	297.7316	184.0674	209.3878	100.3079	235.2204	204.1207	161.2773	127.9771	151.9382	138.1935	88.0936	111.0625	116.3208	112.3721	132.4036	132.7041	138.3670	140.1947	124.1286	160.0543	123.1984	117.3787	164.4043	151.6595	125.1050	171.7156	96.4934	121.2858	158.0078	103.2038	74.6651	85.0057	98.6293	109.6772	74.5551	79.1079	115.5912	89.8123	113.3578
threonine	7588.9159	8005.8787	7649.3902	5428.8261	7073.4861	7160.9662	5113.5481	6864.0811	7577.3313	6268.0287	6989.5308	5690.3475	6457.8510	8044.7230	6518.0299	6811.3294	6501.9902	6980.3729	7655.1939	8280.7708	7627.2788	7175.9138	7429.0793	7425.7738	6245.9143	7618.3197	6679.9654	6173.1116	5781.2400	5311.1927	3139.2008	1618.9476	2357.5729	5052.9502	4262.5108	3220.8750	5775.7716	3547.2805	2318.3333	3507.4375
thymine	505.5220	548.4466	760.3416	194.3259	314.3354	136.1838	177.1651	268.2192	415.0298	197.0030	473.8193	195.3031	435.9926	129.9561	259.4076	569.2490	582.4414	516.5734	171.1246	146.9857	213.6153	282.9574	439.5667	149.0848	288.5563	219.8677	406.5662	371.0167	386.9588	383.8715	50.7906	15.5499	49.1559	31.2200	141.7331	35.4393	41.8479	97.5734	35.3248	65.2238
thymol	70545.8096	63501.4653	84688.0099	92629.5307	78244.5504	55553.2823	74415.0614	87144.0648	120101.4462	80913.1432	60943.3406	70801.7698	63251.8663	62830.5786	68079.3050	75251.3583	79257.8890	60689.6834	43135.4303	65784.2909	69546.8090	75825.5707	62822.6661	80140.4028	78272.3588	80585.1080	91992.6851	96024.5392	102456.0651	72264.5977	55720.6357	51674.7888	70086.9717	70375.0921	35745.3899	60726.9583	64172.4143	34407.5322	66611.7865	41793.1046
trans-4-hydroxy-L-proline	231.2293	227.9255	319.1728	210.2936	251.6786	190.9447	248.2322	287.0093	340.3475	239.6738	394.3833	192.9813	213.5279	277.9309	270.1783	341.6766	223.9379	327.8018	259.4675	230.6221	248.0441	226.0681	261.6200	347.3198	305.2945	338.2879	344.1619	269.0439	212.4098	336.8008	1252.0562	1061.8219	1196.0404	1123.2064	384.2571	738.4460	1592.7582	434.5678	1292.4403	447.7363
tryptophan	5346.8065	5612.7576	7057.7698	6312.5805	5471.2036	6027.1817	6846.0328	6902.9758	6668.1420	5671.1842	7588.7582	5776.2425	6479.9820	5879.2288	4758.2748	6377.7749	5044.1947	5899.0612	5842.2422	5781.2845	7086.4203	7469.4226	7992.7777	8981.7528	8785.8824	11037.5454	6751.0432	7381.6026	6116.1169	6993.1251	107573.3894	68387.5633	69955.3640	64616.1248	130883.0801	60543.6075	46079.4727	91206.7559	62483.0408	130430.6423
xanthommatin	24002.8851	24636.9374	26913.0681	10750.7061	19910.6088	17359.7676	13053.9941	18508.7656	21905.6741	17336.5680	17960.5011	13938.5611	17274.9085	12571.8244	7278.6685	10823.6324	11023.6341	11650.6373	11634.8624	6303.9750	15991.4620	13755.1066	17278.8204	12284.7158	8939.5224	13983.2037	15521.6088	15821.1846	18586.4306	16776.5963	4703.4455	10482.2834	6060.0853	12505.8488	12018.9483	16487.7038	16764.7608	12427.1676	13533.7452	13388.5280
MS_METABOLITE_DATA_END
#METABOLITES
METABOLITES_START
metabolite_name	pubchem_id	inchi_key	kegg_id	other_id	other_id_type	ri	ri_type	moverz_quant	
10-hydroxy-2-decenoic Acid									
20-COOH-leukotriene E4									
2,6-nonadien-1-ol									
2-amino-1-phenylethanol									
3,4-dihydroxydecanoylcarnitine									
3-hydroxy-DL-kynurenine									
4-hydroxy-3-methoxyphenylethanol									
5'-deoxy-5'-(methylthio)adenosine									
9(R)-hydroxydec-2(E)-enoic acid									
acetylhistamine									
acetyl-L-carnitine									
acetylputrescine									
adenosine									
alpinetin methyl ether									
beta-nicotinamide adenine dinucleotide									
caffeine 13C3									
carbamoylpyrrolidine-2-carboxylic acid									
carnitine									
cinnamaldehyde									
cuminyl alcohol									
delta-octanolactone									
dopamine									
dopamine quinone									
D-phenylalanine-d5									
E-3-(4-hydroxy-3-methoxyphenyl)-prop-2-en-1-ol									
E-9-oxodec-2-enoic acid									
estragole									
ethylcarboxamidoadenosine									
ferulic acid-d3									
fructoselysine									
galactosamine									
gamma-aminobutyric acid									
gamma-glutamylglutamine									
gamma-glutamylphenylalanine									
gamma-glutamyltyrosine									
glutamic acid									
glutamine									
glutathione (oxidized)									
glycerophosphocholine									
guanine									
hydroxycaprylic acid									
hydroxyprolyl-valine									
hypoxanthine									
indole									
isophorone									
isoscoparin 2''-(6-(E)-ferulylglucoside)									
kynurenine									
L-2-amino-5-hydroxypentanoic acid									
L-arginine monohydrochloride									
lysine									
maltose									
mannitol									
methionine									
methionine-methyl-d3									
methylguanosine									
methylindole									
methyl-L-histidine									
methyl oleate									
methylpiperidine-2-carboxylic acid									
methyltyrosinate									
N2-methylguanosine									
N6-methyl-lysine									
N6,N6-dimethyllysine									
N-acetyl-5-hydroxytryptamine									
N-acetyl-D-mannosamine									
N-acetyl-glutamic acid									
N-fructosyl isoleucine									
N-fructosyl phenylalanine									
N-fructosyl tyrosine									
nicotinamide									
N-methyl-L-glutamic acid									
N,N-dimethylguanosine									
N,N,N-trimethyllysine									
N-omega-acetylhistamine									
norvaline									
octanoylcarnitine									
octenoic acid									
octopamine									
phenacylamine									
phenylacetic acid									
phenylglycine									
phosphorylcholine									
planteose									
p-menthen-1,2-diol									
proline									
proline, 1-acetyl-4-hydroxy-, cis-									
PS(18:0/18:2)									
pyroglutamic acid									
saccharopine									
S-adenosyl-methionine									
serotonin									
sorbose									
spermidine									
tert-leucine									
threonine									
thymine									
thymol									
trans-4-hydroxy-L-proline									
tryptophan									
xanthommatin									
METABOLITES_END
#END