                      INSTRUMENT CONTROL PARAMETERS:    GCTQ
                      --------------------------------------

   D:\MassHunter\GCMS\All Acquisition method\AA_MTBSTFA_SIM_DB-5_30m_20230330.M
      Fri Mar 31 23:21:21 2023

Control Information
------- -----------

Sample Inlet             : GC
Injection Source         : PAL Sampler
Injection Location:  Front
Mass Spectrometer        : Enabled


PAL3 Sampler
Serial Number:                             Robot
Script Name:                               GC-LIQ-STD-V4.0
Installed Syringe
Name:                                      8010-0163
Maximum Volume (µL):                       10.00
Minimum Volume (µL):                       1.00

Script Parameters
Basic
Wash Station:                              Wash Station
Tool:                                      LS 2
Sample Volume (uL):                        2
Wait for System Ready:                     At start
Wash Vial Depth (mm):                      40
Waste Port Depth (mm):                     10
Bottom Sense:                              Off
Height From Bottom of Sample Vial (mm):    32
Cooled Stack:                              None
Cooled Stack Temperature (°C):             25
GC Cycle Time (min):                       9

Pre Injection
Syringe Fill For Wash (%):                 95
Wash Aspirate Flow Rate (uL/s):            5
Washes with Solvent 1:                     0
Washes with Solvent 2:                     1
Washes with Solvent 3:                     0
Washes with Solvent 4:                     0

Sample
Sample Vial Penetration Depth (mm):        30
Sample Vial Penetration Speed (mm/s):      50
Sample Washes:                             1
Sample Wash Volume (uL):                   1
Filling Strokes:                           4
Fill Strokes Volume (uL):                  3
Filling Strokes Aspirate Flow Rate (uL/s): 5
Delay After Filling Strokes (s):           0.5
Sample Aspirate Flow Rate (uL/s):          1
Sample Post Aspirate Delay (s):            2
Air Volume (uL):                           1
Injection Mode:                            Normal
Injection Signal Mode:                     Plunger Up
Inlet Penetration Depth (mm):              45
Inlet Penetration Speed (mm/s):            100
Pre Inject Time Delay (s):                 0
Injection Flow Rate (uL/s):                100
Post Inject Time Delay (s):                0

Post Injection
Syringe Fill For Wash (%):                 95
Wash Aspirate Flow (uL/s):                 5
Washes with Solvent 1:                     3
Washes with Solvent 2:                     5
Washes with Solvent 3:                     0
Washes with Solvent 4:                     0





 No Sample Prep method has been assigned to this method.


GC
GC Summary
Run Time                                     24.233 min
Post Run Time                                0 min

Oven
Equilibration Time                           0 min
Max Temperature                              325 °C
Maximum Temperature Override                 Enabled
Slow Fan                                     Disabled
Temperature
Setpoint                                     On
(Initial)                                    130 °C
Hold Time                                    0 min
Post Run                                     0 °C
Program
#1 Rate                                      6 °C/min
#1 Value                                     190 °C
#1 Hold Time                                 0 min
#2 Rate                                      30 °C/min
#2 Value                                     230 °C
#2 Hold Time                                 5 min
#3 Rate                                      50 °C/min
#3 Value                                     325 °C
#3 Hold Time                                 6 min



Collision Cell/Backflush
He Quench Gas                                On    2.25 mL/min
N2 Collision Gas                             On    1.5 mL/min
Pressure
Setpoint                                     Off
(Initial)                                    8 psi
Post Run                                     0 psi


Front MM Inlet He
Mode                                         Pulsed Split
Pressure                                     On    17.662 psi
Total Flow                                   On    11.4 mL/min
Septum Purge Flow                            On    3 mL/min
Gas Saver                                    On    15 After 3 min mL/min
Split Ratio                                  5 :1
Split Flow                                   7 mL/min
Injection Pulse Pressure                     35 psi Until 1 min
Cryo                                         Off
Cryo Type                                    N2
Liner                                        Agilent 5190-4048: 35 μL (Straight Ultra Inert Liner for SPME)
Temperature
Setpoint                                     On
(Initial)                                    280 °C


Thermal Aux 2 (MSD Transfer Line)
Temperature
Setpoint                                     On
(Initial)                                    325 °C
Post Run                                     0 °C


Column
Column Outlet Pressure                       0 psi
Column #1
Column Information                           Agilent 122-5532UI
DB-5ms Ultra Inert                           
Temperature Range                            -60 °C—325 °C (350 °C)
Dimensions                                   30 m x 250 μm x 0.25 μm
Column lock                                  Unlocked
In                                           Front MM Inlet He
Out                                          MSD 
(Initial)                                    130 °C
Pressure                                     17.662 psi
Flow                                         1.4 mL/min
Average Velocity                             43.963 cm/sec
Holdup Time                                  1.1373 min
Flow
Setpoint                                     Off
(Initial)                                    1.4 mL/min
Post Run                                     1 mL/min



Aux EPC 4,5,6
Aux EPC 4 N2
                                             ***Excluded from Affecting GC's Readiness State***
Pressure
Setpoint                                     Off
(Initial)                                    4 psi
Post Run                                     0 psi


Aux EPC 5 N2
                                             ***Excluded from Affecting GC's Readiness State***
Pressure
Setpoint                                     Off
(Initial)                                    10 psi
Post Run                                     0 psi


Aux EPC 6 N2
                                             ***Excluded from Affecting GC's Readiness State***
Pressure
Setpoint                                     Off
(Initial)                                    10 psi
Post Run                                     0 psi



Signals
Signal #1:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz

Signal #2:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz

Signal #3:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz

Signal #4:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz






                      END OF INSTRUMENT CONTROL PARAMETERS
                      ------------------------------------
