Return to study ST000892 main page
MB Sample ID: SA052558
Local Sample ID: | EXPL9 |
Subject ID: | SU000929 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Species Group: | Human |
Select appropriate tab below to view additional metadata details:
Subject:
Subject ID: | SU000929 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Species Group: | Human |
Factors:
Local Sample ID | MB Sample ID | Factor Level ID | Level Value | Factor Name |
---|---|---|---|---|
EXPL9 | SA052558 | FL009981 | Extracted plasma | Sample type |
Collection:
Collection ID: | CO000923 |
Collection Summary: | Not available |
Sample Type: | Blood |
Treatment:
Treatment ID: | TR000943 |
Treatment Summary: | Not available |
Sample Preparation:
Sampleprep ID: | SP000936 |
Sampleprep Summary: | Mixing 540 μL of urine with 60 μL D2O potassium buffer + DSS |
Extract Storage: | -80 C |
Analysis:
MB Sample ID: | SA052558 |
Analysis ID: | AN001454 |
Analysis Type: | NMR |
Acquisition Date: | between 8/21/16 and 8/23/16 | between 8/21/16 and 8/23/17 | between 8/21/16 and 8/23/18 | between 8/21/16 and 8/23/19 | between 8/21/16 and 8/23/20 | between 8/21/16 and 8/23/21 | between 8/21/16 and 8/23/22 | between 8/21/16 and 8/23/23 |
Acquisition Parameters File: | plasma-paper-160821/CPMG-1 plasma-paper-160822/CPMG-1 and plasma-paper-160823/CPMG-1 plasma-paper-160821/CPMG-2 plasma-paper-160822/CPMG-2 and plasma-paper-160823/CPMG-2 plasma-paper-160821/CPMG-3 plasma-paper-160822/CPMG-3 and plasma-paper-160823/CPMG-3 plasma-paper-160821/PROJECT-1 plasma-paper-160822/PROJECT-1 and plasma-paper-160826/PROJECT-1 plasma-paper-160821/NOESYPR1D plasma-paper-160822/NOESYPR1D and plasma-paper-160828/NOESYPR1D plasma-paper-160821/PURGE plasma-paper-160822/PURGE and plasma-paper-160828/PURGE plasma-paper-160821/CPMG-4 plasma-paper-160822/CPMG-4 and plasma-paper-160823/CPMG-4 plasma-paper-160821/PROJECT-2 plasma-paper-160822/PROJECT-2 and plasma-paper-160826/PROJECT-2 |
Num Factors: | 2 |
Num Metabolites: | 71 |
Units: | µM |
NMR:
NMR ID: | NM000110 |
Analysis ID: | AN001454 |
Instrument Name: | FT NMR |
Instrument Type: | FT-NMR |
NMR Experiment Type: | 1D 1H |
NMR Comments: | For intact plasma | For intact plasma | For intact plasma | For intact plasma | For extracted plasma | For extracted plasma | For extracted plasma | For extracted plasma |
Field Frequency Lock: | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz |
Spectrometer Frequency: | 600 MHz |
NMR Solvent: | H2O+D2O (90/10) phosphate buffer | H2O+D2O (90/10) phosphate buffer | H2O+D2O (90/10) phosphate buffer | H2O+D2O (90/10) phosphate buffer | D2O phosphate buffer | D2O phosphate buffer | D2O phosphate buffer | D2O phosphate buffer |
NMR Tube Size: | 5 mm |
Shimming Method: | Topshim | Topshim | Topshim | Topshim | Topshim | Topshim | Topshim | Topshim Pulse Sequence | cpmgpr1d | cpmgpr1d | cpmgpr1d | PROJECTpr1d-1 | noesypr1d | zgpurge-gprefocus-2 | cpmgpr1d | PROJECTpr1d-1 |
Water Suppression: | Presaturation |
Pulse Width: | 19.94 μs | 19.94 μs | 19.94 μs | 19.94 μs | 11.82 μs | 11.82 μs | 11.82 μs | 11.82 μs |
Power Level: | 5.5584 W | 5.5584 W | 5.5584 W | 5.5584 W | 5.5584 W | 5.5584 W | 5.5584 W | 5.5584 W |
Receiver Gain: | 90.5 | 90.5 | 90.5 | 90.5 | 90.5 | 90.5 | 90.5 | 90.5 |
Offset Frequency: | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz |
Presaturation Power Level: | 4.13E-05 | 4.13E-05 | 4.13E-05 | 4.13E-05 | 4.13E-05 | 4.13E-05 | 4.13E-05 | 4.13E-05 |
Chemical Shift Ref Cpd: | DSS | DSS | DSS | DSS | DSS | DSS | DSS | DSS |
Temperature: | 310 K | 311 K | 312 K | 313 K | 314 K | 315 K | 316 K | 317 K |
Number Of Scans: | 32 | 32 | 32 | 32 | 32 | 32 | 32 | 32 |
Dummy Scans: | 4 | 4 | 4 | 4 | 4 | 4 | 4 | 4 |
Acquisition Time: | 3.067 | 3.067 | 3.067 | 3.067 | 3.067 | 3.067 | 3.067 | 3.067 |
Relaxation Delay: | 4 s | 4 s | 4 s | 4 s | 5 s | 6 s | 7 s | 8 s |
Spectral Width: | 20.03 ppm | 20.03 ppm | 20.03 ppm | 20.03 ppm | 20.03 ppm | 20.03 ppm | 20.03 ppm | 20.03 ppm |
Num Data Points Acquired: | 73728 | 73728 | 73728 | 73728 | 73728 | 73728 | 73728 | 73728 |
Real Data Points: | 36864 | 36864 | 36864 | 36864 | 36864 | 36864 | 36864 | 36864 |
Line Broadening: | 0.3 Hz | 0.3 Hz | 0.3 Hz | 0.3 Hz | 0.3 Hz | 0.3 Hz | 0.3 Hz | 0.3 Hz |
Zero Filling: | 65536 | 65536 | 65536 | 65536 | 65536 | 65536 | 65536 | 65536 |
Apodization: | Gaussian | Gaussian | Gaussian | Gaussian | Gaussian | Gaussian | Gaussian | Gaussian |
Baseline Correction Method: | Polynomial order 2 | Polynomial order 2 | Polynomial order 2 | Polynomial order 2 | Polynomial order 2 | Polynomial order 2 | Polynomial order 2 | Polynomial order 2 |
Chemical Shift Ref Std: | DSS | DSS | DSS | DSS | DSS | DSS | DSS | DSS |