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MB Sample ID: SA022860
Local Sample ID: | mctrl_039 |
Subject ID: | SU000471 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Age Or Age Range: | Males with CFS were 53 (±2.8) y old (mean±SEM; range, 21–67 y). Females were 52 (±2.5) y old (range, 20–67 y). |
Gender: | 23 females and 22 males with CFS and 18 male and 21 female controls. |
Human Ethnicity: | White/non-Hispanic |
Species Group: | Human |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN000705 | AN000706 |
---|---|---|
Analysis type | MS | MS |
Chromatography type | HILIC | HILIC |
Chromatography system | Shimadzu 20AD | Shimadzu 20AD |
Column | Shodex NH2P-40 2E (250× 2.0 mm) | Shodex NH2P-40 2E (250× 2.0 mm) |
MS Type | ESI | ESI |
MS instrument type | Triple quadrupole | Triple quadrupole |
MS instrument name | ABI Sciex 5500 QTrap | ABI Sciex 5500 QTrap |
Ion Mode | POSITIVE | NEGATIVE |
Units | AUC | AUC |
Chromatography:
Chromatography ID: | CH000510 |
Chromatography Summary: | HILIC |
Instrument Name: | Shimadzu 20AD |
Column Name: | Shodex NH2P-40 2E (250× 2.0 mm) |
Column Pressure: | 920~2600 psi |
Column Temperature: | 25C |
Flow Gradient: | 0-3.5 min: 95%B, 3.6-8 min: 85% B, 8.1-13 min: 75% B, 13.5–35 min: 0% B, 36–46 min: 95% B, 46.1 min: end. |
Flow Rate: | 0.2 ml/min |
Solvent A: | 95% water/5% acetonitrile; 20 mM ammonium carbonate; 38 mM ammonium hydroxide, pH 9.75 |
Solvent B: | 100% acetonitrile |
Analytical Time: | 46.1 min |
Oven Temperature: | 25C |
Sample Loop Size: | 10 ul |
Sample Syringe Size: | 100 ul |
Chromatography Type: | HILIC |