Return to study ST000873 main page
MB Sample ID: SA053399
| Local Sample ID: | S3 |
| Subject ID: | SU000947 |
| Subject Type: | Sheep |
| Subject Species: | Ovis aries |
| Taxonomy ID: | 9940 |
| Gender: | Both |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN001478 | AN001479 |
|---|---|---|
| Analysis type | MS | MS |
| Chromatography type | Reversed phase | Reversed phase |
| Chromatography system | Waters Acquity | Waters Acquity |
| Column | Aquity C18 BEH (100 x 2.1mm,1.7um) | Aquity C18 BEH (100 x 2.1mm,1.7um) |
| MS Type | ESI | ESI |
| MS instrument type | Triple quadrupole | Triple quadrupole |
| MS instrument name | ABI Sciex 6500 QTrap | ABI Sciex 6500 QTrap |
| Ion Mode | NEGATIVE | POSITIVE |
| Units | Concentration (nM) | Concentration (nM) |
Chromatography:
| Chromatography ID: | CH001037 |
| Instrument Name: | Waters Acquity |
| Column Name: | Aquity C18 BEH (100 x 2.1mm,1.7um) |
| Column Temperature: | 60 °C |
| Flow Gradient: | See protocol/methods file |
| Flow Rate: | 0.25 mL/min |
| Internal Standard: | See protocol/methods file |
| Retention Time: | See protocol/methods file |
| Sample Injection: | 5 µL |
| Solvent A: | 100% water; 0.1% acetic acid |
| Solvent B: | 90% acetonitrile/ 10% isopropanol |
| Analytical Time: | 20 min |
| Weak Wash Solvent Name: | 20% methanol, 10% isopropanol |
| Weak Wash Volume: | 600 µL |
| Strong Wash Solvent Name: | 50:50 Acetonitrile:Methanol |
| Strong Wash Volume: | 600 µL |
| Chromatography Type: | Reversed phase |
