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MB Sample ID: SA099057
| Local Sample ID: | 1800-M-UD BPA |
| Subject ID: | SU001436 |
| Subject Type: | Mammal |
| Subject Species: | Peromyscus Californicus |
| Taxonomy ID: | 42520 |
| Age Or Age Range: | PND90 |
| Gender: | Male and female |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN002266 | AN002267 | AN002268 |
|---|---|---|---|
| Analysis type | MS | MS | MS |
| Chromatography type | Reversed phase | GC | GC |
| Chromatography system | Waters Acquity I-Class | Agilent 6890N | Agilent 6890N |
| Column | Waters Acquity BEH C18 (150 x 2mm,1.7um) | DB-5MS (J&W Scientific) 60m | DB-5MS (J&W Scientific) 60m |
| MS Type | ESI | EI | EI |
| MS instrument type | QTOF | Single quadrupole | Single quadrupole |
| MS instrument name | Bruker maXis Impact qTOF | Agilent 5973 | Agilent 5973 |
| Ion Mode | POSITIVE | POSITIVE | POSITIVE |
| Units | intensity | intensity | intensity |
Chromatography:
| Chromatography ID: | CH001665 |
| Instrument Name: | Waters Acquity I-Class |
| Column Name: | Waters Acquity BEH C18 (150 x 2mm,1.7um) |
| Column Pressure: | >11000 psi |
| Column Temperature: | 60 |
| Flow Gradient: | Solvent B (acetonitrile) was increased from 5% to 70% over 30 min, then to 95% over 3 min, held at 95% for 3 min, then returned to 5% for equilibrium |
| Flow Rate: | 0.560 ml/min |
| Internal Standard: | Umbelliferon |
| Retention Time: | 1 to 35 min |
| Solvent A: | 100% water; 0.1% formic acid |
| Solvent B: | 100% acetonitrile |
| Analytical Time: | 40 min |
| Chromatography Type: | Reversed phase |
| Chromatography ID: | CH001666 |
| Chromatography Summary: | 5:1 split for GCMS-polar injection with 1uL injection volume. |
| Instrument Name: | Agilent 6890N |
| Column Name: | DB-5MS (J&W Scientific) 60m |
| Column Pressure: | variable |
| Column Temperature: | variable between 80-315 |
| Flow Rate: | 1mL/Min of Helium gas |
| Internal Standard: | Ribitol |
| Retention Time: | 9 to 61 min |
| Sample Injection: | 5:1 split injection with 1uL injection volume |
| Analytical Time: | 61 min |
| Chromatography Type: | GC |
| Chromatography ID: | CH001667 |
| Chromatography Summary: | 1:1 split for GCMS-nonpolar injection with 1uL injection volume. |
| Instrument Name: | Agilent 6890N |
| Column Name: | DB-5MS (J&W Scientific) 60m |
| Column Pressure: | variable |
| Column Temperature: | variable between 80-315 |
| Flow Rate: | 1mL/Min of Helium gas |
| Internal Standard: | Docosanol |
| Retention Time: | 9 to 61 min |
| Sample Injection: | 1:1 split injection with 1uL injection volume |
| Analytical Time: | 61 min |
| Chromatography Type: | GC |
