Return to study ST001826 main page
MB Sample ID: SA169361
| Local Sample ID: | ODBS5 |
| Subject ID: | SU001903 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Age Or Age Range: | 53 ± 15 |
| Weight Or Weight Range: | 116 ± 25 |
| Gender: | Male and female |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN002962 |
|---|---|
| Analysis type | MS |
| Chromatography type | Normal phase |
| Chromatography system | Q Exactive GC orbitrap |
| Column | Agilent Technologies (30 m x 0.25mm, 0.25um) |
| MS Type | EI |
| MS instrument type | Triple quadrupole |
| MS instrument name | Thermo Q Exactive Orbitrap |
| Ion Mode | POSITIVE |
| Units | Area |
Chromatography:
| Chromatography ID: | CH002195 |
| Chromatography Summary: | GC-HRAM analysis were performed in a Q Exative GC Orbitrap system (Thermo Scientific), mounted with a Rxi Guard column purchased at Restek (10 m X 0.37 mm, 0.25 µm i.d.) and a capillary column provided by Agilent Technologies (30 m, 0.25 mm, 0.25 µm i.d.). Injection (1µ) was done in splitless mode with a TriPlus RSH autosampler system provided by Thermo. Oven temperature was keep at 70 °C for the first 5 minutes. Then, temperature was increased to 260 °C (10 °C/min) to reach in the final step 300 °C (40 °C/min) for 5 min. The carrier gas used was Helium with a flow of 2.0 ml/min. Scan range and resolution were adjusted to 50 – 500 m/z and 60,000 respectively. MS Detector was operated in EI positive mode. |
| Instrument Name: | Q Exactive GC orbitrap |
| Column Name: | Agilent Technologies (30 m x 0.25mm, 0.25um) |
| Chromatography Type: | Normal phase |
