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MB Sample ID: SA186023
Local Sample ID: | CatS_Cons_4 |
Subject ID: | SU002071 |
Subject Type: | Insect |
Subject Species: | Duponchelia fovealis |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN003242 | AN003243 | AN003244 | AN003245 | AN003246 | AN003247 |
---|---|---|---|---|---|---|
Analysis type | MS | MS | MS | MS | MS | MS |
Chromatography type | GC | GC | Reversed phase | Reversed phase | Reversed phase | Reversed phase |
Chromatography system | Agilent 7890A | Agilent 7890A | Waters Acquity UPLC | Waters Acquity UPLC | Waters Acquity UPLC | Waters Acquity UPLC |
Column | Agilent DB-5 (20m x 0.18mm, 0.18um); Restek RX-T 17 (0.9m x 0.10mm, 0.10um) | Agilent DB-5 (20m x 0.18mm, 0.18um); Restek RX-T 17 (0.9m x 0.10mm, 0.10um) | Waters Acquity UPLC HSS (100 x 2.1mm, 1.7um) | Waters Acquity UPLC HSS (100 x 2.1mm, 1.7um) | Waters Acquity UPLC HSS (100 x 2.1mm, 1.7um) | Waters Acquity UPLC HSS (100 x 2.1mm, 1.7um) |
MS Type | EI | API | ESI | ESI | ESI | ESI |
MS instrument type | GC x GC-TOF | GC x GC-TOF | QTOF | QTOF | QTOF | QTOF |
MS instrument name | Leco Pegasus 4D GCxGC TOF | Leco Pegasus 4D GCxGC TOF | Waters Acquity UPLC | Waters Acquity UPLC | Waters Acquity UPLC | Waters Acquity UPLC |
Ion Mode | UNSPECIFIED | UNSPECIFIED | NEGATIVE | POSITIVE | NEGATIVE | POSITIVE |
Units | peak area | Relative intensity | Relative intensity | Relative intensity | Relative intensity |
Chromatography:
Chromatography ID: | CH002391 |
Methods Filename: | Metabolomics_Methods |
Instrument Name: | Agilent 7890A |
Column Name: | Agilent DB-5 (20m x 0.18mm, 0.18um); Restek RX-T 17 (0.9m x 0.10mm, 0.10um) |
Column Temperature: | 70 - 320 ºC |
Flow Rate: | 1 mL.min-1 |
Injection Temperature: | 280 ºC |
Sample Injection: | 1 uL |
Oven Temperature: | 70°C for 2 min, increasing by 15°C·min-1 until it reached 320°C and then held at this temperature for 4 min. |
Chromatography Type: | GC |
Chromatography ID: | CH002392 |
Methods Filename: | Metabolomics_Methods |
Instrument Name: | Waters Acquity UPLC |
Column Name: | Waters Acquity UPLC HSS (100 x 2.1mm, 1.7um) |
Column Temperature: | 35 ºC |
Flow Gradient: | 95% solvent A and 5% B. The gradient increased linearly to 75% A and 25% B over the next 6 min. The polarity was reversed to 25% A and 75% B for 6 min, and finally 5% A and 95% B for 1 min |
Flow Rate: | 0.5 mL·min-1 |
Solvent A: | Water; formic acid |
Solvent B: | 100% acetonitrile; formic acid. |
Capillary Voltage: | 3 kV |
Chromatography Type: | Reversed phase |