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MB Sample ID: SA214468
| Local Sample ID: | Control_Positive_P-14 |
| Subject ID: | SU002330 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN003663 | AN003664 |
|---|---|---|
| Analysis type | MS | MS |
| Chromatography type | HILIC | HILIC |
| Chromatography system | Thermo Dionex Ultimate 3000 | Thermo Dionex Ultimate 3000 |
| Column | Ascentis Express HILIC HPLC (150 x 2.1mm,2.7um) | Ascentis Express HILIC HPLC (150 x 2.1mm,2.7um) |
| MS Type | ESI | ESI |
| MS instrument type | Orbitrap | Orbitrap |
| MS instrument name | Thermo Q Exactive HF hybrid Orbitrap | Thermo Q Exactive HF hybrid Orbitrap |
| Ion Mode | POSITIVE | NEGATIVE |
| Units | intensity | intensity |
Chromatography:
| Chromatography ID: | CH002714 |
| Instrument Name: | Thermo Dionex Ultimate 3000 |
| Column Name: | Ascentis Express HILIC HPLC (150 x 2.1mm,2.7um) |
| Column Temperature: | 35 |
| Flow Gradient: | 10% B for 2 min, and ramped to 30% B in 8 min, and ramped to 100 % B in 5 min, and maintained at 100 % B for 3 min, and back to initial 10 % B in 1 min, and equilibrate at initial condition for 7 min. |
| Flow Rate: | 0.25 ml/min |
| Injection Temperature: | 4 |
| Solvent A: | 95% acetonitrile/5% water; 0.1% acetic acid; 10 mM ammonium acetate |
| Solvent B: | 95% water/5% acetonitrile; 0.1% acetic acid; 10 mM ammonium acetate |
| Analytical Time: | 26min |
| Chromatography Type: | HILIC |
