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MB Sample ID: SA214604
Local Sample ID: | Patient_Negative_P-33 |
Subject ID: | SU002330 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN003663 | AN003664 |
---|---|---|
Analysis type | MS | MS |
Chromatography type | HILIC | HILIC |
Chromatography system | Thermo Dionex Ultimate 3000 | Thermo Dionex Ultimate 3000 |
Column | Ascentis Express HILIC HPLC (150 x 2.1mm,2.7um) | Ascentis Express HILIC HPLC (150 x 2.1mm,2.7um) |
MS Type | ESI | ESI |
MS instrument type | Orbitrap | Orbitrap |
MS instrument name | Thermo Q Exactive HF hybrid Orbitrap | Thermo Q Exactive HF hybrid Orbitrap |
Ion Mode | POSITIVE | NEGATIVE |
Units | intensity | intensity |
Chromatography:
Chromatography ID: | CH002714 |
Instrument Name: | Thermo Dionex Ultimate 3000 |
Column Name: | Ascentis Express HILIC HPLC (150 x 2.1mm,2.7um) |
Column Temperature: | 35 |
Flow Gradient: | 10% B for 2 min, and ramped to 30% B in 8 min, and ramped to 100 % B in 5 min, and maintained at 100 % B for 3 min, and back to initial 10 % B in 1 min, and equilibrate at initial condition for 7 min. |
Flow Rate: | 0.25 ml/min |
Injection Temperature: | 4 |
Solvent A: | 95% acetonitrile/5% water; 0.1% acetic acid; 10 mM ammonium acetate |
Solvent B: | 95% water/5% acetonitrile; 0.1% acetic acid; 10 mM ammonium acetate |
Analytical Time: | 26min |
Chromatography Type: | HILIC |