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MB Sample ID: SA250586
Local Sample ID: | pos-TBI-22 |
Subject ID: | SU002597 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Gender: | Male and female |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN004107 | AN004108 | AN004109 |
---|---|---|---|
Analysis type | MS | MS | MS |
Chromatography type | GC | Reversed phase | Reversed phase |
Chromatography system | Agilent 7890A | Thermo TSQ Vantage HPLC-MS/MS | Thermo TSQ Vantage HPLC-MS/MS |
Column | Agilent DB-5ms (30m x 0.25mm, 0.25um) | Waters ACQUITY UPLC BEH C8 (100 x 2.1mm,1.7um) | Waters ACQUITY UPLC HSS T3 (100 x 2.1mm,1.8um) |
MS Type | EI | ESI | ESI |
MS instrument type | Single quadrupole | Triple quadrupole | Triple quadrupole |
MS instrument name | Agilent 5977 | Thermo TSQ Vantage | Thermo TSQ Vantage |
Ion Mode | UNSPECIFIED | POSITIVE | NEGATIVE |
Units | pmoles/l | pmoles/l | pmoles/l |
Chromatography:
Chromatography ID: | CH003042 |
Instrument Name: | Agilent 7890A |
Column Name: | Agilent DB-5ms (30m x 0.25mm, 0.25um) |
Column Temperature: | 280 |
Flow Gradient: | The oven temperature was initially set to 70°C, held for 3min, and then increased to 310°C at a rate of 5°C/min, and finally kept for 10min. |
Flow Rate: | 1.2 mL/min |
Solvent A: | N/A |
Solvent B: | N/A |
Chromatography Type: | GC |
Chromatography ID: | CH003043 |
Chromatography Summary: | positive ion mode |
Instrument Name: | Thermo TSQ Vantage HPLC-MS/MS |
Column Name: | Waters ACQUITY UPLC BEH C8 (100 x 2.1mm,1.7um) |
Column Temperature: | 50 |
Flow Gradient: | 0~1 min, 0.1~10% B; 1-5 min, 10-40% B; 5-17 min, 40-100% B; 17-22min, 100% B; 22-22.1 min, 100-10% B |
Flow Rate: | 0.25 mL/min |
Solvent A: | water(0.1% formic acid ) |
Solvent B: | acetonitrile(0.1% formic acid ) |
Chromatography Type: | Reversed phase |
Chromatography ID: | CH003044 |
Chromatography Summary: | negative ion mode |
Instrument Name: | Thermo TSQ Vantage HPLC-MS/MS |
Column Name: | Waters ACQUITY UPLC HSS T3 (100 x 2.1mm,1.8um) |
Column Temperature: | 50 |
Flow Gradient: | 0-1min,0.1%B;1-3min,0.1-40%B;3-5min,40-100%B;5-10.5min,100%B;10.5-10.6min,0.1%B;10.6-18min |
Flow Rate: | 0.25 mL/min |
Solvent A: | water(5 mM ammonium bicarbonate ) |
Solvent B: | 95% methanol/water(5mM ammonium bicarbonate ) |
Chromatography Type: | Reversed phase |