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MB Sample ID: SA252859
| Local Sample ID: | Control day 5.3 |
| Subject ID: | SU002611 |
| Subject Type: | Bacteria |
| Subject Species: | Aspergillus niger/Bacillus subtilis |
| Taxonomy ID: | 5061/1423 |
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Combined analysis:
| Analysis ID | AN004135 |
|---|---|
| Analysis type | MS |
| Chromatography type | GC |
| Chromatography system | Agilent 7890B |
| Column | Restek Rtx-5Sil MS (30m x 0.25mm, 0.25um) |
| MS Type | EI |
| MS instrument type | QTOF |
| MS instrument name | Agilent 7200 QTOF |
| Ion Mode | POSITIVE |
| Units | m/z |
Chromatography:
| Chromatography ID: | CH003063 |
| Chromatography Summary: | The volatiles were desorbed from the traps using an desorption unit (Unity TD-100, Markes International Ltd., Llantrisant, UK) at 210 °C for 12 min (He flow 50 mL/min) and trapped on a cold trap at -10 °C. The volatiles were introduced into the GC-Q-TOF (model Agilent 7890B GC and the Agilent 7200A QTOF, Santa Clara, USA) by heating the cold trap for 12 min to 250 °C. The used split ratio was 1:10 and the used column was a 30 × 0.25 mm ID RXI-5MS, film thickness 0.25 µm (Restek 13424-6850, Bellefonte, PA, USA). Temperature program was as follows: 39 °C for 2 min, from 39 °C to 95 °C at 3.5 °C/min, then to 165 °C at 4 °C/min, to 280 °C at 15 °C/min and finally to 320 °C at 30 °C/min, hold 7 min. The volatile organic compounds were ionized in EI mode at eV and mass spectra were acquired in full-scan-mode (30–400 U @ 5 scans/s). Mass-spectra were extracted with MassHunter Qualitative Analysis Software V B.06.00 Build 6.0.633.0 (Agilent Technologies, Santa Clara, USA). |
| Instrument Name: | Agilent 7890B |
| Column Name: | Restek Rtx-5Sil MS (30m x 0.25mm, 0.25um) |
| Column Temperature: | 280°C |
| Flow Gradient: | - |
| Flow Rate: | 50 mL/min |
| Solvent A: | - |
| Solvent B: | - |
| Chromatography Type: | GC |
