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MB Sample ID: SA254154
Local Sample ID: | CC5 |
Subject ID: | SU002621 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
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Combined analysis:
Analysis ID | AN004153 | AN004154 |
---|---|---|
Analysis type | MS | MS |
Chromatography type | Reversed phase | Reversed phase |
Chromatography system | Thermo Vanquish | Thermo Vanquish |
Column | Thermo Accucore C30 (150 x 2.1mm,2.6um) | Thermo Accucore C30 (150 x 2.1mm,2.6um) |
MS Type | ESI | ESI |
MS instrument type | Orbitrap | Orbitrap |
MS instrument name | Thermo Orbitrap ID-X tribrid | Thermo Orbitrap ID-X tribrid |
Ion Mode | NEGATIVE | POSITIVE |
Units | chromatographic peak area | chromatographic peak area |
Chromatography:
Chromatography ID: | CH003073 |
Instrument Name: | Thermo Vanquish |
Column Name: | Thermo Accucore C30 (150 x 2.1mm,2.6um) |
Column Temperature: | 50 |
Flow Gradient: | 0-1 min 80-40% A; 1-5 min 40-30% A; 5-5.5 min 30-15% A; 5.5-8 min 15-10% A; 8-8.2 min 10-0% A; 8.2-10.5 0% A; 10.5-10.7 min 0-80% A; 10.7-12.0 min 80% A. |
Flow Rate: | 0.4 ml min-1 |
Solvent A: | 10 mM ammonium acetate with water/acetonitrile (40:60 v/v) |
Solvent B: | 10 mM ammonium acetate with 2-isopropanol/acetonitrile (90:10 v/v). 0.1% formic acid |
Chromatography Type: | Reversed phase |
Chromatography ID: | CH003074 |
Instrument Name: | Thermo Vanquish |
Column Name: | Thermo Accucore C30 (150 x 2.1mm,2.6um) |
Column Temperature: | 50 |
Flow Gradient: | 0-1 min 80-40% A; 1-5 min 40-30% A; 5-5.5 min 30-15% A; 5.5-8 min 15-10% A; 8-8.2 min 10-0% A; 8.2-10.5 0% A; 10.5-10.7 min 0-80% A; 10.7-12.0 min 80% A. |
Flow Rate: | 0.4 ml min-1 |
Solvent A: | 10 mM ammonium formate with water/acetonitrile (40:60 v/v) and 0.1% formic acid |
Solvent B: | 10 mM ammonium formate with 2-isopropanol/acetonitrile (90:10 v/v) and 0.1% formic acid |
Chromatography Type: | Reversed phase |