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MB Sample ID: SA257282
Local Sample ID: | C5_Hilic_pos |
Subject ID: | SU002659 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Age Or Age Range: | 82 |
Gender: | Female |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN004214 | AN004215 | AN004216 | AN004217 |
---|---|---|---|---|
Analysis type | MS | MS | MS | MS |
Chromatography type | HILIC | HILIC | Reversed phase | Reversed phase |
Chromatography system | Thermo Dionex Ultimate 3000 | Thermo Dionex Ultimate 3000 | Thermo Dionex Ultimate 3000 | Thermo Dionex Ultimate 3000 |
Column | Agilent InfinityLab Poroshell 120 HILIC-Z (150 x 2.1mm,2.7um) | Agilent InfinityLab Poroshell 120 HILIC-Z (150 x 2.1mm,2.7um) | Thermo Accucore C18 (150 x 2.1mm,2.6um) | Thermo Accucore C18 (150 x 2.1mm,2.6um) |
MS Type | ESI | ESI | ESI | ESI |
MS instrument type | QTOF | QTOF | QTOF | QTOF |
MS instrument name | ABI Sciex 6600 TripleTOF | ABI Sciex 6600 TripleTOF | ABI Sciex 6600 TripleTOF | ABI Sciex 6600 TripleTOF |
Ion Mode | POSITIVE | NEGATIVE | POSITIVE | NEGATIVE |
Units | area integration | area integration | area integration | area integration |
Chromatography:
Chromatography ID: | CH003124 |
Chromatography Summary: | Hilic ESI+ |
Instrument Name: | Thermo Dionex Ultimate 3000 |
Column Name: | Agilent InfinityLab Poroshell 120 HILIC-Z (150 x 2.1mm,2.7um) |
Column Temperature: | 50 °C |
Flow Gradient: | 0 min 98% B 3 min 98% B 23 min 5% B 24 min 5% B 24 min 98% B |
Flow Rate: | 0.25 ml/min |
Sample Injection: | 5 μL |
Solvent A: | 10 mM ammonium formate and 0.1 % formic acid in water |
Solvent B: | 9:1 acetonitrile / 10 mM ammonium formate and 0.1 % formic acid in water |
Chromatography Type: | HILIC |
Chromatography ID: | CH003125 |
Chromatography Summary: | Hilic ESI- |
Instrument Name: | Thermo Dionex Ultimate 3000 |
Column Name: | Agilent InfinityLab Poroshell 120 HILIC-Z (150 x 2.1mm,2.7um) |
Column Temperature: | 50 °C |
Flow Gradient: | 0 min 96% B 2 min 96% B 22 min 65% B 24 min 65% B 24 min 96% B |
Flow Rate: | 0.25 ml/min |
Sample Injection: | 5 μL |
Solvent A: | 10 mM ammonium acetate, pH 9 with ammonium hydroxide and 10 µM medronic acid |
Solvent B: | 85:15 acetonitrile / 10 mM ammonium acetate, pH 9 with ammonium hydroxide and 10 µM medronic acid in water |
Chromatography Type: | HILIC |
Chromatography ID: | CH003126 |
Chromatography Summary: | RP ESI+ |
Instrument Name: | Thermo Dionex Ultimate 3000 |
Column Name: | Thermo Accucore C18 (150 x 2.1mm,2.6um) |
Column Temperature: | 40 °C |
Flow Gradient: | 0 min 5% B 1 min 5% B 8 min 100% B 10 min 100% B 10 min 5% B |
Flow Rate: | 0.3 ml/min |
Sample Injection: | 5 μL |
Solvent A: | 0.1 % formic acid in water |
Solvent B: | 0.1 % formic acid in 98:2 acetonitrile / water |
Chromatography Type: | Reversed phase |
Chromatography ID: | CH003127 |
Chromatography Summary: | RP ESI- |
Instrument Name: | Thermo Dionex Ultimate 3000 |
Column Name: | Thermo Accucore C18 (150 x 2.1mm,2.6um) |
Column Temperature: | 40 °C |
Flow Gradient: | 0 min 5% B 1 min 5% B 8 min 100% B 10 min 100% B 10 min 5% B |
Flow Rate: | 0.3 ml/min |
Sample Injection: | 5 μL |
Solvent A: | 0.1 % formic acid in water |
Solvent B: | 0.1 % formic acid in 98:2 acetonitrile / water |
Chromatography Type: | Reversed phase |