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MB Sample ID: SA258094
Local Sample ID: | 2021-11-29_045_E3_E3 |
Subject ID: | SU002668 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Gender: | Male |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN004228 |
---|---|
Analysis type | MS |
Chromatography type | Reversed phase |
Chromatography system | Agilent 6530 qTOF |
Column | Agilent Zorbax Extend C18 (150 x 2.1mm, 1.8um) with matched guard column |
MS Type | ESI |
MS instrument type | QTOF |
MS instrument name | Agilent 6530 QTOF |
Ion Mode | NEGATIVE |
Units | EicCoreArea/Peak Area |
Chromatography:
Chromatography ID: | CH003137 |
Methods Filename: | experiment_metadata |
Instrument Name: | Agilent 6530 qTOF |
Column Name: | Agilent Zorbax Extend C18 (150 x 2.1mm, 1.8um) with matched guard column |
Column Temperature: | 35°C |
Flow Gradient: | 0-2min hold 100/0/0 (%A/%B/%C); 2-12 min linear to 1/99/0, 12-20 min hold 1/99/0, 20-20.5 min linear to 5/0/95, 20.5-26.1 5/0/95, 26.1-26.3 min linear to 100/0/0, 26.3-33 min hold 100/0/0 |
Flow Rate: | 0-20.5 min hold 0.25mL/min, [18 min switch flow direction to backflush], 20.5-21.5 linear to 0.4mL/min, 21.5-22.3 linear to 0.8 mL/min, [26 min switch flow direction to forward] 26-26.1 linear to 0.6mL/min, 26.1-26.3 linear to 0.4 mL/min, 26.3-31.8 min hold 0.4mL/min, 31.8-32 min linear to 0.25mL/min |
Solvent A: | 97% water/3% methanol; 10 mM tributylamine; 5mM acetic acid |
Solvent B: | 100% methanol; 10 mM tributylamine; 5mM acetic acid |
Chromatography Type: | Reversed phase |