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MB Sample ID: SA260824
Local Sample ID: | 90267016813 |
Subject ID: | SU002714 |
Subject Type: | Mammal |
Subject Species: | Rattus norvegicus |
Taxonomy ID: | 10116 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN004284 |
---|---|
Analysis type | MS |
Chromatography type | Reversed phase |
Chromatography system | Waters Acquity UPLC |
Column | Waters Acquity UPLC BEH C8 (150 x 2.1mm, 1.7um) |
MS Type | ESI |
MS instrument type | Triple quadrupole |
MS instrument name | Thermo TSQ Quantiva |
Ion Mode | POSITIVE |
Units | nano moles per vial |
Chromatography:
Chromatography ID: | CH003190 |
Chromatography Summary: | Analytes were chromatographically separated with 40 minutes LC gradient |
Methods Filename: | pass1b_amines_methods.pdf |
Instrument Name: | Waters Acquity UPLC |
Column Name: | Waters Acquity UPLC BEH C8 (150 x 2.1mm, 1.7um) |
Column Temperature: | 43C |
Flow Gradient: | t=0 min: 99.9%/0.1% (%A/%B) @ 0.4 ml/min | t=1 min: 99.9%/0.1% (%A/%B) @ 0.4 ml/min | t=2 min: 99.9%/0.1% (%A/%B) @ 0.4 ml/min | t=5.5 min: 98.1%/1.9% (%A/%B) @ 0.4 ml/min | t=6.5 min: 98%/2% (%A/%B) @ 0.4 ml/min | t=10 min: 97.5%/2.4% (%A/%B) @ 0.4 ml/min | t=12 min: 96%/4% (%A/%B) @ 0.4 ml/min | t=20 min: 88%/12% (%A/%B) @ 0.4 ml/min | t=27 min: 86.5%/13.5% (%A/%B) @ 0.4 ml/min | t=31 min: 80%/20% (%A/%B) @ 0.4 ml/min | t=32 min: 2%/98% (%A/%B) @ 0.5 ml/min | t=35 min: 2%/98% (%A/%B) @ 0.5 ml/min | t=35.5 min: 99.9%/0.1% (%A/%B) @ 0.4 ml/min | t=39 min: 99.9%/0.1% (%A/%B) @ 0.4 ml/min |
Flow Rate: | 0.4 ml/min; 0.5 ml/min |
Solvent A: | 1% acetonitrile/99% water; 0.1% formic acid |
Solvent B: | 1% water/99% acetonitrile |
Chromatography Type: | Reversed phase |