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MB Sample ID: SA317858
Local Sample ID: | s_Con_2 |
Subject ID: | SU003037 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Gender: | Not applicable |
Human Race: | Pacific asian |
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Combined analysis:
Analysis ID | AN004794 | AN004795 |
---|---|---|
Analysis type | MS | MS |
Chromatography type | Reversed phase | Reversed phase |
Chromatography system | Agilent 1290 Infinity | Agilent 1290 Infinity |
Column | Agilent Pursuit 5 C18 (150 x 2.0 mm, 5um) | Agilent Pursuit 5 C18 (150 x 2.0 mm, 5um) |
MS Type | ESI | ESI |
MS instrument type | QTRAP | QTRAP |
MS instrument name | ABI Sciex 5500 QTrap | ABI Sciex 5500 QTrap |
Ion Mode | POSITIVE | POSITIVE |
Units | pmol/mg | pmol/mg |
Chromatography:
Chromatography ID: | CH003625 |
Chromatography Summary: | Ceramides, sphingomyelines, sphinganine, sphingosine |
Instrument Name: | Agilent 1290 Infinity |
Column Name: | Agilent Pursuit 5 C18 (150 x 2.0 mm, 5um) |
Column Temperature: | 35 |
Flow Gradient: | 50 % of B at 0 min, 50 % of B for 5 min, 50-70 % of B for 3 min, 70 % of B for 7 min, 70-90 % of B for 7 min, 90 % of B for 3 min, 90-50 % of B for 0.1 min, 50 % of B for 4.9 min |
Flow Rate: | 200 uL/min |
Solvent A: | 5 mM ammonium formate/MeOH/tetrahydrofuran (500/200/300, v/v/v) |
Solvent B: | 5 mM ammonium formate/MeOH/ tetrahydrofuran (100/200/700, v/v/v) |
Chromatography Type: | Reversed phase |
Chromatography ID: | CH003626 |
Chromatography Summary: | diacylglycerols |
Instrument Name: | Agilent 1290 Infinity |
Column Name: | Agilent Pursuit 5 C18 (150 x 2.0 mm, 5um) |
Column Temperature: | 35 |
Flow Gradient: | 90 % of B for 0 min, 90 % of B for 6 min, 90 to 95 % of B for 0.6 min, 95 % of B for 3.4 min, 95 to 90 % of B for 0.1 min, and 90 % of B for 1.9 min |
Flow Rate: | 200 uL/min |
Solvent A: | 5 mM ammonium formate/MeOH/tetrahydrofuran (500/200/300, v/v/v) |
Solvent B: | 5 mM ammonium formate/MeOH/ tetrahydrofuran (100/200/700, v/v/v) |
Chromatography Type: | Reversed phase |