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MB Sample ID: SA332320

Local Sample ID:T3_6
Subject ID:SU003189
Subject Type:Synthetic sample

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Combined analysis:

Analysis ID AN005032
Analysis type MS
Chromatography type Reversed phase
Chromatography system Thermo Vanquish
Column Merck Supelco Ascentis Express C18 (150 x 2.1mm,2.7um)
MS Type ESI
MS instrument type Orbitrap
MS instrument name Thermo Q Exactive Orbitrap
Ion Mode POSITIVE
Units NA

Chromatography:

Chromatography ID:CH003803
Methods Filename:C18_LC_Conditions.pdf
Instrument Name:Thermo Vanquish
Column Name:Merck Supelco Ascentis Express C18 (150 x 2.1mm,2.7um)
Column Temperature:30
Flow Gradient:0–5 min: gradient was held at 5% B; 2–12.1 min: linear gradient of 5% to 95% B; 12.1–17.0 min: 95% B; 17.1–21.0 min: gradient was returned to 5% B
Flow Rate:0.25 ml/min
Solvent A:100% water; 0.1% formic acid
Solvent B:100% acetonitrile; 0.1% formic acid
Chromatography Type:Reversed phase
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