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MB Sample ID: SA333653
Local Sample ID: | SUB13607p4_SPL09 |
Subject ID: | SU003221 |
Subject Type: | Cultured cells |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN005085 |
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Analysis type | MS |
Chromatography type | HILIC |
Chromatography system | Thermo Vanquish |
Column | Merck SeQuant ZIC-HILIC (150 x 2.1mm,5um) |
MS Type | ESI |
MS instrument type | Orbitrap |
MS instrument name | Thermo Orbitrap ID-X tribrid |
Ion Mode | UNSPECIFIED |
Units | area analyzed by Compound discoverer (counts x seconds) |
Chromatography:
Chromatography ID: | CH003841 |
Instrument Name: | Thermo Vanquish |
Column Name: | Merck SeQuant ZIC-HILIC (150 x 2.1mm,5um) |
Column Temperature: | 40 |
Flow Gradient: | Started at 93% B and 7% A ; 40% B/60% A in 19 min; 100% A in 9 min; 100% A for 5 min; back to 93% B/7% A in 3 min; re-equilibration at 93% B/7% A for 9 min. |
Flow Rate: | 0.05 to 0.15 mL/min in 30 sec; then held at 0.15mL/min |
Solvent A: | 100% Water; 20 mMAmmonium Carbonate, 0.1% Ammonium hydroxide |
Solvent B: | Acetonitrile 97%, 3% water |
Chromatography Type: | HILIC |