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MB Sample ID: SA343101
| Local Sample ID: | 21219108 |
| Subject ID: | SU003290 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Age Or Age Range: | >14 days, |
| Gender: | Male and female |
| Human Inclusion Criteria: | >14 days, MSUD sick patients DBS |
| Human Exclusion Criteria: | </=14 days, any IEM's sick other than MSUD, unknown gender |
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Combined analysis:
| Analysis ID | AN005204 | AN005205 |
|---|---|---|
| Analysis type | MS | MS |
| Chromatography type | Reversed phase | Reversed phase |
| Chromatography system | Waters Acquity UPLC | Waters Acquity UPLC |
| Column | Waters XSelect CSH C18 (100 x 2.1mm 2.5um) | Waters XSelect CSH C18 (100 x 2.1mm 2.5um) |
| MS Type | ESI | ESI |
| MS instrument type | QTOF | QTOF |
| MS instrument name | Waters Xevo-G2-S | Waters Xevo-G2-S |
| Ion Mode | POSITIVE | NEGATIVE |
| Units | Peak area | Peak area |
Chromatography:
| Chromatography ID: | CH003938 |
| Methods Filename: | MSUD_LC_MS_Metabolomics.pdf |
| Instrument Name: | Waters Acquity UPLC |
| Column Name: | Waters XSelect CSH C18 (100 x 2.1mm 2.5um) |
| Column Temperature: | 55 |
| Flow Gradient: | 95–5% A [0–16 min], 5% A [16–19 min], 5–95% A [19–20 min], and 95–95% A [20–22 min]. |
| Flow Rate: | 300 μL/min |
| Solvent A: | 100% water; 0.1% formic acid |
| Solvent B: | 50% MeOH/50% ACN; 0.1% formic acid |
| Chromatography Type: | Reversed phase |
