Summary of Study ST000825
This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR000587. The data can be accessed directly via it's Project DOI: 10.21228/M8SQ3D This work is supported by NIH grant, U2C- DK119886.
See: https://www.metabolomicsworkbench.org/about/howtocite.php
Study ID | ST000825 |
Study Title | CHEAR Christiani Biocrates |
Study Summary | Human cord blood serum samples (200) were provided by David Christiani. The 200 study samples, total pool samples, and external CHEAR Plasma Reference Material samples were prepared and analyzed using the Biocrates AbsoluteIDQ p180 Kit. |
Institute | RTI International |
Department | ACP |
Laboratory | RTI CHEAR Analytical Hub - Untargeted Analysis Resource Core (UARC) |
Last Name | Fennell |
First Name | Timothy |
Address | 3040 E Cornwallis Rd, Durham, North Carolina, 27709, USA |
fennell@rti.org | |
Phone | 919-485-2781 |
Submit Date | 2017-07-18 |
Total Subjects | 200 |
Study Comments | CHEAR Plasma Reference Material samples were aliquots of sub-aliquots that came from parent aliquots that were made from original stock. |
Raw Data Available | Yes |
Raw Data File Type(s) | wiff |
Chear Study | Yes |
Analysis Type Detail | LC-MS |
Release Date | 2019-09-23 |
Release Version | 1 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN001311 | AN001312 | AN001313 |
---|---|---|---|
Analysis type | MS | MS | MS |
Chromatography type | Reversed phase | Isocratic | Isocratic |
Chromatography system | Agilent 1100 | Agilent 1100 | Agilent 1100 |
Column | Agilent Eclipse XDB-C18 (100 x 3.0mm,3.5um) | no column | no column |
MS Type | ESI | ESI | ESI |
MS instrument type | Triple quadrupole | Triple quadrupole | Triple quadrupole |
MS instrument name | ABI Sciex 4000 QTrap | ABI Sciex 4000 QTrap | ABI Sciex 4000 QTrap |
Ion Mode | POSITIVE | POSITIVE | NEGATIVE |
Units | uM | uM | uM |
Chromatography:
Chromatography ID: | CH000918 |
Chromatography Summary: | Reverse Phase Gradient separation |
Instrument Name: | Agilent 1100 |
Column Name: | Agilent Eclipse XDB-C18 (100 x 3.0mm,3.5um) |
Column Pressure: | 30-120 bar |
Column Temperature: | 50°C |
Flow Rate: | 0.5 mL/min |
Sample Injection: | 10 µL |
Target Sample Temperature: | 10 °C |
Sample Loop Size: | 100 µL |
Randomization Order: | Yes |
Chromatography Type: | Reversed phase |
Chromatography ID: | CH000919 |
Chromatography Summary: | FIA analysis |
Instrument Name: | Agilent 1100 |
Column Name: | no column |
Sample Injection: | 20 µL |
Target Sample Temperature: | 10 °C |
Sample Loop Size: | 100 µL |
Randomization Order: | Yes |
Chromatography Type: | Isocratic |