Summary of Study ST001712
This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR001096. The data can be accessed directly via it's Project DOI: 10.21228/M81M6P This work is supported by NIH grant, U2C- DK119886.
See: https://www.metabolomicsworkbench.org/about/howtocite.php
Study ID | ST001712 |
Study Title | Metabolomics analysis of plasma from a mouse model of astrocytoma subjected to radiotherapy |
Study Summary | Mice were randomized in two groups (n=9 mice/group), one group was subjected to radiotherapy (Monday and Friday for 2 consecutive weeks at 3Gy/session) and the other cohort was the control. Sample were taken approximately each 10 days from the tail vein. |
Institute | National Cancer Institute |
Last Name | Larion |
First Name | Mioara |
Address | 37 Convent Dr, Building 37 Room 1136 |
mioara.larion@nih.gov | |
Phone | 2407606825 |
Submit Date | 2021-02-26 |
Analysis Type Detail | LC-MS |
Release Date | 2021-03-09 |
Release Version | 1 |
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Combined analysis:
Analysis ID | AN002787 |
---|---|
Analysis type | MS |
Chromatography type | HILIC |
Chromatography system | Agilent 6545 QTOF-MS |
Column | AdvanceBio Glycan Map (2.1 x 100mm, 2.7µm) |
MS Type | ESI |
MS instrument type | QTOF |
MS instrument name | Agilent 6540 QTOF |
Ion Mode | NEGATIVE |
Units | arbitrary units |
Chromatography:
Chromatography ID: | CH002062 |
Instrument Name: | Agilent 6545 QTOF-MS |
Column Name: | AdvanceBio Glycan Map (2.1 x 100mm, 2.7µm) |
Column Temperature: | 35 |
Flow Gradient: | 100% B, 0.5 min; 95% B, 2.0 min; 60% B, 3.0 min; 35% B, 5 min; hold 0.25 min; 0% B, 6 min; hold 0.5 min; 100% B, 7.8 min; equilibrate for 1.7 min. |
Flow Rate: | 0.2 mL/min |
Solvent A: | 88% water/12% acetonitrile; 10 mM ammonium acetate; titrated with formic acid and ammonium hydroxide to pH 6.85 |
Solvent B: | 90% acetonitrile/10% water; 10 mM ammonium acetate; titrated with formic acid and ammonium hydroxide to pH 6.85 |
Chromatography Type: | HILIC |