Summary of Study ST000163
This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR000141. The data can be accessed directly via it's Project DOI: 10.21228/M8R59V This work is supported by NIH grant, U2C- DK119886.
See: https://www.metabolomicsworkbench.org/about/howtocite.php
This study contains a large results data set and is not available in the mwTab file. It is only available for download via FTP as data file(s) here.
Study ID | ST000163 |
Study Title | Metabolomics of 50 healthy humans and common marmosets (MetabNet) |
Study Type | Healthy subjects |
Institute | Emory University |
Department | Department of Medicine |
Laboratory | Clinical Biomarkers Laboratory |
Last Name | Uppal |
First Name | Karan |
Address | Whitehead Biomedical Research Building, Rm 225, 621 Michael Street, Atlanta, GA 30322 |
kuppal2@emory.edu | |
Submit Date | 2015-04-27 |
Total Subjects | 100 |
Raw Data Available | Yes |
Raw Data File Type(s) | cdf, raw(Thermo) |
Uploaded File Size | 59 G |
Analysis Type Detail | LC-MS |
Release Date | 2015-04-28 |
Release Version | 1 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN000255 |
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Analysis type | MS |
Chromatography type | Anion exchange/Reversed phase |
Chromatography system | Thermo Accela CTC |
Column | Higgins C18 (100 x 2.1mm,5um); Hamilton Anion Exchange 100x2.1mm,7um |
MS Type | ESI |
MS instrument type | Single quadrupole |
MS instrument name | Thermo LTQ |
Ion Mode | POSITIVE |
Units | Intensity |
Chromatography:
Chromatography ID: | CH000180 |
Chromatography Summary: | untargeted dual chromatography (C18 and Anion Exchange column) |
Methods ID: | Methods_LTQVelosOrbi |
Methods Filename: | Methods_LTQVelosOrbi |
Instrument Name: | Thermo Accela CTC |
Column Name: | Higgins C18 (100 x 2.1mm,5um); Hamilton Anion Exchange 100x2.1mm,7um |
Column Pressure: | 200 Bar (max) |
Column Temperature: | 30 |
Flow Gradient: | C18: A% = 5% for 10 minutes, 0-2mins = 60% B, 2-6mins = gradient to 95% B, 6-10mins = 95% B; AE: 1-10mins = 50%B, 0-2mins = 5%A, 2-7mins = gradient to 50%A, 7-10mins = 50%A |
Flow Rate: | 0.35 mL/min |
Injection Temperature: | 4C |
Sample Injection: | 10ul |
Sampling Cone: | ESI |
Solvent A: | 100% water; 0.2% formic acid |
Solvent B: | 100% acetonitrile |
Analytical Time: | LC grade water |
Capillary Voltage: | 10 minutes |
Migration Time: | 100uA (source current) |
Sheath Liquid: | 4.5kV (source voltage) |
Weak Wash Solvent Name: | water with 10% methanol |
Sample Syringe Size: | 20ul |
Chromatography Type: | Anion exchange/Reversed phase |