Summary of Study ST001037
This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR000694. The data can be accessed directly via it's Project DOI: 10.21228/M8ZT2M This work is supported by NIH grant, U2C- DK119886.
See: https://www.metabolomicsworkbench.org/about/howtocite.php
Study ID | ST001037 |
Study Title | High Resolution GC-MS and FID Metabolomics of Human Serum |
Study Type | Human Serum Analysis |
Study Summary | We explored the possibility of performing quantitative metabolomics using a QEGC-MS using both FID and MS detectors as complementary techniques. |
Institute | Wake Forest Baptist Medical Center |
Department | Center for Precision Medicine |
Laboratory | Michael Olivier Laboratory |
Last Name | Misra |
First Name | Biswapriya |
Address | Medical Center Boulevard NRC Building, G#43, Medical Center Boulevard, Winston Salem, NC, 27157, USA |
bbmisraccb@gmail.com | |
Phone | 3522156040 |
Submit Date | 2018-08-13 |
Total Subjects | 1 |
Num Males | 1 |
Study Comments | NA |
Publications | In process |
Raw Data Available | Yes |
Raw Data File Type(s) | raw(Thermo) |
Analysis Type Detail | GC-MS |
Release Date | 2019-01-22 |
Release Version | 1 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN001698 |
---|---|
Analysis type | MS |
Chromatography type | GC |
Chromatography system | QEOrbitrap-GC-MS |
Column | TraceGOLD TG-5SILMS |
MS Type | EI |
MS instrument type | Orbitrap |
MS instrument name | Thermo Q Exactive Orbitrap |
Ion Mode | POSITIVE |
Units | Abundance |
Chromatography:
Chromatography ID: | CH001197 |
Chromatography Summary: | A robotic arm TriPlus™ RSH autosampler (Thermo Scientific™, Bremen, Germany) injected 1µL of derivatized sample into a split/splitless (SSL) injector at 250 °C using a 1:100 split flow on TRACE™ 1310 gas chromatograph (Thermo Scientific™, Austin, TX). Helium carrier gas at a flow rate of 1 mL/min was used for separation on a Thermo Scientific™ TraceGOLD™ TG-5SILMS 30 m length × 0.25 mm i.d. × 0.25 µm film thickness column. The initial oven temperature was held at 70 °C for 4 min, followed by an initial gradient of 20 °C/min ramp rate. The final temperature was 320 °C and held for 8 min. |
Instrument Name: | QEOrbitrap-GC-MS |
Column Name: | TraceGOLD TG-5SILMS |
Chromatography Type: | GC |