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MB Sample ID: SA099426
| Local Sample ID: | P17_t0 |
| Subject ID: | SU001443 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN002283 | AN002284 | AN002285 |
|---|---|---|---|
| Analysis type | MS | MS | MS |
| Chromatography type | Reversed phase | Reversed phase | GC |
| Chromatography system | Agilent 1200 | Agilent 1200 | Agilent 7890A |
| Column | Discovery HS C18 (150 x 2.1mm,3.0um) Supelco,Sigma Aldrich,Germany),with a guard Discovery HS C18 (2 cm x 2.1mm,3um; Supelco,Sigma Aldrich,Germany), | Discovery HS C18 (150 x 2.1mm,3.0um) Supelco,Sigma Aldrich,Germany) | GC-Column DB5-MS (30 m length, 0.25 mm i.d., 0.25 μm film 95% dimethyl/5% diphenylpolysiloxane) with an integrated precolumn (10 m J&W, Agilent) |
| MS Type | ESI | ESI | EI |
| MS instrument type | QTOF | QTOF | Single quadrupole |
| MS instrument name | Agilent 6520 QTOF | Agilent 6520 QTOF | Agilent 5975C |
| Ion Mode | POSITIVE | NEGATIVE | POSITIVE |
| Units | peak area | peak area | peak area |
MS:
| MS ID: | MS002127 |
| Analysis ID: | AN002283 |
| Instrument Name: | Agilent 6520 QTOF |
| Instrument Type: | QTOF |
| MS Type: | ESI |
| MS Comments: | LC−MS analysis was performed on an Agilent HPLC system (1200 series, Agilent Technologies, Waldbronn, Germany), equipped with a degasser, two binary pumps, and a thermostated autosampler coupled with quadrupole-time of flight analyzer (Q-TOF), LC-MS (6520) system (Agilent Technologies, Waldbronn, Germany) |
| Ion Mode: | POSITIVE |
| Capillary Voltage: | 3,500 for ESI (+) |
| Dry Gas Flow: | 10.5 L/min |
| Dry Gas Temp: | 330 °C |
| Fragment Voltage: | 175 V |
| Nebulizer: | 52 psi |
| Octpole Voltage: | 750V |
| MS ID: | MS002128 |
| Analysis ID: | AN002284 |
| Instrument Name: | Agilent 6520 QTOF |
| Instrument Type: | QTOF |
| MS Type: | ESI |
| MS Comments: | LC−MS analysis was performed on an Agilent HPLC system (1200 series, Agilent Technologies, Waldbronn, Germany), equipped with a degasser, two binary pumps, and a thermostated autosampler coupled with quadrupole-time of flight analyzer (Q-TOF), LC-MS (6520) system (Agilent Technologies, Waldbronn, Germany) |
| Ion Mode: | NEGATIVE |
| Capillary Voltage: | 4,000V for ESI (−) |
| Dry Gas Flow: | 10.5 L/min |
| Dry Gas Temp: | 330 °C |
| Fragment Voltage: | 175 V |
| Nebulizer: | 52 psi |
| Octpole Voltage: | 750V |
| MS ID: | MS002129 |
| Analysis ID: | AN002285 |
| Instrument Name: | Agilent 5975C |
| Instrument Type: | Single quadrupole |
| MS Type: | EI |
| MS Comments: | GC-MS analysis was performed by a GC system (Agilent Technologies 7890A) equipped with an autosampler (Agilent 7693) coupled to a mass spectrometer with triple-Axis detector (5975C, Agilent). |
| Ion Mode: | POSITIVE |
| Helium Flow: | 1 mL/min |
| Ionization Energy: | -70 eV |
