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MB Sample ID: SA099448
Local Sample ID: | P30_t2 |
Subject ID: | SU001443 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
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Combined analysis:
Analysis ID | AN002283 | AN002284 | AN002285 |
---|---|---|---|
Analysis type | MS | MS | MS |
Chromatography type | Reversed phase | Reversed phase | GC |
Chromatography system | Agilent 1200 | Agilent 1200 | Agilent 7890A |
Column | Discovery HS C18 (150 x 2.1mm,3.0um) Supelco,Sigma Aldrich,Germany),with a guard Discovery HS C18 (2 cm x 2.1mm,3um; Supelco,Sigma Aldrich,Germany), | Discovery HS C18 (150 x 2.1mm,3.0um) Supelco,Sigma Aldrich,Germany) | GC-Column DB5-MS (30 m length, 0.25 mm i.d., 0.25 μm film 95% dimethyl/5% diphenylpolysiloxane) with an integrated precolumn (10 m J&W, Agilent) |
MS Type | ESI | ESI | EI |
MS instrument type | QTOF | QTOF | Single quadrupole |
MS instrument name | Agilent 6520 QTOF | Agilent 6520 QTOF | Agilent 5975C |
Ion Mode | POSITIVE | NEGATIVE | POSITIVE |
Units | peak area | peak area | peak area |
MS:
MS ID: | MS002127 |
Analysis ID: | AN002283 |
Instrument Name: | Agilent 6520 QTOF |
Instrument Type: | QTOF |
MS Type: | ESI |
MS Comments: | LC−MS analysis was performed on an Agilent HPLC system (1200 series, Agilent Technologies, Waldbronn, Germany), equipped with a degasser, two binary pumps, and a thermostated autosampler coupled with quadrupole-time of flight analyzer (Q-TOF), LC-MS (6520) system (Agilent Technologies, Waldbronn, Germany) |
Ion Mode: | POSITIVE |
Capillary Voltage: | 3,500 for ESI (+) |
Dry Gas Flow: | 10.5 L/min |
Dry Gas Temp: | 330 °C |
Fragment Voltage: | 175 V |
Nebulizer: | 52 psi |
Octpole Voltage: | 750V |
MS ID: | MS002128 |
Analysis ID: | AN002284 |
Instrument Name: | Agilent 6520 QTOF |
Instrument Type: | QTOF |
MS Type: | ESI |
MS Comments: | LC−MS analysis was performed on an Agilent HPLC system (1200 series, Agilent Technologies, Waldbronn, Germany), equipped with a degasser, two binary pumps, and a thermostated autosampler coupled with quadrupole-time of flight analyzer (Q-TOF), LC-MS (6520) system (Agilent Technologies, Waldbronn, Germany) |
Ion Mode: | NEGATIVE |
Capillary Voltage: | 4,000V for ESI (−) |
Dry Gas Flow: | 10.5 L/min |
Dry Gas Temp: | 330 °C |
Fragment Voltage: | 175 V |
Nebulizer: | 52 psi |
Octpole Voltage: | 750V |
MS ID: | MS002129 |
Analysis ID: | AN002285 |
Instrument Name: | Agilent 5975C |
Instrument Type: | Single quadrupole |
MS Type: | EI |
MS Comments: | GC-MS analysis was performed by a GC system (Agilent Technologies 7890A) equipped with an autosampler (Agilent 7693) coupled to a mass spectrometer with triple-Axis detector (5975C, Agilent). |
Ion Mode: | POSITIVE |
Helium Flow: | 1 mL/min |
Ionization Energy: | -70 eV |