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MB Sample ID: SA154970
Local Sample ID: | qc17 |
Subject ID: | SU001759 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Age Or Age Range: | 19-87 |
Gender: | Male and female |
Human Race: | Caucasian |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN002746 |
---|---|
Analysis type | MS |
Chromatography type | Reversed phase |
Chromatography system | Shimadzu 20AD |
Column | Waters Acquity BEH C18 (100 x 2mm,1.7um) |
MS Type | ESI |
MS instrument type | Other |
MS instrument name | Shimadzu LCMS-IT-TOF |
Ion Mode | POSITIVE |
Units | area |
MS:
MS ID: | MS002543 |
Analysis ID: | AN002746 |
Instrument Name: | Shimadzu LCMS-IT-TOF |
Instrument Type: | Other |
MS Type: | ESI |
MS Comments: | The apparatus consisted of a two LC-20AD pumps (Shimadzu, Japan), an automatic sample injector, coupled on-line with an LCMS-IT-TOF (Shimadzu, Japan) mass spectrometer. The column effluent was analyzed by ESI-MS. MS detection was operated in positive ionisation mode with the following parameters: detector voltage, 1.53 kV; interface voltage, +4.5 kV; CDL (curve desolvation line) temperature, 200 ˚C; block heater temperature, 200 ˚C; nebulizing gas flow (He), 1.5 L/min; drying gas pressure, 100 kPa. Full scan MS data were acquired in the range of 80–850 m/z (ion accumulation time, 30 ms; event time, 300 ms; repeat = 3. |
Ion Mode: | POSITIVE |
Capillary Voltage: | +4.5 kV |
Dry Gas Flow: | 100 kPa |
Helium Flow: | 1.5 ml/min |
Ion Source Temperature: | 200 ˚C |
Ionization: | positive |
Mass Accuracy: | 15 ppm |
Source Temperature: | 200 ˚C |
Cdl Temperature: | 200 ˚C |