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MB Sample ID: SA162664
| Local Sample ID: | POL-36 |
| Subject ID: | SU001811 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN002823 |
|---|---|
| Analysis type | MS |
| Chromatography type | HILIC |
| Chromatography system | Agilent 1260 |
| Column | Phenomenex Kinetex HILIC 100A (50 x 2.1 mm,2.6um) |
| MS Type | ESI |
| MS instrument type | Triple quadrupole |
| MS instrument name | Agilent 6470 QQQ |
| Ion Mode | NEGATIVE |
| Units | ug/mg |
MS:
| MS ID: | MS002617 |
| Analysis ID: | AN002823 |
| Instrument Name: | Agilent 6470 QQQ |
| Instrument Type: | Triple quadrupole |
| MS Type: | ESI |
| MS Comments: | The MS conditions were: 5500 V of capillary voltage in positive ESI mode, a nebulizer gas flow rate of 11.0 L/min; a source temperature of 250 °C; and a source pressure of 60 psi. The sample tray temperature was maintained at 4 °C. Each transition was optimized adjusting the fragmentor and collision energy voltages. Data were acquired in MassHunter Workstation B.05.00 (Agilent Technologies), and re-processed using MassHunter QQQ Quantitative Analysis B.08.00 (Agilent) where peak areas were integrated. Concentration of metabolites were calculated using calibration curves with the standard addition method. |
| Ion Mode: | NEGATIVE |
