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MB Sample ID: SA162668
Local Sample ID: | POL-14 |
Subject ID: | SU001811 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
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Combined analysis:
Analysis ID | AN002823 |
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Analysis type | MS |
Chromatography type | HILIC |
Chromatography system | Agilent 1260 |
Column | Phenomenex Kinetex HILIC 100A (50 x 2.1 mm,2.6um) |
MS Type | ESI |
MS instrument type | Triple quadrupole |
MS instrument name | Agilent 6470 QQQ |
Ion Mode | NEGATIVE |
Units | ug/mg |
MS:
MS ID: | MS002617 |
Analysis ID: | AN002823 |
Instrument Name: | Agilent 6470 QQQ |
Instrument Type: | Triple quadrupole |
MS Type: | ESI |
MS Comments: | The MS conditions were: 5500 V of capillary voltage in positive ESI mode, a nebulizer gas flow rate of 11.0 L/min; a source temperature of 250 °C; and a source pressure of 60 psi. The sample tray temperature was maintained at 4 °C. Each transition was optimized adjusting the fragmentor and collision energy voltages. Data were acquired in MassHunter Workstation B.05.00 (Agilent Technologies), and re-processed using MassHunter QQQ Quantitative Analysis B.08.00 (Agilent) where peak areas were integrated. Concentration of metabolites were calculated using calibration curves with the standard addition method. |
Ion Mode: | NEGATIVE |