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MB Sample ID: SA170988
Local Sample ID: | SER_g1 _Subcutaneous1_2h |
Subject ID: | SU001915 |
Subject Type: | Mammal |
Subject Species: | Mus musculus |
Taxonomy ID: | 10090 |
Genotype Strain: | albino C57BL/6 |
Age Or Age Range: | 6-8 weeks |
Gender: | Female |
Animal Animal Supplier: | Jackson Laboratories (Bar Harbor, ME) |
Animal Housing: | NCI-Bethesda Animal Facility |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN002980 |
---|---|
Analysis type | MS |
Chromatography type | HILIC |
Chromatography system | Agilent 1290 Infinity II |
Column | Agilent AdvanceBio Glycan Map 2.1 x 100 mm 2.7µm column |
MS Type | ESI |
MS instrument type | QTOF |
MS instrument name | Agilent 6545 QTOF |
Ion Mode | POSITIVE |
Units | ng |
MS:
MS ID: | MS002770 |
Analysis ID: | AN002980 |
Instrument Name: | Agilent 6545 QTOF |
Instrument Type: | QTOF |
MS Type: | ESI |
MS Comments: | MS/MS Using Masshunter Qtof Quant-My-Way 10.0 software, GSK126 was detected at elution time 2.6 min using precursor ion m/z 527.3129 and transition m/z 375.2183 generated via N2 gas collision-induced fragmentation (CID) at a collision energy (CE) of 12 V. Internal standard (IS) debrisoquine detected at elution time of 2.5 mins with precursor m/z 176.1182 and transition m/z 134.0964 generated at CE 12V. |
Ion Mode: | POSITIVE |
Capillary Temperature: | 325°C |
Capillary Voltage: | 3kV |
Collision Energy: | 12V |
Collision Gas: | N2 |
Dry Gas Flow: | 9 L/min |
Dry Gas Temp: | 250°C |
Fragment Voltage: | 100 V |
Fragmentation Method: | MS/MS |
Ion Source Temperature: | 325°C |
Mass Accuracy: | 2 kDa |
Source Temperature: | 325°C |
Cdl Temperature: | RT |
Desolvation Temperature: | 325°C |
Nebulizer: | 45 psig |
Octpole Voltage: | 750V |