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MB Sample ID: SA171012
| Local Sample ID: | LLN_g1 _Intra4_6h |
| Subject ID: | SU001915 |
| Subject Type: | Mammal |
| Subject Species: | Mus musculus |
| Taxonomy ID: | 10090 |
| Genotype Strain: | albino C57BL/6 |
| Age Or Age Range: | 6-8 weeks |
| Gender: | Female |
| Animal Animal Supplier: | Jackson Laboratories (Bar Harbor, ME) |
| Animal Housing: | NCI-Bethesda Animal Facility |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN002980 |
|---|---|
| Analysis type | MS |
| Chromatography type | HILIC |
| Chromatography system | Agilent 1290 Infinity II |
| Column | Agilent AdvanceBio Glycan Map 2.1 x 100 mm 2.7µm column |
| MS Type | ESI |
| MS instrument type | QTOF |
| MS instrument name | Agilent 6545 |
| Ion Mode | POSITIVE |
| Units | ng |
MS:
| MS ID: | MS002770 |
| Analysis ID: | AN002980 |
| Instrument Name: | Agilent 6545 |
| Instrument Type: | QTOF |
| MS Type: | ESI |
| MS Comments: | MS/MS Using Masshunter Qtof Quant-My-Way 10.0 software, GSK126 was detected at elution time 2.6 min using precursor ion m/z 527.3129 and transition m/z 375.2183 generated via N2 gas collision-induced fragmentation (CID) at a collision energy (CE) of 12 V. Internal standard (IS) debrisoquine detected at elution time of 2.5 mins with precursor m/z 176.1182 and transition m/z 134.0964 generated at CE 12V. |
| Ion Mode: | POSITIVE |
| Capillary Temperature: | 325°C |
| Capillary Voltage: | 3kV |
| Collision Energy: | 12V |
| Collision Gas: | N2 |
| Dry Gas Flow: | 9 L/min |
| Dry Gas Temp: | 250°C |
| Fragment Voltage: | 100 V |
| Fragmentation Method: | MS/MS |
| Ion Source Temperature: | 325°C |
| Mass Accuracy: | 2 kDa |
| Source Temperature: | 325°C |
| Cdl Temperature: | RT |
| Desolvation Temperature: | 325°C |
| Nebulizer: | 45 psig |
| Octpole Voltage: | 750V |
